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A Feasibility study of neutron powder diffraction under high pressure with the Engineering Materials Diffractometer "TAKUMI" at J-PARC

Abe, Jun; Hattori, Takanori ; Komatsu, Kazuki*; Arima, Hiroshi; Arakawa, Masashi*; Okuchi, Takuo*; Kagi, Hiroyuki; Yagi, Takehiko*; Uwatoko, Yoshiya*; Matsubayashi, Kazuyuki*; Harjo, S.  ; Ito, Takayoshi; Aizawa, Kazuya ; Arai, Masatoshi; Utsumi, Wataru

We have examined the feasibility of in situ neutron powder diffraction under high pressure with the Engineering Materials Diffractometer "TAKUMI", which has been constructed at BL19 in the Materials and Life Science Facility (MLF) of J-PARC. We have tested two types of high pressure devices at TAKUMI, a Paris-Edinburgh press and a Palm cubic anvil cell. Neutron poder diffraction profiles of Pb placed in the high pressure devices as a standard material were collected. As results, diffraction peaks of Pb were clearly observed. In this study, it has been confirmed that in situ neutron powder diffraction under high pressure can be made with a combination of the high pressure devices and the TAKUMI at J-PARC.

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