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Report No.
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Quantitative analysis on the surface of Lithium-6 enriched lithium titanate using proton RBS (Cooperative research)

Kubota, Naoyoshi; Fujiwara, Yoshio*; Okumura, Kazutaka*; Ochiai, Kentaro; Kitamura, Akira*; Furuyama, Yuichi*; Taniike, Akira*; Nishitani, Takeo

Surface analysis of lithium-6 ($$^{6}$$Li) was performed for both 95 % and 40 % $$^{6}$$Li-enriched lithium titanate (Li$$_{2}$$TiO$$_{3}$$) samples as the candidate tritium breeding material using 2.6 MeV-proton Rutherford Backscattering Spectroscopy (RBS). The depth resolution of this method was enough to measure the $$^{6}$$Li depth profile in terms of the evaluation of thermal neutron transportation. The atomic density of $$^{6}$$Li could be measured within the error of 27 % for both samples although the accuracy of 5 % was not achieved for the evaluation of tritium breeding. It was confirmed that the sample atomic compositions agreed with Li$$_{2}$$TiO$$_{3}$$ within errors of 30 % for Li/Ti and 15 % for O/Ti. The whole errors were caused by the data accuracy of scattering cross sections predominately. Providing more accurate cross section data can lead to the utilization of the RBS method for tritium breeding materials analysis.

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