Micro-PIXE analysis on adsorbent of extraction chromatography for MA(III) recovery

Takahatake, Yoko; Watanabe, So; Kofuji, Hirohide; Takeuchi, Masayuki; Nomura, Kazunori; Sato, Takahiro*

International Journal of PIXE, 26(3&4), p.73 - 83, 2017/09

BB2016-1248.pdf:0.36MB

https://doi.org/10.1142/S0129083517500012

JAEA has been conducting research and development of MA(III) recovery from HLLW by extraction chromatography technology for reduction in amount and environmental impact of radioactive waste. The behavior of adsorbed cations inside the adsorbent packed in a column is necessary to be evaluated for improvement of the adsorbent or flow-sheet to achieve targeted MA(III) recovery performance. In this paper, micro-PIXE analysis was carried out on the particles sampled from various positions of the column to reveal the behavior of cations inside the packed column with CMPO/SiO -P adsorbent. Simple experiment and data analysis were shown to be effective to reveal inside of the column, and formation and transportation of the adsorption bands were observed for some cations which are extractable by the CMPO extractant. Some part of Zr(IV) and Mo(VI) were found to remain inside the column without distinct transportation even after the elution operation.

Distribution of elements in the phases produced by reaction between CaO-stabilized zirconia and simulated high-level radioactive waste

; ; Akabori, Mitsuo

Journal of Nuclear Science and Technology, 23(5), p.469 - 471, 1986/00

https://doi.org/10.3327/jnst.23.469

no abstracts in English

A Laser-acoustic technique for simultaneous measurement of elemental and surface imaging of fuel debris

Batsaikhan, M.; Oba, Hironori; Wakaida, Ikuo

no journal, , 

Fiber-coupled acoustic wave-assisted microchip LIBS system for elemental composition and surface imaging of nuclear fuel debris

Batsaikhan, M.; Oba, Hironori; Karino, Takahiro; Akaoka, Katsuaki; Wakaida, Ikuo

no journal, ,