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Journal Articles

Ion tracks and nanohillocks created in natural zirconia irradiated with swift heavy ions

Ishikawa, Norito; Fukuda, Shoma; Nakajima, Toru; Ogawa, Hiroaki; Fujimura, Yuki; Taguchi, Tomitsugu*

Materials, 17(3), p.547_1 - 547_21, 2024/02

Natural monoclinic zirconia (baddeleyite) was irradiated with 340-MeV Au ions, and the irradiation-induced nanostructures (i.e., ion tracks and nanohillocks) were observed using transmission electron microscopy. The diameter of the nanohillocks is approximately 10 nm, which is similar to the maximum molten region size calculated using the analytical thermal spike model. Ion tracks are imaged as strained regions that maintain their crystalline structure. The cross-sections of most of the ion tracks are imaged as parallelopiped or rectangular contrasts as large as 10 nm. These results strongly indicate that the molten region is recrystallized anisotropically, reflecting the lattice structure. Furthermore, low-density track cores are formed in the center of the ion tracks. The formation of low-density track cores can be attributed to the ejection of molten matter toward the surface.

Journal Articles

Examination of the wet analysis for the (U-Th)/He method; Attempt to determine the contents of parent nuclides based on the calibration curve method

Fukuda, Shoma; Kagami, Saya

Fisshion, Torakku Nyusureta, (36), p.14 - 18, 2023/12

For the determination of parent nuclides in the (U-Th)/He method, the isotope dilution method using U and Th isotope spikes is commonly employed worldwide, and much knowledge has been accumulated. On the other hand, the possession and use of these spikes are strictly restricted, which makes the application of the isotope dilution method itself difficult. After the complete dissolution of apatite and zircon by the wet method, we have therefore attempted to verify the calibration curve method for measuring the concentration of the parent nuclides. Durango apatite and Fish Canyon Tuff zircon, which are well-known as the age standard samples for the fission track method, were used as analytical samples. In this presentation, we will introduce some of the results of the determination of parent nuclides (U, Th, Sm) in each mineral sample based on the calibration curve method as well as results of evaluating the suitable internal standards (Bi, Tl) to determine the contents of parent nuclides.

Journal Articles

Zircon U-Pb dates from the Taiheizan Complex Plutons in Akita Prefecture, NE Japan

Nakajima, Toru; Nagata, Mitsuhiro; Fukuda, Shoma; Sueoka, Shigeru

Chishitsugaku Zasshi (Internet), 129(1), p.503 - 507, 2023/11

Zircon U-Pb dating was carried out on granitic rocks from plutons in the Taiheizan Complex in Akita Prefecture, NE Japan. Two granodiorites from the Main Intrusive Rocks yielded weighted mean 206Pb/238U dates of 103.4$$pm$$1.0 Ma and 115.6$$pm$$1.1 Ma (1SE). Three porphyrygranite from the Young Intrusive Rocks yielded weighted mean 206Pb/238U dates of 11.4$$pm$$0.1 Ma, 4.7$$pm$$0.1Ma, and 4.8$$pm$$0.1 Ma (1SE). The older and younger dates can be interpreted as the ages of early and later stages of granitic intrusion at the sampling locations. The Pliocene U-Pb dates suggest that the Nibetsu Body in the Young Intrusive Rocks is one of the youngest granitic plutons currently exposed on Earth.

JAEA Reports

Research plan on geosphere stability for long-term isolation of radioactive waste (Scientific program for fiscal year 2023)

Niwa, Masakazu; Shimada, Koji; Sueoka, Shigeru; Fujita, Natsuko; Yokoyama, Tatsunori; Ogita, Yasuhiro; Fukuda, Shoma; Nakajima, Toru; Kagami, Saya; Ogata, Manabu; et al.

JAEA-Review 2023-017, 27 Pages, 2023/10

JAEA-Review-2023-017.pdf:0.94MB

This report is a plan of research and development (R&D) on geosphere stability for long-term isolation of high-level radioactive waste (HLW) in Japan Atomic Energy Agency (JAEA), in fiscal year 2023. The objectives and contents in fiscal year 2023 are described in detail based on the JAEA 4th Medium- and Long-term Plan (fiscal years 2022-2028). In addition, the background of this research is described from the necessity and the significance for site investigation and safety assessment, and the past progress. The plan framework is structured into the following categories: (1) Development and systematization of investigation techniques, (2) Development of models for long-term estimation and effective assessment, (3) Development of dating techniques.

JAEA Reports

Annual report for research on geosphere stability for long-term isolation of radioactive waste in fiscal year 2022

Niwa, Masakazu; Shimada, Koji; Sueoka, Shigeru; Ishihara, Takanori; Ogawa, Hiroki; Hakoiwa, Hiroaki; Watanabe, Tsuyoshi; Nishiyama, Nariaki; Yokoyama, Tatsunori; Ogata, Manabu; et al.

JAEA-Research 2023-005, 78 Pages, 2023/10

JAEA-Research-2023-005.pdf:6.51MB

This annual report documents the progress of research and development (R&D) in the 1st fiscal year of the Japan Atomic Energy Agency 4th Medium- and Long-term Plan (fiscal years 2022-2028) to provide the scientific base for assessing geosphere stability for long-term isolation of high-level radioactive waste. The plan framework is structured into the following categories: (1) Development and systematization of investigation techniques, (2) Development of models for long-term estimation and effective assessment, (3) Development of dating techniques. The current status of R&D activities with previous scientific and technological progress is summarized.

Journal Articles

Evaluation of suitability of zircon as standard materials based on thermal history; Example of the Wassogatake Formation in Ishikawa Prefecture

Nagata, Mitsuhiro; Nakajima, Toru; Fukuda, Shoma; Sueoka, Shigeru; Yagi, Koshi*; Yokoyama, Tatsunori

Fisshion, Torakku Nyusureta, (36), p.9 - 13, 2023/00

Zircon U-Pb and fission track (FT) dating and moonstone (sanidine) K-Ar dating of the Wassogatake Formation in the southern part of Hakusan City, Ishikawa Prefecture were carried out as part of the search for zircon standard materials for dating. The weighted average U-Pb dates obtained from the three samples are ca. 21.9-21.7 Ma, overlapping within the uncertainty range. Zircon FT and moonstone K-Ar dates were obtained younger ages from some samples. In addition, the track lengths of the three samples are short. Based on the above results, the zircons of the Wassogatake Formation are effective for the high closure temperature dating method (e.g., U-Pb dating), but are not suitable for the low closure temperature dating method (e.g., FT dating).

Journal Articles

Toward fission-track dating of baddeleyite; First reports and discussions on etching experiments

Nakajima, Toru; Fukuda, Shoma; Nagata, Mitsuhiro; Danhara, Toru*; Iwano, Hideki*; Sueoka, Shigeru

Fisshion, Torakku Nyusureta, (35), p.34 - 36, 2022/12

In this presentation, we report the results of fission-track etching experiments for the practical use of baddeleyite fission-track dating and a brief discussion of the results.

Journal Articles

Evaluation of potential age standards for zircon (U-Th)/He thermochronometry; Results from further chronometric investigations

Fukuda, Shoma; Kohn, B. P.*; Sueoka, Shigeru; Danhara, Toru*; Iwano, Hideki*; Tagami, Takahiro*

Fisshion, Torakku Nyusureta, (35), p.7 - 10, 2022/12

In order to establish the age standard of zircon (U-Th)/He method, we performed zircon (U-Th)/He (hereinafter, ZHe) dating on 4 zircon samples. In this presentation, the Nohi rhyolite and the Mt. Wasso moonstone rhyolite as domestic samples, and Mt. Dromedary and OD-3 were also adopted as age standard zircons of fission-track and U-Pb methods. Consequently, regarding the ZHe age of the Nohi rhyolite indicated younger, which possibly reflected secondary heating, while ones of the others indicated consistent with previous thermochronometric data. Integrated with previously obtained ZHe data about 7 samples, the Utaosa rhyolite in the previous study showed a small age dispersion in grain ages, which infers a suitable candidate for the ZHe age standard. As future prospects, we are planning to conduct geochemical analyses and structure observations of these zircons for exploring the causal factors in age dispersions.

Journal Articles

An Experiment of complete dissolution of zircon crystals by high-temperature and pressure acid digestion for the (U-Th)/He method

Fukuda, Shoma; Kagami, Saya

Fisshion, Torakku Nyusureta, (35), p.11 - 14, 2022/12

In this study, we firstly attempted the wet-chemical analyses at Tono Geoscience Center based on a high-temperature and pressure acid digestion for determination of U-Th contents in zircon crystals. In the beginning, zircon crystals were annealed at 900 degrees Celsius for 48 hours to recover radiation damages, and annealed zircons were transferred and sunk into 29 M HF, and finally zircons were digested at 220 degrees Celsius for 70 hours. To verify that zircons were digested completely, Zr contents in zircons were measured as major elements by using ICP-MS (Agilent 7700x) based on the calibration curve method. As a result, theoretical values for Zr contents were obtained, these experimental conditions are thus valid for zircon digestion. Now, we are considering to perform these analyses in the clean booth and to select more appropriate analyses instruments and conditions for decreasing a blank level, which contributes to improve the determination of U-Th contents for zircon (U-Th)/He dating.

Journal Articles

Estimation of thermal/denudation histories in the Tanigawa-dake area based on thermochronological methods

Minami, Saki*; Sueoka, Shigeru; Fukuda, Shoma; Nagata, Mitsuhiro; Kohn, B. P.*; Yokoyama, Tatsunori; Kagami, Saya; Kajita, Yuya*; Tagami, Takahiro*

Fisshion, Torakku Nyusureta, (35), p.22 - 26, 2022/12

no abstracts in English

Journal Articles

Thermochronological data in the Kitakami Mountains and their interpretation

Kajita, Yuya*; Sueoka, Shigeru; Fukuda, Shoma; Tagami, Takahiro*

Fisshion, Torakku Nyusureta, (35), p.19 - 21, 2022/12

no abstracts in English

JAEA Reports

Research plan on geosphere stability for long-term isolation of radioactive waste (Scientific program for fiscal year 2022)

Sasao, Eiji; Ishimaru, Tsuneari; Niwa, Masakazu; Shimada, Akiomi; Shimada, Koji; Watanabe, Takahiro; Sueoka, Shigeru; Yokoyama, Tatsunori; Fujita, Natsuko; Ogita, Yasuhiro; et al.

JAEA-Review 2022-022, 29 Pages, 2022/09

JAEA-Review-2022-022.pdf:0.97MB

This report is a plan of research and development (R&D) on geosphere stability for long-term isolation of high-level radioactive waste (HLW) in Japan Atomic Energy Agency (JAEA), in fiscal year 2022. The objectives and contents in fiscal year 2022 are described in detail based on the JAEA 4th Medium- and Long-term Plan (fiscal years 2022-2028). In addition, the background of this research is described from the necessity and the significance for site investigation and safety assessment, and the past progress. The plan framework is structured into the following categories: (1) Development and systematization of investigation techniques, (2) Development of models for long-term estimation and effective assessment, (3) Development of dating techniques

Journal Articles

U-Pb zircon dates from the Utaosa Rhyolite of the Teragi Group

Nagata, Mitsuhiro; Fukuda, Shoma; Sueoka, Shigeru; Nakajima, Toru; Kajita, Yuya*; Minami, Saki*; Okamoto, Akira*; Tagami, Takahiro*

Fisshion, Torakku Nyusureta, (35), p.15 - 18, 2022/09

We performed U-Pb dating on zircons from the Utaosa Rhyolite of the Teragi Group as part of the search for standard materials for dating of zircons. Previous studies about Utaosa Rhyolite have reported ca. 2.30-2.77 Ma zircon fission track, zircon (U-Th)/He, and biotite K-Ar ages. U-Pb dating was carried out on the multi-collector inductively coupled plasma mass spectrometer with a laser ablation system. The weighted mean $$^{238}$$U-$$^{206}$$Pb ages of 2.65$$pm$$0.16 Ma and 2.66$$pm$$0.15 Ma were obtained from two samples. These ages are consistent with the ages from the previous studies. Therefore the results show that zircons from the Utaosa Rhyolite may be effective as a standard material.

Journal Articles

Low-temperature thermochronology of active arc-arc collision zone, South Fossa Magna region, central Japan

Sueoka, Shigeru; Kobayashi, Yumi*; Fukuda, Shoma; Kohn, B. P.*; Yokoyama, Tatsunori; Sano, Naomi*; Hasebe, Noriko*; Tamura, Akihiro*; Morishita, Tomoaki*; Tagami, Takahiro*

Tectonophysics, 828, p.229231_1 - 229231_17, 2022/04

 Times Cited Count:1 Percentile:24.42(Geochemistry & Geophysics)

The South Fossa Magna zone, central Japan, has been an active collision zone between the Honshu Arc and the Izu-Bonin Arc since the middle Miocene and provides an excellent setting for reconstructing the earliest stages of continent formation. Multi-system geo-thermochronometry was applied to different domains of the South Fossa Magna zone, together with some previously published data, to reveal mountain formation processes, i.e., vertical crustal movements. Nine granitic samples yielded zircon U-Pb ages of 10.2-5.8 Ma ($$n$$ = 2), apatite (U-Th)/He (AHe) ages of 42.8-2.6 Ma ($$n$$ = 7), and apatite fission-track (AFT) ages of 44.1-3.0 Ma ($$n$$ = 9). Thermal history inversion modeling based on the AHe and AFT data suggested rapid cooling events confined within the study region at $$sim$$6-2 Ma. The Kanto Mountains may have undergone a domal uplift in association with their collision with the Tanzawa Block at $$sim$$5 Ma. However, this uplift may have slowed down following the migration of the plate boundary and late Pliocene termination of the Tanzawa collision. The Minobu Mountains and possibly adjacent mountains may have been uplifted by the motional change of the Philippine Sea plate at $$sim$$3 Ma. Therefore, the mountain formation in the South Fossa Magna zone was mainly controlled by collisions of the Tanzawa and Izu Blocks and motional change of the Philippine Sea plate. Earlier collisions of the Kushigatayama Block at $$sim$$13 Ma and Misaka Block at $$sim$$10 Ma appeared to have had little effect on mountain formation. Together with a $$sim$$90 deg. clockwise rotation of the Kanto Mountains at 12-6 Ma, these observations suggest that horizontal deformation predominated during the earlier stage of arc-arc collision, and vertical movements due to buoyancy resulting from crustal shortening and thickening developed at a later stage.

Journal Articles

Two pulse intrusive events of the Pliocene Tanigawa-dake granites revealed from zircon U-Pb dating

Minami, Saki*; Nagata, Mitsuhiro; Sueoka, Shigeru; Fukuda, Shoma; Kajita, Yuya*; Ogita, Yasuhiro; Kagami, Saya; Yokoyama, Tatsunori; Tagami, Takahiro*

Earth, Planets and Space (Internet), 73(1), p.231_1 - 231_7, 2021/12

 Times Cited Count:1 Percentile:8.69(Geosciences, Multidisciplinary)

Journal Articles

Exploration of the age standard zircon for (U-Th)/He method; Chronometric investigations of the Nisatai Dacite

Fukuda, Shoma; Sueoka, Shigeru; Kanno, Mizuho; Kohn, B. P.*; Tagami, Takahiro*

Fisshion, Torakku Nyusureta, (34), p.9 - 13, 2021/12

In order to explore suitable zircon samples as standard minerals for the zircon (U-Th)/He (namely, ZHe) method, we have attempted to conduct ZHe analyses of the Nisatai dacite sampled in Iwate prefecture. Previous researches reported solid ages at 22-21 Ma and a rapid cooling pattern based on various geochronometric investigations, which inferred a potential of an age standard for ZHe method. Consequently, ZHe ages in this study yielded at 21.5 $$pm$$ 0.2 Ma having wide dispersion of grain ages from 40 Ma to 15 Ma, probably caused by random errors. As possible causes of age dispersion, the zoning of parent nuclei in a crystal and the heterogeneous rock pieces revealed by observations of thin-section are considerable. Therefore, the Nisatai dacite was concluded as unsuitable sample for the ZHe age standard. However, geochronologic data of other methods showed comparable ages such as zircon fission-track and U-Pb method, the Nisatai dacite may be used as these age standards. We will continue to explore another candidates for ZHe age standard, e.g., U-Pb age standards.

Journal Articles

Estimation of denudation history of the Kitakami Mountains based on apatite fission-track thermochronology

Kajita, Yuya*; Sueoka, Shigeru; Fukuda, Shoma; Yokoyama, Tatsunori; Kagami, Saya; Nagata, Mitsuhiro; Tagami, Takahiro*

Fisshion, Torakku Nyusureta, (34), p.14 - 16, 2021/12

For reconstructing the uplift/denudation history of the fore-arc side of the NE Japan Arc on geologic timescales, U-Pb dating and apatite fission-track (AFT) thermochronometry were applied to granitoids in Kitakami mountains. In addition, U-Pb dating for the Jodogahama rhyolite at the easternmost Kitakami mountains was also carried out to estimate the timing of volcanism and its thermal effect. Consequently, U-Pb ages of 122.7 Ma and 117.3 Ma for 2 samples of the Cretaceous granites and AFT ages ranging from 156.8 Ma to 70.3 Ma of 15 samples were obtained. Concerning the Jodogahama rhyolite, U-Pb age of 44.3 Ma was obtained. Integrated AFT data of this study and previous ones in Kitakami mountains, the trend of ages shows younging toward west. Although such age trend can be explained by volcanism of the Jodogahama reflecting the migration of a paleo-volcanic front, all AFT ages exhibited significantly older than U-Pb data of the Jodogahama and the thermal inverse modeling based on track length distributions provided slow cooling patterns. These observations did not supported the reheating of volcanism as a cause of age trend. As future prospects, we are planning to improve the reliability of age data based on additional analyses and apply an ultra low-temperature thermochronometer, e.g., ESR method.

Journal Articles

Estimation of intrusion ages in the Miocene-Pliocene granodiorite around the Tanigawa-dake based on zircon U-Pb dating

Minami, Saki*; Nagata, Mitsuhiro; Sueoka, Shigeru; Fukuda, Shoma; Kajita, Yuya*; Ogita, Yasuhiro; Yokoyama, Tatsunori; Kagami, Saya; Tagami, Takahiro*

Fisshion, Torakku Nyusureta, (34), p.4 - 8, 2021/12

This study employed U-Pb dating for determining the intrusive age of young (several Ma) granitoids in Tanigawa-dake area, where rapid and intense uplift/denudation has probably occurred in Japan. As results, U-Pb age of 109 Ma for the Cretaceous granodiorite and 3.95-3.19 Ma about 3 samples of the Pliocene granodiorites were obtained. These U-Pb ages showed consistent with previously reported ages based on thermochronometers having lower closure temperatures such as K-Ar or zircon fission-track methods. All previous data indicated younger ages than U-Pb ones in this study. Therefore, our U-Pb data can be interpreted as intrusive ages of young granitoids, inferring multiple events possibly occurred at least twice and contributed to the formation in young granitoids in the Tanigawa-dake area.

Journal Articles

Report on the 17th International Conference on Thermochronology

Nakajima, Toru; Fukuda, Shoma; Ogata, Manabu; Sueoka, Shigeru

Fisshion, Torakku Nyusureta, (34), p.25 - 26, 2021/12

The 17th International Conference on Thermochronology (Thermo2021) was held on September 12-17, 2021 at the Eldorado Resort in downtown Santa Fe, New Mexico, USA. Due to the social situation and the spread of the COVID-19, the event had been postponed. In this paper, I report on the circumstances surrounding our participation in the conference, the contents and trends of the presentations made at the conference, and the tasks for the 2023 and 2025 conferences.

JAEA Reports

Annual report for research on geosphere stability for long-term isolation of radioactive waste in fiscal year 2020

Ishimaru, Tsuneari; Ogata, Nobuhisa; Kokubu, Yoko; Shimada, Koji; Niwa, Masakazu; Shimada, Akiomi; Watanabe, Takahiro; Sueoka, Shigeru; Yokoyama, Tatsunori; Fujita, Natsuko; et al.

JAEA-Research 2021-007, 65 Pages, 2021/10

JAEA-Research-2021-007.pdf:4.21MB

This annual report documents the progress of research and development (R&D) in the 6th fiscal year during the JAEA 3rd Mid- and Long-term Plan (fiscal years 2015-2021) to provide the scientific base for assessing geosphere stability for long-term isolation of the high-level radioactive waste. The planned framework is structured into the following categories: (1) Development and systematization of investigation techniques, (2) Development of models for long-term estimation and effective assessment, (3) Development of dating techniques. The current status of R&D activities with previous scientific and technological progress is summarized.

88 (Records 1-20 displayed on this page)