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Journal Articles

R&D status in thermochemical water-splitting hydrogen production iodine-sulfur process at JAEA

Noguchi, Hiroki; Takegami, Hiroaki; Kasahara, Seiji; Tanaka, Nobuyuki; Kamiji, Yu; Iwatsuki, Jin; Aita, Hideki; Kubo, Shinji

Energy Procedia, 131, p.113 - 118, 2017/12

 Times Cited Count:9 Percentile:0.22

The IS process is the most deeply investigated thermochemical water-splitting hydrogen production cycle. It is in a process engineering stage in JAEA to use industrial materials for components. Important engineering tasks are verification of integrity of the total process and stability of hydrogen production in harsh environment. A test facility using corrosion-resistant materials was constructed. The hydrogen production ability was 100 L/h. Operation tests of each section were conducted to confirm basic functions of reactors and separators, etc. Then, a trial operation for integration of the sections was successfully conducted to produce hydrogen of about 10 L/h for 8 hours.

Journal Articles

IS process hydrogen production test for components and system made of industrial structural material, 1; Bunsen and HI concentration section

Tanaka, Nobuyuki; Takegami, Hiroaki; Noguchi, Hiroki; Kamiji, Yu; Iwatsuki, Jin; Aita, Hideki; Kasahara, Seiji; Kubo, Shinji

Proceedings of 8th International Topical Meeting on High Temperature Reactor Technology (HTR 2016) (CD-ROM), p.1022 - 1028, 2016/11

Japan Atomic Energy Agency (JAEA) has manufactured 100 NL/h-H$$_2$$-scale hydrogen test apparatus. In advance to conduct the continuous operation, we investigated performance of the components in each section of the IS process. In this paper, the results of test of Bunsen and HI concentration sections was shown. In Bunsen reaction, section, we confirmed that outlet gas flow rate included no SO$$_{2}$$ gas, indicating that all the feed SO$$_{2}$$ gas was absorbed to the solution in the Bunsen reactor for the Bunsen reaction. On the basis of these results, we evaluated that Bunsen reactor was workable. In HI concentration section, HI concentration was conducted by EED stack. As a result, it can concentrate HI in HIx solution as theoretically predicted on the basis of the previous paper. Based on the results added to that shown in Series II, we have conducted a trial continuous operation and succeeded it for 8 hours.

JAEA Reports

HTTR hydrogen production system structure and main specifications of mock-up test facility (Contract research)

Kato, Michio; Hayashi, Koji; Aita, Hideki; Ohashi, Hirofumi; Sato, Hiroyuki; Inaba, Yoshitomo; Iwatsuki, Jin; Takada, Shoji; Inagaki, Yoshiyuki

JAEA-Technology 2007-022, 209 Pages, 2007/03

JAEA-Technology-2007-022.pdf:14.46MB

The mock-up test facility was fabricated to investigate performance of the steam generator for mitigation of the temperature fluctuation of helium gas and transient behavior of the hydrogen production system for HTTR and to obtain experimental data for verification of a dynamic analysis code. The test facility has an approximate hydrogen production capacity of 120Nm$$^{3}$$/h and the steam reforming process of methane; CH$$_{4}$$+H$$_{2}$$O=3H$$_{2}$$+CO, was used for hydrogen production of the test facility. An electric heater was used as a heat source instead of the reactor in order to heat helium gas up to 880 $$^{circ}$$C (4MPa) at the chemical reactor inlet which is the same temperature as the HTTR hydrogen production system. Fabrication of the test facility was completed in February in 2002, and seven cycle operations were carried out from March in 2002 to December in 2004. This report describes the structure and main specifications of the test facility.

JAEA Reports

Annual report on experimental operations and maintenances of mock-up model test facility with a full-scale reaction tube for HTTR hydrogen production system in 2004 fiscal year (Contract research)

Hayashi, Koji; Ohashi, Hirofumi; Morisaki, Norihiro; Kato, Michio; Aita, Hideki; Takeda, Tetsuaki; Nishihara, Tetsuo; Inaba, Yoshitomo; Takada, Shoji; Inagaki, Yoshiyuki

JAEA-Technology 2006-013, 73 Pages, 2006/03

JAEA-Technology-2006-013.pdf:6.27MB

This is annual report on the experimental test operations and maintenances of the mock-up test facility with a full-scale reaction tube for the HTTR hydrogen production system in 2004 fiscal year. The improvement work of catalyst dust filter in combustion system was performed in May 2004, and the performance was confirmed. The sixth experimental test operation was performed from June to July 2004. Periodic inspections on boiler equipment and high-pressure gas production facilities were performed from end of July to September 2004. The seventh experimental test operation was performed from October to December 2004 for chemical reaction shutdown test. From the results, a behavior of the helium-gas cooling system, consists of steam generator and radiator, during chemical reaction shutdown was confirmed. This report is summarized with the outline and the results of the test, maintenance works and inspections, and operation records in mentioned above.

JAEA Reports

Annual report on experimental operations and maintenances of mock-up model test facility with a full-scale reaction tube for HTTR hydrogen production system in 2003 fiscal year (Contract research)

Hayashi, Koji; Morisaki, Norihiro; Ohashi, Hirofumi; Kato, Michio; Aita, Hideki; Takeda, Tetsuaki; Nishihara, Tetsuo; Inaba, Yoshitomo; Takada, Shoji; Inagaki, Yoshiyuki

JAEA-Technology 2006-012, 98 Pages, 2006/03

JAEA-Technology-2006-012.pdf:7.83MB

This is a report on the experimental operations and maintenances of the mock-up test facility with a full-scale reaction tube for the HTTR hydrogen production system in 2003 fiscal year. The fourth and fifth experimental test operations were performed, from May to July and from October to December in 2003, for the following tests; (a)start-up and shutdown operation test, (b)process change test, (c)continuous hydrogen-production test and (d)chemical reaction shutdown test. From the results, a long time-range stability of the hydrogen production system was confirmed, a behavior of the helium-gas cooling system, consists of steam generator and radiator, during chemical reaction shutdown, was understanded, and so on. Periodic inspections on boiler equipment and high-pressure gas production facilities were performed from end of July 2003. This report is summarized on outlines and results of the tests, outlines and results of the periodic inspections, and operation records of the mock-up test facility.

JAEA Reports

Annual report on experimental operations and maintenances of mock-up model test facility with a full-scale reaction tube for HTTR hydrogen production system in 2002 fiscal year (Contract research)

Hayashi, Koji; Ohashi, Hirofumi; Inaba, Yoshitomo; Kato, Michio; Aita, Hideki; Morisaki, Norihiro; Takeda, Tetsuaki; Nishihara, Tetsuo; Takada, Shoji; Inagaki, Yoshiyuki

JAEA-Technology 2006-011, 132 Pages, 2006/03

JAEA-Technology-2006-011.pdf:9.47MB

This report describes 2002 fiscal-year experimental test operations of the mock-up test facility with a full-scale reaction tube for the HTTR hydrogen production system. The improvement works were performed in May 2002. The second experimental test operation was performed from June 2002 and the performances of the improved parts were confirmed. Periodic inspections on boiler equipment and high-pressure gas production facilities were performed from end of July 2002. The third experimental test operation was performed, from October 2002, for (a)start-up and shutdown test, (b)process change test, (c)chemical reaction shutdown test and (d)characteristics test on steam reformer. It was confirmed that the changes of helium gas temperature, caused at steam reformer, could be mitigated into the target range by the steam generator. Maintenance works of high-pressure gas production facilities were also performed in February 2003. This report is summarized with the outline and the results of the test, maintenance works and inspections, and operation records in mentioned above.

JAEA Reports

Annual report on experimental operation of mock-up model test facility with a full-scale reaction tube for HTTR hydrogen production system in 2001 fiscal year (Contract research)

Hayashi, Koji; Inagaki, Yoshiyuki; Kato, Michio; Fujisaki, Katsuo*; Aita, Hideki; Takeda, Tetsuaki; Nishihara, Tetsuo; Inaba, Yoshitomo; Ohashi, Hirofumi; Katanishi, Shoji; et al.

JAERI-Tech 2005-032, 46 Pages, 2005/06

JAERI-Tech-2005-032.pdf:4.79MB

This is annual report on the experimental operation of the mock-up test facility with a full-scale reaction tube for the HTTR hydrogen production system in 2001 fiscal year. The first experimental operation was performed during two weeks from March 1, 2002 to March 13, 2002 to test on the thermal hydraulic performance of the steam reformer and also to train the operators. The thermal hydraulic performance test of the steam reformer was performed to evaluate the heat transfer characteristics between helium gas and process gas in the steam reformer. This report is summarized with an overview of the test, the results and its operation records.

JAEA Reports

Heat transfer characteristics evaluation of heat exchangers of mock-up test facility with full-scale reaction tube for HTTR hydrogen production system (Contract research)

Shimizu, Akira; Ohashi, Hirofumi; Kato, Michio; Hayashi, Koji; Aita, Hideki; Nishihara, Tetsuo; Inaba, Yoshitomo; Takada, Shoji; Morisaki, Norihiro; Sakaki, Akihiro*; et al.

JAERI-Tech 2005-031, 174 Pages, 2005/06

JAERI-Tech-2005-031.pdf:20.71MB

Connection of hydrogen production system by steam reforming of methane to the High Temperature Engineering Test Reactor (HTTR) of the Japan Atomic Energy Research Institute (JAERI) has been surveyed until now. Mock-up test facility of this steam reforming system with full-scale reaction tube was constructed in FY 2001, and a lot of operational test data on heat exchanges were obtained in these tests.In this report specifications, structures and heat transfer formulae of steam reformer, steam superheater, steam generator, condenser, helium gas cooler, feed gas heater and feed gas superheater were described. Evaluation codes were newly made to evaluate heat transfer characteristics from measured test data. Overall heat-transfer coefficient obtained from the experimental data were compared and evaluated with the prospective value calculated with heat transfer formulae. As a result, heat transfer performance and thermal efficiency of these heat exchangers were confirmed to be appropriate.

JAEA Reports

Improvement works report on mock-up model test facility with a full-scale reaction tube for HTTR hydrogen production system (Contract research)

Sakaki, Akihiro*; Kato, Michio; Hayashi, Koji; Fujisaki, Katsuo*; Aita, Hideki; Ohashi, Hirofumi; Takada, Shoji; Shimizu, Akira; Morisaki, Norihiro; Maeda, Yukimasa; et al.

JAERI-Tech 2005-023, 72 Pages, 2005/04

JAERI-Tech-2005-023.pdf:14.86MB

In order to establish the system integration technology to connect a hydrogen production system to a high temperature gas cooled reactor, the mock-up test facility with a full-scale reaction tube for the steam reforming HTTR hydrogen production system was constructed in fiscal year 2001 and its functional test operation was performed in the year. Seven experimental test operations were performed from fiscal year 2001 to 2004. On a period of each test operation, there happened some troubles. For each trouble, the cause was investigated and the countermeasures and the improvement works were performed to succeed the experiments. The tests were successfully achieved according to plan.This report describes the improvement works on the test facility performed from fiscal year 2001 to 2004.

JAEA Reports

Performance test results of mock-up model test facility with a full-scale reaction tube for HTTR hydrogen production system (Contract research)

Inagaki, Yoshiyuki; Hayashi, Koji; Kato, Michio; Fujisaki, Katsuo; Aita, Hideki; Takeda, Tetsuaki; Nishihara, Tetsuo; Inaba, Yoshitomo; Ohashi, Hirofumi; Katanishi, Shoji; et al.

JAERI-Tech 2003-034, 129 Pages, 2003/05

JAERI-Tech-2003-034.pdf:7.62MB

no abstracts in English

JAEA Reports

Performance test results of helium gas circulator of mock-up test facility with full-scale reaction tube for HTTR hydrogen production system (Contract research)

Shimizu, Akira; Kato, Michio; Hayashi, Koji; Fujisaki, Katsuo; Aita, Hideki; Takeda, Tetsuaki; Nishihara, Tetsuo; Katanishi, Shoji; Takada, Shoji; Inaba, Yoshitomo; et al.

JAERI-Tech 2003-033, 105 Pages, 2003/03

JAERI-Tech-2003-033.pdf:8.35MB

no abstracts in English

Oral presentation

Completion of decommissioning project of RI using facility

Takai, Toshihide; Shimakawa, Satoshi; Terunuma, Takashi; Aita, Hideki; Midorikawa, Hiroshi

no journal, , 

Decommissioning project of RI using facility was started on 2011 and finished on 2013. The Great East Japan Earthquake was occurred during this period, and a lot of radioactive materials were released to an atmosphere of the wide area because of Fukushima Nuclear Accident. Considering the effect of fallout derived from foregoing accident was required to complete this project.

Oral presentation

Research and development for HTGR heat application technology, 5; IS process hydrogen production test for total components and system; Preset status of the test

Iwatsuki, Jin; Takegami, Hiroaki; Noguchi, Hiroki; Tanaka, Nobuyuki; Kamiji, Yu; Aita, Hideki; Terada, Atsuhiko; Kubo, Shinji

no journal, , 

Japan Atomic Energy Agency is advancing the research and development of the IS process hydrogen production method as one of the heat utilization technology that the heat source the high temperature gas-cooled reactor with inherent safety diverse industrial use is expected. Currently, produced a continuous hydrogen production test equipment made industrial materials, we have been the instrument function confirmation towards the verification of reliability validation and continuous hydrogen production performance of the plant the entire system. In this paper, we report on the current status of this continuous hydrogen production test.

Oral presentation

Research and development for HTGR heat application technology, 4; IS process hydrogen production test for total components and system; Outline of test facility

Takegami, Hiroaki; Noguchi, Hiroki; Tanaka, Nobuyuki; Iwatsuki, Jin; Kamiji, Yu; Kasahara, Seiji; Aita, Hideki; Terada, Atsuhiko; Kubo, Shinji

no journal, , 

Japan Atomic Energy Agency (JAEA) has studied iodine-sulfur (IS) process, a thermochemical cycle to produce hydrogen by water splitting. This process is a candidate application of high temperature heat from high temperature gas-cooled reactors. An experimental apparatus of the total IS process has just been constructed to verify integrity of process components of industrial materials. In this report, an outline of the test facility is explained.

Oral presentation

Research and development for HTGR heat application technology, 3; Integrity test of IS process components; HI decomposer

Kamiji, Yu; Aita, Hideki; Noguchi, Hiroki; Iwatsuki, Jin; Onuki, Kaoru; Kubo, Shinji

no journal, , 

JAEA has been carring out the integrity test of IS process components in order to confirm its reliability for high temperature corrosive environment. We have conducted the HI decomposition test using HI decomposer made of Nickel-based alloy (Hastelloy C-276) 100 hours testing time. As a result, it was confirmed that Hydrogen was generated at the equilibrium conversion rate. In addition, black deliquescent corrosion product was observed on the corrosion specimen.

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