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Small-angle neutron scattering study of sintered Nd-Fe-$$^{11}$$B magnets with different coercivity values

Akiya, Takahiro*; Takeda, Masayasu  ; Suzuki, Junichi; Yamaguchi, Daisuke; Kato, Hiroaki*

In spite of tremendous efforts, a role of intergranular Nd-rich phase in sintered Nd-Fe-B magnets on the coercivity ($$H_{c}$$) seems to be still unclear. The purpose of this work is to perform small-angle neutron scattering experiments on the sintered Nd-Fe-$$^{11}$$B magnets with different $$H_{c}$$ values and to investigate whether there exists any correlation between the average structure and the magnitude of $$H_{c}$$. We found that the value of characterized intensity $$I(0)$$ did not depend on the $$H_{c}$$ when $$vec{q}$$ is parallel to the $$c$$-axis of the main Nd$$_{2}$$Fe$$_{14}$$B grain. On the other hand, for the $$vec{q} perp c{rm -axis}$$ configuration, we found that log $$I(0)$$ linearly increases with increasing $$H_{c}$$, for five different samples with $$H_{c}$$ ranging from 13 to 16 kOe owing to different annealing conditions.

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