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Characterization of ZrN, ZrO$$_{2}$$ and $$beta$$'-Zr$$_{7}$$O$$_{11}$$N$$_{2}$$ nanoparticles synthesized by pulsed wire discharge

パルスワイヤ放電法によるZrN, ZrO$$_{2}$$, $$beta$$'-Zr$$_{7}$$O$$_{11}$$N$$_{2}$$ナノ粒子の特性評価

Lam, Do Van*; 末松 久幸*; 小川 徹

Lam, Do Van*; Suematsu, Hisayuki*; Ogawa, Toru

ZrN, ZrO$$_{2}$$ならびに$$beta$$'-Zr$$_{7}$$O$$_{11}$$N$$_{2}$$のナノ粒子をパルスワイヤ放電法により合成した。生成物をX線回折とFE-TEMにより同定した。さらに、明視野透過観察、EELSならびに制限視野電子回折により、これらの粒子の特性を調べた。

Nanoparticles of ZrN, ZrO$$_{2}$$ and ZrN, $$beta$$'-Zr$$_{7}$$O$$_{11}$$N$$_{2}$$ were synthesized by pulsed wire discharge. Morphology and phase analyses were carried out by X-ray diffraction and field-emission transmission electron microscopy (FE-TEM). By bright field image observation, electron energy loss spectroscopy (EELS) and selected area electron diffraction (SAD) analyses, those nanoparticles were separately characterized.

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パーセンタイル:8.04

分野:Materials Science, Ceramics

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