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論文

Structural phase transition in cobalt oxyfluoride Co$$_{3}$$Sb$$_{4}$$O$$_{6}$$F$$_{6}$$ observed by high-resolution synchrotron and neutron diffraction

下野 聖矢*; 石橋 広記*; 永吉 祐輔*; 池野 豪一*; 河口 彰吾*; 萩原 雅人; 鳥居 周輝*; 神山 崇*; 市橋 克哉*; 西原 禎文*; et al.

Journal of Physics and Chemistry of Solids, 163, p.110568_1 - 110568_7, 2022/04

 被引用回数:0 パーセンタイル:17.17(Chemistry, Multidisciplinary)

The structural phase transition from cubic ($$Ibar{4}3m$$) to a $$c > a$$ tetragonal ($$Ibar{4}$$) at $$T_{rm S}$$ $$sim$$ 180 K was found in non-centrosymmetric oxyfluoride Co$$_{3}$$Sb$$_{4}$$O$$_{6}$$F$$_{6}$$ by high-resolution neutron and synchrotron powder diffraction. To investigate this phase transition, specific heat, magnetization, and dielectric measurements were performed. Although the specific heat and dielectric constant showed anomalies at $$T_{rm S}$$, a phase transition to ferroelectricity was not observed in the polarization hysteresis loop down to 30 K. The rotation of the CoO$$_{2}$$F$$_{4}$$ octahedron was observed at $$T_{rm S}$$ from the structural analysis using synchrotron and neutron powder diffraction data. It was found that the magnetic phase transition from paramagnetic to G-type antiferromagnetic occurred at $$T_{rm N}$$ $$sim$$ 67 K, at which a peak was observed in the specific heat measurements, via magnetic structure analysis using neutron powder diffraction data. The magnetic moments of Co$$^{2+}$$ were aligned along the tetragonal $$c$$-axis direction with a Co$$^{2+}$$ moment of 2.80(1) $$mu_{rm B}$$ at 13 K.

論文

Magnetic structures of FeTiO$$_3$$-Fe$$_2$$O$$_3$$ solid solution thin films studied by soft X-ray magnetic circular dichroism and ab initio multiplet calculations

北條 元*; 藤田 晃司*; 池野 豪一*; 的場 智彦*; 溝口 照康*; 田中 功*; 中村 哲也*; 竹田 幸治; 岡根 哲夫; 田中 勝久*

Applied Physics Letters, 104(11), p.112408_1 - 112408_5, 2014/03

AA2015-0416.pdf:1.6MB

 被引用回数:7 パーセンタイル:34.83(Physics, Applied)

The solid solutions between ilmenite and hematite have recently attracted considerable attention as a spintronic material due to their interesting magnetic and electrical properties. In this study, the electronic and magnetic structures of epitaxially grown ilmenite-hematite solid solution thin films were investigated by combining X-ray absorption near-edge structure (XANES), X-ray magnetic circular dichroism (XMCD) for two different crystallographic projections, and first-principles theoretical calculations.

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