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In situ observation of reductive deposition of uranium on an electrode/electrolyte interface by optical waveguide spectroscopy

Nankawa, Takuya; Suzuki, Yoshinori; Onuki, Toshihiko

We report the first in situ and real-time observation of UV-vis absorption spectra of uranium electrodeposited on indium-tin-oxide electrodes by slab optical waveguide spectroscopy. An absorption peak around 670 nm was distinguished after a 30-min holding period at -0.2 V (vs. Ag/AgCl). X-ray absorption near edge structure spectroscopy confirmed the presence of uranium(IV) in the uranium electrodeposited on the ITO electrode.

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Category:Chemistry, Multidisciplinary

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