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中性子照射したオーステナイト系ステンレス鋼に形成する局所変形組織の評価

Evaluation of locally deformed step structure in austenitic stainless steel irradiated with neutrons

橘内 裕寿*; 笠原 茂樹; 知見 康弘; 西山 裕孝 ; 茶谷 一宏*; 越石 正人*

Kitsunai, Yuji*; Kasahara, Shigeki; Chimi, Yasuhiro; Nishiyama, Yutaka; Chatani, Kazuhiro*; Koshiishi, Masato*

中性子照射ステンレス鋼の高温水中応力腐食割れ(SCC)機構の検討に資することを目的として、照射ステンレス鋼に特有な局所変形組織形成が表面の酸化皮膜形成に及ぼす影響を検討中である。本報告では、JMTRで中性子照射した後に0.1-2%のひずみを付与したSUS316Lの表面に発現した変形組織に着目し、走査型電子顕微鏡(SEM)及び電子線後方散乱回折法(EBSD)を用いて、局所的な結晶方位の変化について観察・評価した。その結果、照射量及びひずみ付与量に応じて試験片表面にすべり線状の段状組織の形成が認められ、結晶粒界に局所的なひずみ蓄積が示唆される結果が得られた。発表では、すべり線状の組織に着目し、その発現形態・密度等と照射量・ひずみ付与量等との相関について議論する。

In order to consider mechanism on irradiation-assisted stress corrosion cracking (IASCC), oxide films on surface of locally deformed structure in irradiated stainless steel are investigated. The miniature tensile specimens are made of 316L stainless steels irradiated with neutrons in the Japan Materials Testing Reactor (JMTR). The specimens are strained up to 0.1-2%, and surface structure and crystal misorientation among grains are observed by scanning electron microscope (SEM) and electron backscattering diffraction (EBSD). As a result, visible step structure due to slip plane is appeared on the specimen surface, depending on the neutron fluence and the applied strain level. Furthermore, the data from EBSD suggests that the localization of strain occurred in the vicinity of grain boundaries. The visible step structure characterized from the viewpoints of the morphology and density, and the effects of neutron fluence and stain are discussed on the step structure are discussed.

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