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論文

Quantifying the dislocation structures of additively manufactured Ti-6Al-4V alloys using X-ray diffraction line profile analysis

山中 謙太*; 黒田 あす美*; 伊藤 美優*; 森 真奈美*; Bian, H.*; 菖蒲 敬久; 佐藤 茂男*; 千葉 明彦*

Additive Manufacturing, 37, p.101678_1 - 101678_12, 2021/01

 被引用回数:24 パーセンタイル:86.75(Engineering, Manufacturing)

Ti-6Al-4V alloy is widely used in aerospace and biomedical industries, and its preparation using additive manufacturing techniques has recently attracted considerable attention. Herein, the dislocation structures developed during electron beam and laser beam powder-bed fusion (EB-PBF and LB-PBF, respectively) of the Ti-6Al-4V alloy were quantitatively examined via XRD line profile analysis. Accordingly, a higher dislocation density and finer crystallite size were observed at the top cross-section from the XRD line profile analysis, suggesting that the extent of phase decomposition depended on the duration of the exposure to the elevated temperature. Nonetheless, the saturated dislocation density was as high as 10$$^{14}$$ m$$^{-2}$$, where dislocation strengthening affected the overall strength of the EB-PBF specimen. Diffraction peaks of sufficient intensity that enabled the analysis of the dislocation structures in both the $$alpha$$ ($$alpha$$')-matrix and the nanosized beta-phase precipitates at the $$alpha$$ ($$alpha$$')-laths were obtained under high-energy synchrotron radiation; this revealed that the beta-phase had a much higher dislocation density than the surrounding $$alpha$$ ($$alpha$$')-matrix. The enhanced dislocation accumulation in the nanosized $$beta$$-phase precipitates probably reflects the elemental partitioning that occurred during post-solidification cooling. The valuable insights provided in this study are expected to promote further development of alloy preparation using additive manufacturing processes.

論文

Tuning strain-induced $$gamma$$-to-$$varepsilon$$ martensitic transformation of biomedical Co-Cr-Mo alloys by introducing parent phase lattice defects

森 真奈美*; 山中 謙太*; 佐藤 茂男*; 椿 真貴*; 佐藤 こずえ*; 熊谷 正芳*; 今福 宗行*; 菖蒲 敬久; 千葉 明彦*

Journal of the Mechanical Behavior of Biomedical Materials, 90, p.523 - 529, 2019/02

 被引用回数:19 パーセンタイル:70.43(Engineering, Biomedical)

In this study, we examined the effect of pre-existing dislocation structures in a face-centered cubic gamma-phase on strain-induced martensitic transformation (SIMT) to produce a hexagonal close-packed epsilon-phase in a hot-rolled biomedical Co-Cr-Mo alloy. The as-rolled microstructure was characterized by numerous dislocations as well as stacking faults and deformation twins. SIMT occurred just after macroscopic yielding in tensile deformation. Using synchrotron X-ray diffraction line-profile analysis, we successfully captured the nucleation of epsilon-martensite during tensile deformation in terms of structural evolution in the surrounding gamma-matrix: many dislocations that were introduced into the gamma-matrix during the hot-rolling process were consumed to produce epsilon-martensite, together with strong interactions between dislocations in the gamma-matrix. As a result, the SIMT behavior during tensile deformation was accelerated through the consumption of these lattice defects, and the nucleation sites for the SIMT epsilon-phase transformed into intergranular regions upon hot rolling. Consequently, the hot-rolled Co-Cr-Mo alloy simultaneously exhibited an enhanced strain hardening and a high yield strength. The results of this study suggest the possibility of a novel approach for controlling the $$gamma$$ to $$varepsilon$$ SIMT behavior, and ultimately, the performance of the alloy in service by manipulating the initial dislocation structures.

論文

Diagnostics system of JT-60U

杉江 達夫; 波多江 仰紀; 小出 芳彦; 藤田 隆明; 草間 義紀; 西谷 健夫; 諫山 明彦; 佐藤 正泰; 篠原 孝司; 朝倉 伸幸; et al.

Fusion Science and Technology (JT-60 Special Issue), 42(2-3), p.482 - 511, 2002/09

 被引用回数:6 パーセンタイル:3.03(Nuclear Science & Technology)

JT-60Uの計測診断システムは、約50の計測装置から構成されている。近年、プラズマパラメータの半径方向の分布計測が精度よく行なわれるようになった結果、プラズマの内部構造が明らかになった。また、ミリ波反射計/電子サイクロトロン放射計測により、電子密度/電子温度揺動の測定が行なわれ、プラズマ閉じ込めに関する理解が進展した。さらに、電子温度,中性子発生率,放射パワー,電子温度勾配等の実時間制御実験が、関係する計測装置のデータを利用して行なわれた。これらの計測,及び実時間制御を駆使することにより、高性能プラズマを実現することができた。次期核融合実験炉用計測装置としては、炭酸ガスレーザ干渉計/偏光計,及び協同トムソン散乱計測装置を開発している。

口頭

JT-60SAのプラズマ計測装置開発

久保 博孝; 伊丹 潔; 千葉 真一; 福本 正勝; 濱野 隆; 波多江 仰紀; 諫山 明彦; 今澤 良太; 神谷 健作; 河野 康則; et al.

no journal, , 

JT-60SAでは、プラズマ計測は、トカマク装置の運転及び安全に加え、プラズマの評価、物理研究、実時間制御に欠くことができない。JT-60SAの計測装置にはできる限りJT-60Uで使用されていた計測装置の構成部品を再利用するが、長パルス高加熱を伴う新たな超伝導トカマク装置に適応するために、また新たな研究の必要性を満たすために、開発が必要である。特に、対物光学系などプラズマ近傍の構成部品の多くは再設計しなければならない。ここでは、JT-60SAのプラズマ計測装置の開発状況について発表する。

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