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Report No.
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Investigation of early oxide-layer formation using neutron reflectometer

Rivai, A. K.; Bolind, A. M.*; Saito, Shigeru   ; Yamazaki, Dai  ; Kikuchi, Kenji*

Investigation of early oxide-layer formation has been done using the neutron reflectometer, i.e., SUIREN (apparatus for Surface and Interface investigations with Reflection of Neutrons), at the nuclear reactor research JRR-3 of JAEA. The tested materials were pre-oxidized, solution-annealed, JPCA steel specimens. Two types of early oxide layers were investigated, i.e., oxidation in air at 900$$^{circ}$$C for 1 minute and oxidation in air at 450$$^{circ}$$C for 75 hours. The results showed that the neutron reflectometer was able to detect the early formation of oxide layers.

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