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論文

Fingerprint of vortexlike flux closure in an isotropic Nd-Fe-B bulk magnet

Bersweiler, M.*; 大場 洋次郎; Sinaga, E. P.*; Peral, I.*; Titov, I.*; Adams, M. P.*; Rai, V.*; Metlov, K. L.*; Michels, A.*

Physical Review B, 108(9), p.094434_1 - 094434_7, 2023/09

Magnetic nanostructure in an isotropic Nd-Fe-B bulk magnet was investigated using small-angle neutron scattering. The two-dimensional scattering patterns show the so-called spike anisotropy, which points the presence of a strong magnetodipolar interaction within the sample. The field-dependence of the scattering intensity is explained by a vortex-like flux closure structure. This suggests that magnetic vortices form pairs.

論文

Effect of annealing on the magnetic microstructure of high-pressure torsion iron; The Relevance of higher-order contributions to the magnetic small-angle neutron scattering cross section

Bersweiler, M.*; 佐藤 宏和*; 足立 望*; 戸高 義一*; Peral, I.*; Kohlbrecher, J.*; Zaporozhets, V. D.*; Metlov, K. L.*; Michels, A.*; 大場 洋次郎

IUCrJ, 10(4), p.411 - 419, 2023/07

 被引用回数:1 パーセンタイル:87.7

Magnetic microstructures in severely deformed iron produced via high-pressure torsion (HPT) straining have been investigated using small-angle neutron scattering. The results reveal that nonneglibible third-order scattering contribution in the inhomogeneities amplitude of magnetization is induced via HPT straining and the contribution becomes small with subsequent annealing. The contribution has negative values, which suggest that the inhomogeneity of the magnetic anisotropy enhanced via HPT is a possible origin of the third-order contribution.

論文

Small-angle neutron scattering by spatially inhomogeneous ferromagnets with a nonzero average uniaxial anisotropy

Zaporozhets, V. D.*; 大場 洋次郎; Michels, A.*; Metlov, K. L.*

Journal of Applied Crystallography, 55(3), p.592 - 600, 2022/06

 被引用回数:7 パーセンタイル:91.48(Chemistry, Multidisciplinary)

Micromagnetic theory well explains the magnetic small-angle neutron scattering (SANS) data of bulk ferromagnets. However, only the samples having random magnetic anisotropy are mainly handled. In this study, the micromagnetic SANS theory is extended to allow to analyze uniaxial magnetic anisotropy. Micromagnetic response functions for SANS are computed analytically for several practical arrangements of anisotropy and external magnetic field orientations. This theory agrees well with the experimental SANS data of a practical soft magnet and plastically-deformed Ni and successfully provides the uniaxial anisotropy quality factors.

論文

Role of higher-order effects in spin-misalignment small-angle neutron scattering of high-pressure torsion nickel

大場 洋次郎; Bersweiler, M.*; Titov, I.*; 足立 望*; 戸高 義一*; Gilbert, E. P.*; Steinke, N.-J.*; Metlov, K. L.*; Michels, A.*

Physical Review Materials (Internet), 5(8), p.084410_1 - 084410_9, 2021/08

 被引用回数:3 パーセンタイル:22.98(Materials Science, Multidisciplinary)

We found that nanosized spin misalignments in pure nickel processed via high-pressure torsion straining persist up to the magnetic field 4 T using small-angle neutron scattering (SANS). The spin-misalignment scattering patterns are elongated perpendicular to the applied magnetic field and different from the conventional micromagnetic SANS theory based on the second order contribution in spin misalignment amplitude. This means that the high-pressure torsion straining makes higher-order effects in the micromagnetic SANS cross sections observable. This results will fuel the further development of the micromagnetic SANS theory.

論文

Revealing defect-induced spin disorder in nanocrystalline Ni

Bersweiler, M.*; Sinaga, E. P.*; Peral, I.*; 足立 望*; Bender, P.*; Steinke, N.-J.*; Gilbert, E. P.*; 戸高 義一*; Michels, A.*; 大場 洋次郎

Physical Review Materials (Internet), 5(4), p.044409_1 - 044409_7, 2021/04

 被引用回数:7 パーセンタイル:49.88(Materials Science, Multidisciplinary)

Using small-angle neutron scattering (SANS), we found that the high-density of crystal defects induced via high-pressure torsion (HPT) straining cause a significant spin-misalignment scattering in pure Ni. The analysis of the correlation length of the spin misalignments provided that the spin misalignments surround the defect with the size of 11 nm in HPT-strained nickel.

論文

Heat suppresses activation of an auxin-responsive promoter in cultured guard cell protoplasts of tree tobacco

Dong, M. A.*; Bufford, J. L.*; 大野 豊; Church, K.*; Dau, M. Q.*; Michels, K.*; Haughton, M.*; Tallman, G.*

Plant Physiology, 145(2), p.367 - 377, 2007/10

 被引用回数:3 パーセンタイル:9.41(Plant Sciences)

タバコ培養孔辺細胞プロトプラスト(GCP)は、高温耐性や高温障害の細胞情報伝達機構の研究のための新規システムを構成する。GCPは、オーキシン及びサイトカイニンを含む培地で32$$^{circ}$$Cで培養すると細胞壁を再構築し分裂を開始する。一方38$$^{circ}$$Cでは、GCPは高温耐性を獲得し、細胞壁の構築は行われず、細胞周期が開始されない。この現象がオーキシン制御遺伝子の発現抑制によるものではないかと考え、オーキシン応答性プロモーター制御下にGFPをつなげた遺伝子をGCPに導入し解析した。その結果、高温処理は、オーキシンによる遺伝子発現の活性化を抑制することが明らかとなった。高温ストレスに曝された細胞は、活性酸素種を蓄積することが知られているが、H$$_{2}$$O$$_{2}$$は32$$^{circ}$$CでオーキシンによるGFPの発現活性を抑制しなかった。またスーパーオキシドやH$$_{2}$$O$$_{2}$$スカベンジャーは38$$^{circ}$$CにおけるGFPの発現抑制を解除しなかった。

口頭

Revealing defect-induced spin disorder in nanocrystalline Ni

Bersweiler, M.*; Sinaga, E. P.*; Peral, I.*; 足立 望*; Bender, P.*; Steinke, N.-J.*; Gilbert, E. P.*; 戸高 義一*; 大場 洋次郎; Michels, A.*

no journal, , 

Magnetic properties of nanocrystalline nickel prepared via high-pressure torsion straining was investigated using magnetometry and magnetic small-angle neutron scattering to study the influence of the microstructure on magnetism. The magnetometry shows a significant increase of the coercivity compared to nondeformed polycrystalline nickel. The neutron data detect a nanoscale spin misalignment caused by the high density of crystal defects created by severe plastic deformation during the sample preparation. These results indicate that magnetic anisotropy is enhanced around the crystal defects.

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