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論文

Quantifying the dislocation structures of additively manufactured Ti-6Al-4V alloys using X-ray diffraction line profile analysis

山中 謙太*; 黒田 あす美*; 伊藤 美優*; 森 真奈美*; Bian, H.*; 菖蒲 敬久; 佐藤 茂男*; 千葉 明彦*

Additive Manufacturing, 37, p.101678_1 - 101678_12, 2021/01

 被引用回数:23 パーセンタイル:86.72(Engineering, Manufacturing)

Ti-6Al-4V alloy is widely used in aerospace and biomedical industries, and its preparation using additive manufacturing techniques has recently attracted considerable attention. Herein, the dislocation structures developed during electron beam and laser beam powder-bed fusion (EB-PBF and LB-PBF, respectively) of the Ti-6Al-4V alloy were quantitatively examined via XRD line profile analysis. Accordingly, a higher dislocation density and finer crystallite size were observed at the top cross-section from the XRD line profile analysis, suggesting that the extent of phase decomposition depended on the duration of the exposure to the elevated temperature. Nonetheless, the saturated dislocation density was as high as 10$$^{14}$$ m$$^{-2}$$, where dislocation strengthening affected the overall strength of the EB-PBF specimen. Diffraction peaks of sufficient intensity that enabled the analysis of the dislocation structures in both the $$alpha$$ ($$alpha$$')-matrix and the nanosized beta-phase precipitates at the $$alpha$$ ($$alpha$$')-laths were obtained under high-energy synchrotron radiation; this revealed that the beta-phase had a much higher dislocation density than the surrounding $$alpha$$ ($$alpha$$')-matrix. The enhanced dislocation accumulation in the nanosized $$beta$$-phase precipitates probably reflects the elemental partitioning that occurred during post-solidification cooling. The valuable insights provided in this study are expected to promote further development of alloy preparation using additive manufacturing processes.

論文

Tuning strain-induced $$gamma$$-to-$$varepsilon$$ martensitic transformation of biomedical Co-Cr-Mo alloys by introducing parent phase lattice defects

森 真奈美*; 山中 謙太*; 佐藤 茂男*; 椿 真貴*; 佐藤 こずえ*; 熊谷 正芳*; 今福 宗行*; 菖蒲 敬久; 千葉 明彦*

Journal of the Mechanical Behavior of Biomedical Materials, 90, p.523 - 529, 2019/02

 被引用回数:19 パーセンタイル:71.16(Engineering, Biomedical)

In this study, we examined the effect of pre-existing dislocation structures in a face-centered cubic gamma-phase on strain-induced martensitic transformation (SIMT) to produce a hexagonal close-packed epsilon-phase in a hot-rolled biomedical Co-Cr-Mo alloy. The as-rolled microstructure was characterized by numerous dislocations as well as stacking faults and deformation twins. SIMT occurred just after macroscopic yielding in tensile deformation. Using synchrotron X-ray diffraction line-profile analysis, we successfully captured the nucleation of epsilon-martensite during tensile deformation in terms of structural evolution in the surrounding gamma-matrix: many dislocations that were introduced into the gamma-matrix during the hot-rolling process were consumed to produce epsilon-martensite, together with strong interactions between dislocations in the gamma-matrix. As a result, the SIMT behavior during tensile deformation was accelerated through the consumption of these lattice defects, and the nucleation sites for the SIMT epsilon-phase transformed into intergranular regions upon hot rolling. Consequently, the hot-rolled Co-Cr-Mo alloy simultaneously exhibited an enhanced strain hardening and a high yield strength. The results of this study suggest the possibility of a novel approach for controlling the $$gamma$$ to $$varepsilon$$ SIMT behavior, and ultimately, the performance of the alloy in service by manipulating the initial dislocation structures.

報告書

FINAS汎用非線形構造解析システム解析例題書(第2版)

岩田 耕司; 月森 和之; 千葉 隆久*; 酒井 新吉*; 上野 睦郎*; 坂井 哲也*; 酒井 光*

JNC TN9520 2003-006, 569 Pages, 2003/09

JNC-TN9520-2003-006.pdf:9.55MB

本解析例題書は、汎用非線形構造解析システムFINAS (Finite Element Nonlinear Structural Analysis System)による各種解析例を収録したものである。解析例題書は基礎編と応用編に分かれており、基礎編は解析タイプごとに理論解等の参照解がある基本的例題を、応用編はより複雑で実際的な例題を取り上げている。各例題は、初心者でも追計算が可能なように、できる限り全入力データリストと主要結果を載せるようにした。なお、ここでの解析はすべてFINAS Version 13.0により実行したものである。

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