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論文

Reverse austenite transformation behavior in a tempered martensite low-alloy steel studied using ${it in situ}$ neutron diffraction

友田 陽*; Gong, W.*; Harjo, S.; 篠崎 智也*

Scripta Materialia, 133, p.79 - 82, 2017/05

AA2017-0349.pdf:2.43MB

https://doi.org/10.1016/j.scriptamat.2017.02.017
 被引用回数：24 パーセンタイル：74.12(Nanoscience & Nanotechnology)

The microstructure evolution during reverse transformation of a Cr-Ni-Mo steel consisting of tempered lath martensite and Cr carbide was examined using ${it in situ}$ neutron diffraction at high temperatures. The microstructural change from a reversed coarse-grained structure to a fine-grained polygonal structure by further annealing was monitored through a decrease in the diffraction intensity caused by primary extinction and the full width at half maximum. This result is different from that for a bainite steel, showing good coincidence with the observations using electron back scatter diffraction.

論文

Encapsulating mobile proton carriers into structural defects in coordination polymer crystals; High anhydrous proton conduction and fuel cell application

犬飼 宗弘*; 堀毛 悟史*; 板倉 智也*; 篠崎 良太*; 荻原 直希*; 梅山 大樹*; Nagarker, S.*; 西山 裕介*; Malon, M.*; 林 灯*; et al.

Journal of the American Chemical Society, 138(27), p.8505 - 8511, 2016/07

https://doi.org/10.1021/jacs.6b03625
 被引用回数：135 パーセンタイル：95.46(Chemistry, Multidisciplinary)

We describe encapsulation of mobile proton carriers into defect sites in non-porous coordination polymers. The proton carriers are encapasulated with high mobility and provide high proton conductivity at 150$$^{circ}$$C under anhydrous condition. The high proton conductivity and non-porous nature allow power generation by fuel cell in which CPs are used as electrolyte. To observe defects and mobile proton carriers, we carried out solid-state NMR, XAFS, XRD, and ICP-AES/EA. On the basis of these analyses, we elucidated that the defect sites provide space for mobile uncoordinated H$$_{3}$$PO$$_{4}$$, H$$_{2}$$PO$$_{4}$$$$^{-}$$, and H$$_{2}$$O. These mobile carriers play a key role to expand proton hopping path and promote the mobility of all protons in coordination frameworks, leading to high proton conductivity and fuel cell power generation.

口頭

Q&Pプロセスにおける相変態と炭素分配に及ぼすオーフォミングの影響

Gong, W.*; Harjo, S.; 柴田 曉伸*; 友田 陽*; 篠崎 智也*; 辻 伸泰*

no journal, , 

Quenching and partitioning (Q&P) process is an effective approach to control the amount and stability of retained austenite. Our previous study confirmed that carbon partitioning and isothermal transformation simultaneously occurred below martensitic transformation starting (Ms) temperature. In order to deepen the understanding on controlling microstructures through Q&P processes, the effect of ausforming on phase transformation and carbon partitioning during the Q&P process were investigated by the use of in-situ neutron diffraction in the present study.

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