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Synthesis of polycrystalline LaFeAs(O,F) oxypnictide superconductor

Ishikado, Motoyuki; Shamoto, Shinichi  ; Kito, Hijiri*; Iyo, Akira*; Eisaki, Hiroshi*

We successfully synthesized pure LaFeAsO1-xFx polycrtstalline sample 0 $$leq$$ x $$leq$$ 0.2 with almost no impurity. Especially, in high Fluorine concentration region that is no well studied so far, superconductivity suppresses(Tc $$<$$ 7K). Furthermore, we measured actual Fluorine content by SIMS (Secondary Ionization Mass Spectroscopy) method, and make phase diagram for actual Fluorine content vs. Tc, and we report about the detail.

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