Proposal of healthiness confirmation procedure in electro manometer system in terms of nuclear material accountancy

Shoji, Kaoru; Mukai, Yasunobu ; Nakamura, Hironobu ; Yoshimoto, Katsunobu; Hayashi, Hiroyuki*

In general, electro manometer system for volume measurement in high concentrated Pu, U solution is used. The measurement uncertainty of volume measurement should be kept within 0.36% in the nuclear material accountancy. Not only manometer censors are calibrated periodically, but also operator should maintain the integrity of entire volume measurement system. If clogging at a tip of dip-tube is occurred, it causes measurement bias. Therefore, we studied confirmation procedure of healthiness in the system during solution storage. As result, it is confirmed that following points are effective: (1) Confirmation of consistency in the Kumar's density formula by using actual Pu, U concentration, density and acidity determined by periodical sampling and high accuracy DA. In addition, Pu, U mass is maintained within the uncertainty from the previous sampling/DA result. (2) In order to confirm the integrity of differential pressure for density that may be impacted regarding the measurement bias by clogging, comparison between measured differential pressure for density and analyzed density with high accuracy is important. In the confirmation for density, correction method between different temperatures was established by the result of evaluation of temperature effect derived by Kumar's density formula.