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Journal Articles

Internal strain measurement by neutron diffraction under transverse compressive stress for Nb$$_{3}$$Sn wires with and without Cu-Nb reinforcement

Nakamoto, Mio*; Sugano, Michinaka*; Ogitsu, Toru*; Sugimoto, Masahiro*; Taniguchi, Ryo*; Hirose, Kiyoshige*; Kawasaki, Takuro; Gong, W.; Harjo, S.; Awaji, Satoshi*; et al.

IEEE Transactions on Applied Superconductivity, 34(5), p.8400806_1 - 8400806_6, 2024/08

Journal Articles

Mechanical properties of base metal and heat-affected zone in friction-stir-welded AA6061-T6 at ultra-low temperature of 20 K

Nguyen, T.-D.*; Singh, C.*; Kim, Y. S.*; Han, J. H. *; Lee, D.-H.*; Lee, K.*; Harjo, S.; Lee, S. Y.*

Journal of Materials Research and Technology, 31, p.1547 - 1556, 2024/07

Journal Articles

Microscopic insights of the extraordinary work-hardening due to phase transformation

Ma, Y.*; Naeem, M.*; Zhu, L.*; He, H.*; Sun, X.*; Yang, Z.*; He, F.*; Harjo, S.; Kawasaki, Takuro; Wang, X.-L.*

Acta Materialia, 270, p.119822_1 - 119822_13, 2024/05

Journal Articles

In-situ neutron diffraction study of serration-involved ultra-cryogenic deformation behavior at 15 K

Kim, Y. S.*; Chae, H.*; Lee, D.-Y.*; Han, J. H. *; Hong, S.-K.*; Na, Y. S.*; Harjo, S.; Kawasaki, Takuro; Woo, W.*; Lee, S.-Y.*

Materials Science & Engineering A, 899, p.146453_1 - 146453_7, 2024/05

Journal Articles

Mechanical stability of retained austenite and texture evolution in additively manufactured stainless steel

Chae, H.*; Huang, E.-W.*; Jain, J.*; Lee, D.-H.*; Harjo, S.; Kawasaki, Takuro; Lee, S. Y.*

Metals and Materials International, 30(5), p.1321 - 1330, 2024/05

Journal Articles

Recrystallization of bulk nanostructured magnesium alloy AZ31 after severe plastic deformation; An in situ diffraction study

Liss, K.-D.*; Han, J.-K.*; Blankenburg, M.*; Lienert, U.*; Harjo, S.; Kawasaki, Takuro; Xu, P. G.; Yukutake, Eitaro*; Kawasaki, M.*

Journal of Materials Science, 59(14), p.5831 - 5853, 2024/04

 Times Cited Count:0 Percentile:0.00(Materials Science, Multidisciplinary)

Journal Articles

${it In situ}$ neutron diffraction revealing the achievement of excellent combination of strength and ductility in metastable austenitic steel by grain refinement

Mao, W.; Gong, W.; Harjo, S.; Morooka, Satoshi; Gao, S.*; Kawasaki, Takuro; Tsuji, Nobuhiro*

Journal of Materials Science & Technology, 176, p.69 - 82, 2024/03

 Times Cited Count:0 Percentile:0.00(Materials Science, Multidisciplinary)

The yield stress of Fe-24Ni-0.3C (wt.%) metastable austenitic steel increased 3.5 times (158 $$rightarrow$$ 551 MPa) when the average grain size decreased from 35 $$mu$$m (coarse-grained [CG]) to 0.5 $$mu$$m (ultrafine-grained [UFG]), whereas the tensile elongation was kept large (0.87 $$rightarrow$$ 0.82). ${it In situ}$ neutron diffraction measurements of the CG and UFG Fe-24Ni-0.3C steels were performed during tensile deformation at room temperature to quantitatively elucidate the influence of grain size on the mechanical properties and deformation mechanisms. The initial stages of plastic deformation in the CG and UFG samples were dominated by dislocation slip, with deformation-induced martensitic transformation (DIMT) also occurring in the later stage of deformation. Results show that grain refinement increases the initiation stress of DIMT largely and suppresses the rate of DIMT concerning the strain, which is attributed to the following effects. (i) Grain refinement increased the stabilization of austenite and considerably delayed the initiation of DIMT in the $$<$$111$$>$$//LD (LD: loading direction) austenite grains, which were the most stable grains for DIMT. As a result, most of the $$<$$111$$>$$//LD austenite grains in the UFG specimens failed to transform into martensite. (ii) Grain refinement also suppressed the autocatalytic effect of the martensitic transformation. Nevertheless, the DIMT with the low transformation rate in the UFG specimen was more efficient in increasing the flow stress and more appropriate to maintain uniform deformation than that in the CG specimen during deformation. The above phenomena mutually contributed to the excellent combination of strength and ductility of the UFG metastable austenitic steel.

Journal Articles

Cryogenic deformation behavior of a dual-phase Mg-Li alloy investigated by in-situ neutron diffraction

Gong, W.; Gholizadeh, R.*; Kawasaki, Takuro; Aizawa, Kazuya; Harjo, S.

Magnesium Technology 2024, p.89 - 90, 2024/03

Journal Articles

Contributions of multimodal microstructure in the deformation behavior of extruded Mg alloys containing LPSO phase

Hagihara, Koji*; Mayama, Tsuyoshi*; Yamasaki, Michiaki*; Harjo, S.; Tokunaga, Toko*; Yamamoto, Kazuki*; Sugita, Mika*; Aoyama, Kairi*; Gong, W.; Nishimoto, Soya*

International Journal of Plasticity, 173, p.103865_1 - 103865_21, 2024/02

Journal Articles

Microstructure and plasticity evolution during L$"u$ders deformation in an Fe-5Mn-0.1C medium-Mn steel

Koyama, Motomichi*; Yamashita, Takayuki*; Morooka, Satoshi; Sawaguchi, Takahiro*; Yang, Z.*; Hojo, Tomohiko*; Kawasaki, Takuro; Harjo, S.

Tetsu To Hagane, 110(3), p.197 - 204, 2024/02

 Times Cited Count:0 Percentile:0.02

Journal Articles

Hierarchical deformation heterogeneity during L$"u$ders band propagation in an Fe-5Mn-0.1C medium Mn steel clarified through ${it in situ}$ scanning electron microscopy

Koyama, Motomichi*; Yamashita, Takayuki*; Morooka, Satoshi; Yang, Z.*; Varanasi, R. S.*; Hojo, Tomohiko*; Kawasaki, Takuro; Harjo, S.

Tetsu To Hagane, 110(3), p.205 - 216, 2024/02

 Times Cited Count:0 Percentile:0.02

Journal Articles

Martensitic transformation behavior of Fe-Ni-C alloys monitored by ${it in-situ}$ neutron diffraction during cryogenic cooling

Yamashita, Takayuki*; Harjo, S.; Kawasaki, Takuro; Morooka, Satoshi; Gong, W.; Fujii, Hidetoshi*; Tomota, Yo*

ISIJ International, 64(2), p.192 - 201, 2024/01

 Times Cited Count:0 Percentile:0.02

Journal Articles

Multi-aspect characterization of low-temperature tempering behaviors in high-carbon martensite

Zhang, Y.*; Marusawa, Kenji*; Kudo, Kohei*; Morooka, Satoshi; Harjo, S.; Miyamoto, Goro*; Furuhara, Tadashi*

ISIJ International, 64(2), p.245 - 256, 2024/01

 Times Cited Count:0 Percentile:0.02

Journal Articles

Deformation-induced martensitic transformation at tensile and compressive deformations of bainitic steels with different carbon contents

Ueji, Rintaro*; Gong, W.; Harjo, S.; Kawasaki, Takuro; Shibata, Akinobu*; Kimura, Yuji*; Inoue, Tadanobu*; Tsuchida, Noriyuki*

ISIJ International, 64(2), p.459 - 465, 2024/01

Journal Articles

Probing deformation behavior of a refractory high-entropy alloy using ${it in situ}$ neutron diffraction

Zhou, Y.*; Song, W.*; Zhang, F.*; Wu, Y.*; Lei, Z.*; Jiao, M.*; Zhang, X.*; Dong, J.*; Zhang, Y.*; Yang, M.*; et al.

Journal of Alloys and Compounds, 971, p.172635_1 - 172635_7, 2024/01

 Times Cited Count:0 Percentile:0.00(Chemistry, Physical)

Journal Articles

Principal preferred orientation evaluation of steel materials using time-of-flight neutron diffraction

Xu, P. G.; Zhang, S.-Y.*; Harjo, S.; Vogel, S. C.*; Tomota, Yo*

Quantum Beam Science (Internet), 8(1), p.7_1 - 7_13, 2024/01

Journal Articles

Stress evaluation method by neutron diffraction for HCP-structured magnesium alloy

Harjo, S.; Gong, W.; Kawasaki, Takuro

Quantum Beam Science (Internet), 7(4), p.32_1 - 32_13, 2023/12

Journal Articles

Effects of dislocation arrangement and character on the work hardening of lath martensitic steels

Dannoshita, Hiroyuki*; Hasegawa, Hiroshi*; Higuchi, Sho*; Matsuda, Hiroshi*; Gong, W.; Kawasaki, Takuro; Harjo, S.; Umezawa, Osamu*

Scripta Materialia, 236, p.115648_1 - 115648_5, 2023/11

 Times Cited Count:0 Percentile:0.00(Nanoscience & Nanotechnology)

Journal Articles

Measurement of mechanical behavior of $$^{11}$$B-enriched MgB$$_{2}$$ wire using a pulsed neutron source

Machiya, Shutaro*; Osamura, Kozo*; Hishinuma, Yoshimitsu*; Taniguchi, Hiroyasu*; Harjo, S.; Kawasaki, Takuro

Quantum Beam Science (Internet), 7(4), p.34_1 - 34_17, 2023/10

Journal Articles

Quantitatively evaluating the huge L$"u$ders band deformation in an ultrafine grain stainless steel by combining ${it in situ}$ neutron diffraction and digital image correlation analysis

Mao, W.; Gao, S.*; Gong, W.; Harjo, S.; Kawasaki, Takuro; Tsuji, Nobuhiro*

Scripta Materialia, 235, p.115642_1 - 115642_6, 2023/10

 Times Cited Count:3 Percentile:78.38(Nanoscience & Nanotechnology)

In the present study, a hybrid ${it in situ}$ neutron diffraction and digital image correlation measurement was performed on tensile deformation of an ultrafine grain (UFG) stainless steel exhibiting a huge L$"u$ders band deformation to evaluate the individual contribution of the austenite matrix and the deformation-induced martensite to the strain hardening during the propagation of the band. Quantitative analysis revealed that the strain hardening of the austenite matrix was insufficient to maintain a uniform deformation when the flow stress was greatly enhanced by the UFG structure. The strain hardening required for the L$"u$ders band to propagate was mostly provided by the formation of martensite and the high internal stress within it.

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