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Abe, Kazuhide
JAEA-Review 2024-065, 26 Pages, 2025/03
The Japan Atomic Energy Agency's research reactor, JRR-3, resumed operations on February 26, 2021, after nearly a decade. As a shared-use facility, JRR-3 is operated to accommodate external users as well. The procedures, from research proposal submissions to final report submissions, are conducted through the online system JRR-3 RING (Research Information NaviGator) (https://jrr3ring.jaea.go.jp/). RING enables integrated management of proposal submissions, schedule adjustments, data sharing, and report submissions, and it has been upgraded in preparation for the resumption of JRR-3 operations. RING is specifically designed to enhance the convenience of beamline users, featuring simplified application processes, improved flexibility in schedule coordination, and enhanced data management capabilities. With the implementation of this system, users can conduct their research more efficiently and securely. Moving forward, JRR-3 aims to expand its role as a platform for neutron research, accessible to a diverse range of researchers both domestically and internationally. The resumption of operations and the expansion of RING mark a significant step toward revitalizing neutron research and fostering collaboration with industries and academia.
Kamiya, Junichiro; Abe, Kazuhide; Fujimori, Shinichi; Fukuda, Tatsuo; Kobata, Masaaki; Morohashi, Yuko; Tsuda, Yasutaka; Yamada, Ippei; Yoshigoe, Akitaka
e-Journal of Surface Science and Nanotechnology (Internet), 22(4), p.316 - 326, 2024/08
The activation and deterioration mechanisms of the Ti-Zr-V non-evaporable getter (NEG) coating have been investigated. Operando analysis of the surface chemical composition change of the Ti-Zr-V coating was performed by the synchrotron radiation photoelectron spectroscopy (SRPES) during the process of raising the sample temperature to 250C, corresponding to the activation process of NEG coating. The surface oxidation process was also characterized by the SRPES during the injection of O_2 gas into the chamber while keeping the sample temperature at 250
C, corresponding to the deterioration process of NEG coating, i.e. surface oxidation and oxygen diffusion to the coating interior. The depth profile of the oxidized sample was measured with X-ray photoelectron spectroscopy. The results shows, in the activation process, the surface Zr gets the oxygen from the oxides of Ti and V at the first stage, resulting in the metallic Ti and V on the surface, and the oxygen of the Zr-oxide and/or Zr sub-oxides diffuse to the interior of the coating in the continuous temperature rise, resulting in the metallic Zr on the surface. It is further suggested that the deterioration of the Ti-Zr-V NEG coating means the Zr and secondary Ti are oxidized deep into the coating, resulting in the restriction of the oxygen migration from the NEG compositions on the surface and consequently the lack of surface metallization.
Tamura, Itaru; Kodama, Katsuaki; Igawa, Naoki; Abe, Kazuhide; Matsue, Hideaki
no journal, ,
no abstracts in English
Kobata, Masaaki; Fukuda, Tatsuo; Tanida, Hajime; Kamiya, Junichiro; Morohashi, Yuko; Yamada, Ippei; Abe, Kazuhide
no journal, ,
The mechanism of how the substrate titanium contributes to the advanced getter performance has not been elucidated. In this study, NEG/Ti interface analysis was performed using HAXPES at BL22XU to clarify the effect of Ti substrate on NEG performance.
Kobata, Masaaki; Morohashi, Yuko; Abe, Kazuhide; Yamada, Ippei; Fukuda, Tatsuo; Koarai, Kazuma; Tanida, Hajime; Kamiya, Junichiro
no journal, ,
This study aimed to improve non-evaporable getter (NEG) coating technology on titanium substrates, focusing on lowering activation temperatures and enhancing repeatability. Using Hard X-ray Photoelectron Spectroscopy (HAXPES) and Secondary Ion Mass Spectrometry (SIMS), we analyzed NEG activation and degradation mechanisms. The effects of titanium, stainless steel (SUS316), and beryllium copper (BeCu) substrates on NEG properties were compared. Results suggested that the BeCu substrate had the lowest activation temperature, indicating its potential advantage for low-temperature NEG activation.
Morohashi, Yuko; Kamiya, Junichiro; Abe, Kazuhide; Kobata, Masaaki; Tsuda, Yasutaka
no journal, ,
no abstracts in English
Kamiya, Junichiro; Abe, Kazuhide; Kobata, Masaaki; Tsuda, Yasutaka; Fukuda, Tatsuo; Fujimori, Shinichi; Morohashi, Yuko; Yamada, Ippei; Yoshigoe, Akitaka
no journal, ,
Sequence measurements with XPS have been performed to understand more detail about the activation and deterioration mechanism. The sample of a titanium plate with Ti-Zr-V coating of 1 um thickness was prepared. The sample was set in the surface science station in the BL23SU of SPring-8. At first, the XPS measurements for the sample surface were performed during the sample temperature was raised to 250C. After that, the XPS was subsequently performed during the injection of oxygen gas into the chamber while keeping the sample temperature at 250
C, which corresponds to the accelerated deterioration test. After that, the depth profile of the sample was measured with another XPS apparatus with an X-ray tube by argon etching. The result showed that the surface Zr gets the oxygen from Ti oxide and V oxide at the first stage of the activation and the oxygen of the Zr oxide would diffuse to the bulk in the continuous temperature rise. It was revealed that the concentrated oxygen in the coating exists in the forms of mainly Zr oxide and Ti oxide in the second place.
Matsue, Hideaki; Osakabe, Toyotaka; Abe, Kazuhide
no journal, ,
no abstracts in English
Wada, Kaoru*; Shiga, Takashi; Okahashi, Kazunari*; Kamiya, Junichiro; Kobata, Masaaki; Morohashi, Yuko; Abe, Kazuhide; Kishikawa, Shinsuke*; Sasaki, Masanao*; Kuroiwa, Masahide*; et al.
no journal, ,
Tokyo Electronics Co., Ltd. manufactures and sells ultra-high vacuum equipment using BeCu material. By integrating this with the NEG coating technology from the Japan Atomic Energy Agency, the company has developed a getter-type BeCu vacuum chamber that can operate without electricity. In a series of experiments, the chamber was opened to the atmosphere, evacuated, and then subjected to a baking (activation) process at 200 for 8.5 hours, repeated five times. The results showed that the NEG coating significantly improved the pumping speed and reduced the ultimate pressure. Additionally, during buildup pressure measurements, this process was repeated five times. While there was no substantial difference in pressure before the tests, a noticeable improvement in pressure was observed with the NEG coating as the tests progressed. This demonstrates that the NEG coating not only enhances the efficiency of the vacuum system but also plays a crucial role in maintaining an ultra-high vacuum environment.
Tamura, Itaru; Kodama, Katsuaki; Igawa, Naoki; Abe, Kazuhide; Matsue, Hideaki
no journal, ,
no abstracts in English