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Yomogida, Takumi; Hashimoto, Tadashi; Okumura, Takuma*; Yamada, Shinya*; Tatsuno, Hideyuki*; Noda, Hirofumi*; Hayakawa, Ryota*; Okada, Shinji*; Takatori, Sayuri*; Isobe, Tadaaki*; et al.
Analyst, 149(10), p.2932 - 2941, 2024/03
In this study, we successfully applied a transition-edge sensor (TES) spectrometer as a detector for microbeam X-ray measurements from a synchrotron X-ray light source to determine uranium (U) distribution at the micro-scale and its chemical species in biotite obtained from the U mine. It is difficult to separate the fluorescent X-ray of the U L
line at 13.615 keV from that of the Rb K line at 13.395 keV in the X-ray fluorescence spectrum with an energy resolution of approximately 220 eV of the conventional silicon drift detector (SDD). Meanwhile, the fluorescent X-rays of U L and Rb K were fully separated by TES with 50 eV energy resolution at the energy of around 13 keV. The successful peak separation by TES led to an accurate mapping analysis of trace U in micro-X-ray fluorescence measurements and a decrease in the signal-to-background ratio in micro-X-ray absorption near edge structure spectroscopy.
Kikuchi, Kenji*; Okada, Noriyuki*; Kato, Mikio*; Uchida, Hiroshi*; Saito, Shigeru
Journal of Nuclear Materials, 450(1-3), p.237 - 243, 2014/07
Times Cited Count：3 Percentile：23.66(Materials Science, Multidisciplinary)Three-dimensional atom probe techniques were applied to the investigation on the oxide scale in 12Cr ferritic-martensitic steel, HCM12A. A duplex oxide scale was formed in lead bismuth eutectic at 450-500
C, during 5500 h. Samples were located 500-700 nm away from the boundary between magnetite and Fe-Cr spinel layers, while the total oxide layer thickness is 18 
m. It detected super enrichment of Cr with a size of ten nm roughly, as well as depletion of Fe and enrichment of O at the same site. Surrounding the Cr super enrichment area, enrichment of Si was newly noticed due to the scanned profile of detected atom counts. It is also confirmed that Pb and Bi concentration in the observed spinel region is almost null or less than 0.01 atomic percent, which is possible detecting lowest limit.
Kitagishi, Shigeru; Endo, Yasuichi; Okada, Yuji; Hanawa, Hiroshi; Matsui, Yoshinori
UTNL-R-0486, p.7_1 - 7_10, 2014/03
no abstracts in English
Matsumura, Hiroyoshi*; Adachi, Motoyasu; Sugiyama, Shigeru*; Okada, Shino*; Yamakami, Megumi*; Tamada, Taro; Hidaka, Koshi*; Hayashi, Yoshio*; Kimura, Toru*; Kiso, Yoshiaki*; et al.
Acta Crystallographica Section F, 64(11), p.1003 - 1006, 2008/11
Times Cited Count：17 Percentile：77.78(Biochemical Research Methods)This paper reports the crystallization and preliminary neutron diffraction measurements of HIV-1 protease, a potential target for anti-HIV therapy, complexed with an inhibitor (KNI-272). The aim of this neutron diffraction study is to obtain structural information about the H atoms and to determine the protonation states of the residues within the active site. The crystal was grown to a size of 1.4 mm
by repeated macroseeding and a slow-cooling method using a two-liquid system. Neutron diffraction data were collected at room temperature using a BIX-4 diffractometer at the JRR-3 research reactor of the Japan Atomic Energy Agency (JAEA). The data set was integrated and scaled to 2.3 
resolution in space group P2(1)2(1)2, with unit-cell parameters a = 59.5, b = 87.4, c = 46.8 .
Kagohara, Kyoko*; Imaizumi, Toshifumi*; Miyauchi, Takahiro*; Sato, Hiroshi*; Uchida, Takuma*; Echigo, Tomoo*; Ishiyama, Tatsuya*; Matsuta, Nobuhisa*; Okada, Shinsuke*; Ikeda, Yasutaka*; et al.
Chigaku Zasshi, 115(6), p.691 - 714, 2006/12
The eastern marginal fault zone of the Yokote Basin is one of seismogenic reverse faults developed in Northeast Japan, generating the 1896 Riku-u Earthquake (M7.2). We discussed the relationship among fault traces, geomorphic displacements and fault geometries on the Senya fault, based on a data from high-resolution seismic reflection profiling, investigations in tectonic geomorphology and structural geology, with the help of the balanced cross section method. By the restoring the balanced cross sections, the horizontal shortening amount is estimated to be totally 3 km through the thrust system, and the thrusting is retroactive to 2.4 Ma. Depending on the strike of fault traces and the morphotectonic features, the Senya fault is subdivided into three, the northern, central and southern portion. The initiation of thrust front migration is ca.1.6 Ma at the central portion and 0.6 Ma at the northern portion. This means that the central portion preceded the northern portion as an emergent fault, and suggests that the initial propagated fault extends from the fault end to the boundary fault.
Takeuchi, Sukune*; Okada, Shigeru*; Kobayash, Naoki*; *; Oya, Naohiko*; *
PNC TJ7552 97-001, 220 Pages, 1997/02
no abstracts in English
Takeuchi, Sukune*; Okada, Shigeru*; Kobayash, Naoki*; *; Oya, Naohiko*; *
PNC TJ7552 96-002, 328 Pages, 1996/03
None
Kitagishi, Shigeru; Endo, Yasuichi; Okada, Yuji; Hanawa, Hiroshi; Matsui, Yoshinori; Tsuchiya, Kunihiko; Yamaura, Takayuki
no journal, ,
no abstracts in English
Hasegawa, Noboru*; Nishikino, Masaharu*; Mikami, Katsuhiro*; Okada, Hajime*; Kondo, Shuji*; Kawachi, Tetsuya*; Shimada, Yoshinori*; Kurahashi, Shinri*; Kitamura, Toshiyuki*; Kotyaev, O.*; et al.
no journal, ,
no abstracts in English
