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Report No.
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Recent development of soft-X-ray emission spectroscopy instruments for a conventional analytical transmission electron microscope

Terauchi, Masami*; Koike, Masato

Characterization with nm-scale spatial resolution is important for developments of new functional materials. Information of electronic structure of valence electrons (bonding electrons) is imperative for characterizing a material. A soft-X-ray emission spectroscopy (XES) instrument for a transmission electron microscope (TEM) presented us that a density of states (DOS) of the valence band can be obtained from a specified small specimen area. A project to improve the spectrometer to attach to a conventional analytical TEM has been conducted by using a multilayer-coated VLS grating for the high dispersion type spectrometer. Pt M-emission spectrum showed two peaks of M$$alpha$$(2050eV) and M$$beta$$(2127eV). A FWHM value of the M$$alpha$$ peak was 13 eV.

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