neutron diffraction revealing the achievement of excellent combination of strength and ductility in metastable austenitic steel by grain refinement

Mao, W.; Gong, W.; Harjo, S.; Morooka, Satoshi; Gao, S.*; Kawasaki, Takuro; Tsuji, Nobuhiro*

Journal of Materials Science & Technology, 176, p.69 - 82, 2024/03

https://doi.org/10.1016/j.jmst.2023.07.036

The yield stress of Fe-24Ni-0.3C (wt.%) metastable austenitic steel increased 3.5 times (158 551 MPa) when the average grain size decreased from 35 m (coarse-grained [CG]) to 0.5 m (ultrafine-grained [UFG]), whereas the tensile elongation was kept large (0.87 0.82). neutron diffraction measurements of the CG and UFG Fe-24Ni-0.3C steels were performed during tensile deformation at room temperature to quantitatively elucidate the influence of grain size on the mechanical properties and deformation mechanisms. The initial stages of plastic deformation in the CG and UFG samples were dominated by dislocation slip, with deformation-induced martensitic transformation (DIMT) also occurring in the later stage of deformation. Results show that grain refinement increases the initiation stress of DIMT largely and suppresses the rate of DIMT concerning the strain, which is attributed to the following effects. (i) Grain refinement increased the stabilization of austenite and considerably delayed the initiation of DIMT in the 111//LD (LD: loading direction) austenite grains, which were the most stable grains for DIMT. As a result, most of the 111//LD austenite grains in the UFG specimens failed to transform into martensite. (ii) Grain refinement also suppressed the autocatalytic effect of the martensitic transformation. Nevertheless, the DIMT with the low transformation rate in the UFG specimen was more efficient in increasing the flow stress and more appropriate to maintain uniform deformation than that in the CG specimen during deformation. The above phenomena mutually contributed to the excellent combination of strength and ductility of the UFG metastable austenitic steel.

Hierarchical deformation heterogeneity during Lders band propagation in an Fe-5Mn-0.1C medium Mn steel clarified through scanning electron microscopy

Koyama, Motomichi*; Yamashita, Takayuki*; Morooka, Satoshi; Yang, Z.*; Varanasi, R. S.*; Hojo, Tomohiko*; Kawasaki, Takuro; Harjo, S.

Tetsu To Hagane, 110(3), p.205 - 216, 2024/02

https://doi.org/10.2355/tetsutohagane.TETSU-2023-052

Lattice parameters of austenite and martensite during transformation for Fe-18Ni alloy investigated through neutron diffraction

Gong, W.; Harjo, S.; Tomota, Yo*; Morooka, Satoshi; Kawasaki, Takuro; Shibata, Akinobu*; Tsuji, Nobuhiro*

Acta Materialia, 250, p.118860_1 - 118860_16, 2023/05

https://doi.org/10.1016/j.actamat.2023.118860

Hierarchical deformation heterogeneity during Lders band propagation in an Fe-5Mn-0.1C medium Mn steel clarified through scanning electron microscopy

Koyama, Motomichi*; Yamashita, Takayuki*; Morooka, Satoshi; Yang, Z.*; Varanasi, R. S.*; Hojo, Tomohiko*; Kawasaki, Takuro; Harjo, S.

ISIJ International, 62(10), p.2043 - 2053, 2022/10

https://doi.org/10.2355/isijinternational.ISIJINT-2022-098

structure observation of pyroelectric ceramics during power generation cycle

Kawasaki, Takuro; Fukuda, Tatsuo; Yamanaka, Satoru*; Sakamoto, Tomokazu*; Murayama, Ichiro*; Kato, Takanori*; Baba, Masaaki*; Hashimoto, Hideki*; Harjo, S.; Aizawa, Kazuya; et al.

Journal of Applied Physics, 131(13), p.134103_1 - 134103_7, 2022/04

https://doi.org/10.1063/5.0084166

Work hardening behavior of dual phase copper-iron alloy at low temperature

Yamashita, Takayuki*; Koga, Norimitsu*; Kawasaki, Takuro; Morooka, Satoshi; Tomono, Shohei*; Umezawa, Osamu*; Harjo, S.

Materials Science & Engineering A, 819, p.141509_1 - 141509_10, 2021/07

https://doi.org/10.1016/j.msea.2021.141509

Effect of solute carbon on the characteristic hardening of steel at high temperature

Koga, Norimitsu*; Umezawa, Osamu*; Yamamoto, Masayuki*; Yamamoto, Takashi*; Yamashita, Takayuki; Morooka, Satoshi; Kawasaki, Takuro; Harjo, S.

Metallurgical and Materials Transactions A, 52(3), p.897 - 901, 2021/03

https://doi.org/10.1007/s11661-020-06113-4

Role of retained austenite in low alloy steel at low temperature monitored by neutron diffraction

Yamashita, Takayuki; Morooka, Satoshi; Harjo, S.; Kawasaki, Takuro; Koga, Norimitsu*; Umezawa, Osamu*

Scripta Materialia, 177, p.6 - 10, 2020/03

https://doi.org/10.1016/j.scriptamat.2019.10.002

Change in mechanical properties by high-cycle loading up to Gigacycle for 316L stainless steel

Naoe, Takashi; Harjo, S.; Kawasaki, Takuro; Xiong, Z.*; Futakawa, Masatoshi

JPS Conference Proceedings (Internet), 28, p.061009_1 - 061009_6, 2020/02

https://doi.org/10.7566/JPSCP.28.061009

At the J-PARC, a mercury target vessel made of 316L SS suffers proton and neutron radiation environment. The target vessel also suffers cyclic impact stress caused by the proton beam-induced pressure waves. The vessel suffers higher than 4.510 cyclic loading during the expected service life of 5000 h. We have investigated fatigue strength 316L SS up to gigacycle in the previous studies. The cyclic hardening and softening behavior were observed. In this study, to evaluate the cyclic hardening/softening behavior, the dislocation densities of specimens were measured using the neutron diffraction method at the MLF BL-19. The result showed that the dislocation density of a 316L SS was increased with increasing the number of loading cycles. By contrast, in the case of cold-rolled 316L SS, annihilation and re-accumulation of dislocation by cyclic loading were observed. In the workshop, result of neutron diffraction measurement will be introduced with the progress of fatigue test.

Study on a unified criterion for preventing plastic strain accumulation due to long distance travel of temperature distribution

Okajima, Satoshi; Wakai, Takashi; Kawasaki, Nobuchika

Mechanical Engineering Journal (Internet), 4(5), p.16-00641_1 - 16-00641_11, 2017/10

http://doi.org/10.1299/mej.16-00641