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JAEA Reports

FBR metallic materials test manual (2023 revised edition)

Imagawa, Yuya; Toyota, Kodai; Onizawa, Takashi; Kato, Shoichi

JAEA-Testing 2023-004, 76 Pages, 2024/03

JAEA-Testing-2023-004.pdf:2.08MB

This manual describes the methods for conducting material tests in air, argon gas, and sodium, and for organizing the data obtained, as a part of the development of high-temperature structural design technology for fast reactors. This manual reflects the revision of test methods in Japanese Industrial Standards (JIS) to the "FBR Metallic Materials Test Manual, PNC TN241 77-03" published in 1977 and the "FBR Metallic Materials Test Manual (Revised Edition), JNC TN9520 2001-001" published in 2001. Also, it was written with reference to the recommended room temperature / elevated temperature tensile test method by the Japan Society of Mechanical Engineers (JSME) and the test standard for the elevated-temperature low-cycle fatigue test method by the Society of Materials Science, Japan (JSMS), which are the standard for material test methods in the domestic academic society.

Journal Articles

Validation of the applicability of the best-fit fatigue curves for 550$$^{circ}$$C in Mod.9Cr-1Mo steel to 1$$times$$10$$^{11}$$ cycles

Toyota, Kodai; Imagawa, Yuya; Onizawa, Takashi; Kato, Shoichi; Furuya, Yoshiyuki*

Nihon Kikai Gakkai Rombunshu (Internet), 89(928), p.23-00206_1 - 23-00206_15, 2023/12

In order to design fast reactors, it is necessary to consider high cycle fatigue of structural materials up to 1$$times$$10$$^{9}$$ cycles; to evaluate high cycle fatigue at 1$$times$$10$$^{9}$$ cycles, it is necessary to develop a best-fit fatigue curve applicable up to 1$$times$$10$$^{11}$$ cycles. In this study, high cycle fatigue tests were conducted under strain-controlled conditions and ultrasonic fatigue tests were also conducted to develop a high cycle fatigue evaluation method for Mod.9Cr-1Mo steel, which is a candidate material for fast reactor structural materials. Based on the test results, the best-fit fatigue curves were extended and the applicability of the JSME best-fit fatigue curves up to 1$$times$$10$$^{11}$$ cycles was verified.

Journal Articles

Material data acquisition activities to develop the material strength standard for sodium-cooled fast reactors

Toyota, Kodai; Onizawa, Takashi; Wakai, Takashi; Hashidate, Ryuta; Kato, Shoichi

Proceedings of International Conference on Fast Reactors and Related Fuel Cycles; Sustainable Clean Energy for the Future (FR22) (Internet), 10 Pages, 2022/04

JAEA Reports

Evaluation of tensile and creep properties on 9Cr-ODS steel claddings

Yano, Yasuhide; Hashidate, Ryuta; Tanno, Takashi; Imagawa, Yuya; Kato, Shoichi; Onizawa, Takashi; Ito, Chikara; Uwaba, Tomoyuki; Otsuka, Satoshi; Kaito, Takeji

JAEA-Data/Code 2021-015, 64 Pages, 2022/01

JAEA-Data-Code-2021-015.pdf:2.6MB

From a view point of practical application of fast breeder reactor cycles, which takes advantage of safety and economic efficiency and makes a contribution of volume reduction and mitigation of degree of harmfulness of high-level radioactive waste, it is necessary to develop fuel cladding materials for fast reactors (FRs) in order to achieve high-burnup. Oxide dispersion strengthened (ODS) steel have been studied for use as potential fuel cladding materials in FRs owing to their excellent resistance to swelling and their high-temperature strength in Japan Atomic Energy Agency. It is very important to establish the materials strength standard in order to apply ODS steels as a fuel cladding. Therefore, it is necessary to acquire the mechanical properties such as tensile, creep rupture strength tests and so on. In this study, tensile and creep rupture strengths of 9Cr-ODS steel claddings were evaluated using by acquired these data. Because of the phase transformation temperature of 9Cr-ODS steel, temperature range for the evaluation was divided into two ones at AC1 transformation temperature of 850$$^{circ}$$C.

Journal Articles

Development of a supplementary outboard side thruster system for dynamic positioning control of autonomous surface vehicle

Kato, Tetsu*; Kawamura, Yamato*; Tahara, Junichiro*; Baba, Shoichiro*; Sanada, Yukihisa; Fujii, Shun*

International Journal of Offshore and Polar Engineering, 31(3), p.316 - 324, 2021/09

 Times Cited Count:2 Percentile:20.79(Engineering, Civil)

The development of a side thruster system (vehicle (ASV)) that can maintain the direction of travel on the autonomous surface will be explained. Currently, we are working on a mud radioactivity survey in collaboration with Japan Agency for Marine-Earth Science and Technology, Japan Atomic Energy Agency, and Tokyo University of Marine Science and Technology. Deposited at the mouth of Fukushima Prefecture, Japan, the main purpose is to collect unmanned mud using ASV. The Mad Collection has developed a side thruster system and implemented it in ASV. We have confirmed the operation of the ASV with the joystick by using the thruster system for operating the ASV by one person using the joystick.

Journal Articles

Proposal of simulation material test technique for clarifying the structure failure mechanisms under excessive seismic loads

Hashidate, Ryuta; Kato, Shoichi; Onizawa, Takashi; Wakai, Takashi; Kasahara, Naoto*

Proceedings of ASME 2021 Pressure Vessels and Piping Conference (PVP 2021) (Internet), 9 Pages, 2021/07

It is very essential to clarify the structure failure mechanisms under excessive seismic loads. However, structural tests using actual structural materials are very difficult and expensive. Therefore, we have proposed the structure test approach using lead alloys in order to simulate the structure failure mechanisms under the excessive seismic loads. In this study, we conducted material tests using lead alloy and verified the effectiveness of the simulated material tests. Moreover, we formulated inelastic constitutive equations (best fit fatigue curve equation and cyclic stress range - strain range relationship equation) of lead alloy based on the results of a series of material tests. Nonlinear numerical analyses, e.g. finite element analyses, can be performed using the proposed equations. A series of simulation material test technique enables structural tests and analyses using lead alloy to simulate the structure failure phenomena under excessive seismic loads.

Journal Articles

Invention of automatic movement and dynamic positioning control method of unmanned vessel for mud mining

Fujii, Shun*; Kato, Tetsu*; Kawamura, Yamato*; Tahara, Junichiro*; Baba, Shoichiro*; Sanada, Yukihisa

Proceedings of 26th International Symposium on Artificial Life and Robotics (AROB 26th 2021), p.280 - 285, 2021/01

In recent years, autonomously navigating unmanned vessels have been actively studied, and many of these vessels are designed to perform unmanned operations such as observation and transportation. On the other hand, this study uses an unmanned ship with a moon pool that collects seabed mud, which is difficult for ordinary ships. Vessels used since the area are highly turbulent due to wind, so it is necessary to maintain a fixed point and orientation when removing mud. The ship is equipped with side thrusters to maintain a fixed point and bow direction. In this study, the control method was devised to maintain fixed point and orientation, and the control method is based on robust sliding mode control. The proposed control method was verified by simulation, and the desired behavior was confirmed.

Journal Articles

Development of side thruster system for ASV

Kato, Tetsu*; Kawamura, Yamato*; Tahara, Junichiro*; Baba, Shoichiro*; Sanada, Yukihisa

Proceedings of the 30th (2020) International Ocean and Polar Engineering Conference (ISOPE 2020) (USB Flash Drive), p.1255 - 1260, 2020/10

Journal Articles

High-temperature creep deformation in FeCrAl-oxide dispersion strengthened alloy cladding

Ukai, Shigeharu; Kato, Shoichi; Furukawa, Tomohiro; Otsuka, Satoshi

Materials Science & Engineering A, 794, p.139863_1 - 139863_13, 2020/09

 Times Cited Count:44 Percentile:95.09(Nanoscience & Nanotechnology)

The FeCrAl-oxide dispersion strengthened (ODS) alloy is the promising cladding material for the accident-tolerant fuel (ATF) of the light water reactors (LWR). Ring-creep tests for FeCrAl-ODS alloy cladding were carried out at 973 K and 1273 K. The dislocation detachment stress from the dispersoid was derived by considering the dislocation-dispersoid elastic interaction and the dislocation relaxation effect by climb motion. When the applied stress exceeds the dislocation detachment stress, dislocations overcome the dispersoids with the reduced values of the stress exponent. When the stress is lower than the dislocation detachment stress, grain boundary sliding (GBS) is dominant factor for the low strain rate creep deformation at 1273 K. Based on those findings, new constitutive equations for creep deformation were constructed, which is applicable to low stress, low strain rate and high temperature conditions encountered at the reactor sever accident.

Journal Articles

Proposal of simulation materials test technique and their constitutive equations for structural tests and analyses simulating severe accident conditions

Hashidate, Ryuta; Kato, Shoichi; Onizawa, Takashi; Wakai, Takashi; Kasahara, Naoto*

Proceedings of ASME 2020 Pressure Vessels and Piping Conference (PVP 2020) (Internet), 9 Pages, 2020/08

Although it is very essential to clarify how the structure collapses under the severe accident conditions, the failure mechanisms in excessive high temperatures are not clarified. However, it is very difficult and expensive to perform structural tests using actual structural materials. Therefore, we propose to use lead alloys instead of actual structural materials. For demonstration of analogy between the failure mechanisms of lead alloys structure at low temperature and those of the actual structures at high temperature, numerical analyses are required. Although the authors proposed inelastic constitutive equations for numerical analyses in 2019, the equations could not successfully express because of large variations observed in the material tests of the lead alloy. In this study, we propose the improved inelastic constitutive equations of the lead alloy on the basis of the material test results used by aged alloy which can stabilized the material characteristic.

Journal Articles

Electronic effects of nitrogen atoms of supports on Pt-Ni rhombic dodecahedral nanoframes for oxygen reduction

Kato, Masaru*; Nakahoshiba, Ryota*; Ogura, Kazuya*; Tokuda, Shoichi*; Yasuda, Satoshi; Higashi, Kotaro*; Uruga, Tomoya*; Uemura, Yohei*; Yagi, Ichizo*

ACS Applied Energy Materials (Internet), 3(7), p.6768 - 6774, 2020/07

 Times Cited Count:15 Percentile:62.59(Chemistry, Physical)

To understand electronic effects of nitrogen-doped and polymer-coated carbon supports on the catalytic activity of Pt-based nanostructured catalysts, we prepared Pt$$_{3}$$Ni nanoframes (NFs) supported on polybenzimidazole (PBI)-coated and uncoated carbon nanotubes for the oxygen reduction reaction (ORR), and then compared their catalytic activities and electronic properties with those of NFs immobilized on nitrogen-doped and undoped carbon supports. Although both PBI-coating and nitrogen-doping approaches improved the catalytic activity of NFs, ${it ex situ}$ X-ray photoelectron spectroscopy and ${it in situ}$ X-ray absorption spectroscopy revealed that nitrogen doping showed electronic effects on NFs, whereas PBI-coating showed almost no impact on the electronic state of NFs but stabilized Pt(OH)$$_{rm ad}$$ species under electrochemical conditions. Our studies demonstrate that difference in microscopic environments of nitrogen atoms at the catalyst/support interface is highly sensitive to the electronic effects of supports on Pt-based electrocatalysts.

Journal Articles

Development of ODS tempered martensitic steel for high burn up fuel cladding tube of SFR

Otsuka, Satoshi; Tanno, Takashi; Oka, Hiroshi; Yano, Yasuhide; Tachi, Yoshiaki; Kaito, Takeji; Hashidate, Ryuta; Kato, Shoichi; Furukawa, Tomohiro; Ito, Chikara; et al.

2018 GIF Symposium Proceedings (Internet), p.305 - 314, 2020/05

Oxide Dispersion Strengthened (ODS) steel has been developed worldwide as a high-strength and radiation-tolerant steel used for advanced nuclear system. Japan Atomic Energy Agency (JAEA) has been developing ODS steel as the primary candidate material of Sodium cooled Fast Reactor (SFR) high burn-up fuel cladding tube. Application of high burn-up fuel to SFR core can contribute to improvement of economical performance of SFR in conjunction with volume and hazardousness reduction of radioactive waste. This paper described the current status and future prospects of ODS tempered martensitic steel development in JAEA for SFR fuel application.

JAEA Reports

Material test data of SUS316 and SUS321, 1

Hashidate, Ryuta; Kato, Shoichi; Kurihara, Akikazu

JAEA-Data/Code 2019-005, 117 Pages, 2019/07

JAEA-Data-Code-2019-005.pdf:2.54MB

SUS316 and SUS321 are used for structural materials of the Fast Breeder Reactors (FBRs), because of excellent high creep strength. This report summarized the mechanical properties data on SUS316 and SUS321 obtained in various tests including the long-term material tests and the material tests in sodium.

Journal Articles

Ultra-high temperature creep rupture and transient burst strength of ODS steel claddings

Yano, Yasuhide; Sekio, Yoshihiro; Tanno, Takashi; Kato, Shoichi; Inoue, Toshihiko; Oka, Hiroshi; Otsuka, Satoshi; Furukawa, Tomohiro; Uwaba, Tomoyuki; Kaito, Takeji; et al.

Journal of Nuclear Materials, 516, p.347 - 353, 2019/04

 Times Cited Count:15 Percentile:86.05(Materials Science, Multidisciplinary)

9Cr-ODS steel claddings consisting of tempered martensitic matrix, showed prominent creep rupture strength at 1000 $$^{circ}$$C, which surpassed that of heat-resistant austenitic steels although creep rupture strength of tempered martensitic steels is generally lower than that of austenitic steels at high temperatures. The measured creep rupture strength of 9Cr-ODS steel claddings at 1000 $$^{circ}$$C was higher than that from extrapolated creep rupture trend curves formulated using data at temperatures from 650 to 850 $$^{circ}$$C. This superior strength seemed to be owing to transformation of the matrix from the $$alpha$$-phase to the $$gamma$$-phase. The transient burst strengths for 9Cr-ODS steel were much higher than those for 11Cr-ferritic/martensitic steel (PNC-FMS). Cumulative damage fraction analyses suggested that the life fraction rule can be used for the rupture life prediction of 9Cr-ODS steel and PNC-FMS claddings in the transient and accidental events with a certain accuracy.

Journal Articles

Post irradiation experiment about SiC-coated oxidation-resistant graphite for high temperature gas-cooled reactor

Shibata, Taiju; Mizuta, Naoki; Sumita, Junya; Sakaba, Nariaki; Osaki, Takashi*; Kato, Hideki*; Izawa, Shoichi*; Muto, Takenori*; Gizatulin, S.*; Shaimerdenov, A.*; et al.

Proceedings of 9th International Topical Meeting on High Temperature Reactor Technology (HTR 2018) (USB Flash Drive), 7 Pages, 2018/10

Graphite materials are used for the in-core components of High Temperature Gas-cooled Reactor (HTGR). Oxidation damage on the graphite components in air ingress accident is a crucial issue for the safety point of view. SiC coating on graphite surface is a possible technique to enhance oxidation resistance. However, it is important to confirm the integrity of this material against high temperature and neutron irradiation for the application of the in-core components. JAEA and Japanese graphite companies carried out the R&D to develop the oxidation-resistant graphite. JAEA and INP investigated the irradiation effects on the oxidation-resistant graphite by using a framework of ISTC partner project. This paper describes the results of post irradiation experiment about the neutron irradiated SiC-coated oxidation-resistant graphite. A brand of oxidation-resistant graphite shows excellent performance against oxidation test after the irradiation.

Journal Articles

Enhancement of oxidation tolerance of graphite materials for high temperature gas-cooled reactor

Mizuta, Naoki; Sumita, Junya; Shibata, Taiju; Osaki, Takashi*; Kato, Hideki*; Izawa, Shoichi*; Muto, Takenori*; Gizatulin, S.*; Sakaba, Nariaki

Tanso Zairyo Kagaku No Shinten; Nihon Gakutsu Shinkokai Dai-117-Iinkai 70-Shunen Kinen-Shi, p.161 - 166, 2018/10

To enhance oxidation resistance of graphite material for in-core components of HTGR, JAEA and four Japanese graphite companies; Toyo Tanso, IBIDEN, Tokai Carbon and Nippon Techno-Carbon, are carrying out for development of oxidation-resistant graphite by CVD-SiC coating. This paper describes the outline of neutron irradiation test about the oxidation-resistant graphite by WWR-K reactor of INP, Kazakhstan through an ISTC partner project. Prior to the irradiation test, the oxidation-resistant graphite by CVD-SiC coating of all specimens showed enough oxidation resistance under un-irradiation condition. The neutron irradiation test was already completed and out-of-pile oxidation test will be carried out at the hot-laboratory of WWR-K.

Journal Articles

Model calculation of Cr dissolution behavior of ODS ferritic steel in high-temperature flowing sodium environment

Otsuka, Satoshi; Tanno, Takashi; Oka, Hiroshi; Yano, Yasuhide; Kato, Shoichi; Furukawa, Tomohiro; Kaito, Takeji

Journal of Nuclear Materials, 505, p.44 - 53, 2018/07

AA2017-0603.pdf:1.7MB

 Times Cited Count:2 Percentile:20.93(Materials Science, Multidisciplinary)

A calculation model was constructed to systematically study the effects of environmental conditions (i.e. Cr concentration in sodium, test temperature, axial temperature gradient of fuel pin, and sodium flow velocity) on Cr dissolution behavior. Chromium dissolution was largely influenced by small changes in Cr concentration (i.e. chemical potential of Cr) in liquid sodium in the model calculation. Chromium concentration in sodium coolant, therefore, should be recognized as a critical parameter for the prediction and management of Cr dissolution behavior in the sodium-cooled fast reactor (SFR) core. Because the fuel column length showed no impact on dissolution behavior in the model calculation, no significant downstream effects possibly take place in the SFR fuel cladding tube due to the much shorter length compared with sodium loops in the SFR plant and the large axial temperature gradient. The calculated profile of Cr concentration along the wall-thickness direction was consistent with that measured in BOR-60 irradiation test where Cr concentration in sodium bulk flow was set at 0.07 wt ppm in the calculation.

Journal Articles

Thermal fatigue test on dissimilar welded joint between Gr.91 and 304SS

Wakai, Takashi; Kobayashi, Sumio; Kato, Shoichi; Ando, Masanori; Takasho, Hideki*

Proceedings of 25th International Conference on Nuclear Engineering (ICONE-25) (CD-ROM), 7 Pages, 2017/07

This paper describes a thermal fatigue test on a structural model with a dissimilar welded joint. In the present design of JSFR, there may be dissimilar welded joints between ferritic and austenitic steels especially in IHX and SG. Creep-fatigue is one of the most important failure modes in JSFR components. However, the creep-fatigue damage evaluation method has not been established for dissimilar welded joint. To investigate the evaluation method, structural test will be needed for verification. Therefore, a thermal fatigue test on a thick-wall cylinder with a circumferential dissimilar welded joint between Mod.9Cr-1Mo steel and 304SS was performed. Since the coefficients of thermal expansion of these steels were significantly different, buttering layer of Ni base alloy was installed between them. After the completion of the test, deep cracks were observed at the HAZ in 304SS, as well as at HAZ in Mod.9Cr-1Mo steel. There were many tiny surface cracks in BM of 304SS. According to the fatigue damage evaluation based on the finite element analysis results, the largest fatigue damage was calculated at HAZ in 304SS. Large fatigue damage was also estimated at BM of 304SS. Fatigue cracks were observed at HAZ and BM of 304SS in the test, so that analytical results are in a good agreement with the observations. However, though relatively small fatigue damage was estimated at HAZ in Mod.9Cr-1Mo steel, deep fatigue cracks were observed in the test. To identify the cause of such a discrepancy between the test and calculations, we performed a series of finite element analyses. Some metallurgical investigations were also performed.

Journal Articles

Ultra-high temperature tensile properties of ODS steel claddings under severe accident conditions

Yano, Yasuhide; Tanno, Takashi; Oka, Hiroshi; Otsuka, Satoshi; Inoue, Toshihiko; Kato, Shoichi; Furukawa, Tomohiro; Uwaba, Tomoyuki; Kaito, Takeji; Ukai, Shigeharu*; et al.

Journal of Nuclear Materials, 487, p.229 - 237, 2017/04

 Times Cited Count:37 Percentile:96.77(Materials Science, Multidisciplinary)

Ultra-high temperature ring tensile tests were carried out to investigate the tensile behavior of oxide dispersion strengthened (ODS) steel claddings and wrapper materials under severe accident conditions; temperatures ranged from room temperature to 1400$$^{circ}$$C which is near the melting point of core materials. The experimental results showed that tensile strength of 9Cr-ODS steel claddings was highest in the core materials at the ultra-high temperatures between 900 and 1200$$^{circ}$$C, but that there was significant degradation in tensile strength of 9Cr-ODS steel claddings above 1200$$^{circ}$$C. This degradation was attributed to grain boundary sliding deformation with $$gamma$$/$$delta$$ transformation, which was associated with reduced ductility. On the other hand, tensile strength of recrystallized 12Cr-ODS and FeCrAl-ODS steel claddings retained its high value above 1200 $$^{circ}$$C unlike the other tested materials. Present study includes the result of "R&D of ODS ferritic steel fuel cladding for maintaining fuel integrity at the high temperature accident condition" entrusted to Hokkaido University by the Ministry of Education, Culture, Sports, Science and Technology of Japan (MEXT).

Journal Articles

Evaluation on tolerance to failure of ODS ferritic steel claddings at the accident conditions of fast reactors

Uwaba, Tomoyuki; Yano, Yasuhide; Otsuka, Satoshi; Naganuma, Masayuki; Tanno, Takashi; Oka, Hiroshi; Kato, Shoichi; Kaito, Takeji; Ukai, Shigeharu*; Kimura, Akihiko*; et al.

Proceedings of 2017 International Congress on Advances in Nuclear Power Plants (ICAPP 2017) (CD-ROM), 7 Pages, 2017/04

Tolerance of fast rector fuel elements to failure in the typical accident conditions was evaluated for the oxide-dispersion-strengthened (ODS) ferritic steel claddings that are candidate of the cladding material for advanced fast reactors. The evaluation was based on the cladding creep damage, which was quantified by the cumulative damage fractions (CDFs). It was shown that the CDFs of the ODS ferritic steel cladding were substantially lower than the breach limit of 1.0 in the loss of flow and transient over power conditions until a passive reactor shutdown system operates.

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