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論文

Unique deformation behavior of ultrafine-grained 304 stainless steel at 20 K

Mao, W.*; Gong, W.; 川崎 卓郎; Gao, S.*; 伊東 達矢; 山下 享介*; Harjo, S.; Zhao, L.*; Wang, Q.*

Scripta Materialia, 264, p.116726_1 - 116726_6, 2025/07

 被引用回数:0

An ultrafine-grained 304 austenitic stainless steel exhibited pronounced serrated Luders deformation at 20 K, with stress and temperature oscillations reaching 200 MPa and 20 K. ${it In-situ}$ neutron diffraction and digital image correlation revealed discontinuous Luders band propagation and burst martensite formation. During deformation, austenite phase stress remained lower than at upper yielding, indicating elastic behavior. Notably, martensite phase stress stayed lower than austenite until fracture, likely due to stress relaxation from burst martensitic transformation at 20 K. The low martensite stress delayed brittle fracture until austenite plastically yielded during uniform deformation.

論文

Role of solute hydrogen on mechanical property enhancement in Fe-24Cr-19Ni austenitic steel; An ${it in situ}$ neutron diffraction study

伊東 達矢; 小川 祐平*; Gong, W.; Mao, W.*; 川崎 卓郎; 岡田 和歩*; 柴田 曉伸*; Harjo, S.

Acta Materialia, 287, p.120767_1 - 120767_16, 2025/04

 被引用回数:0 パーセンタイル:0.00(Materials Science, Multidisciplinary)

Incorporating solute hydrogen into Fe-Cr-Ni-based austenitic stainless steels enhances both strength and ductility, providing a promising solution to hydrogen embrittlement by causing solid-solution strengthening and assisting deformation twinning. However, its impacts on the relevant lattice defects evolution (${it i.e.}$, dislocations, stacking faults, and twins) during deformation remains unclear. This study compared the tensile deformation behavior in an Fe-24Cr-19Ni (mass%) austenitic steel with 7600 atom ppm hydrogen-charged (H-charged) and without hydrogen-charged (non-charged) using ${it in situ}$ neutron diffraction. Hydrogen effects on the lattice expansion, solid-solution strengthening, stacking fault probability, stacking fault energy, dislocation density, and strain/stress for twin evolution were quantitatively evaluated to link them with the macroscale mechanical properties. The H-charged sample showed improvements in yield stress, flow stress, and uniform elongation, consistent with earlier findings. However, solute hydrogen exhibited minimal influences on the evolution of dislocation and stacking fault. This fact contradicts the previous reports on hydrogen-enhanced dislocation and stacking fault evolutions, the latter of which can be responsible for the enhancement of twinning. The strain for twin evolution was smaller in the H-charged sample compared to the non-charged one. Nevertheless, when evaluated as the onset stress for twin evolution, there was minimal change between the two samples. These findings suggest that the increase in flow stress due to the solid-solution strengthening by hydrogen is a root cause of accelerated deformation twinning at a smaller strain, leading to an enhanced work-hardening rate and improved uniform elongation.

論文

In situ neutron diffraction study of strain evolution and load partitioning during elevated temperature tensile test in HIP-Treated electron beam powder bed fusion manufactured Ti-6Al-4V

Pandian, K.*; Neikter, M.*; Ekh, M.*; Harjo, S.; 川崎 卓郎; Woracek, R.*; Hansson, T.*; Pederson, R.*

JOM, 77(4), p.1803 - 1815, 2025/04

 被引用回数:0 パーセンタイル:0.00(Materials Science, Multidisciplinary)

To produce dense Ti-6Al-4V components, electron beam powder bed fusion is typically followed by post-heat treatment like hot isostatic pressing (HIP). Standard HIP at 920$$^{circ}$$C/100 MPa for 2 h coarsens the microstructure and reduces yield strength, while low-temp HIP at 800$$^{circ}$$C/200 MPa for 2 h limits coarsening and retains strength comparable to as-built material. A coarser microstructure negatively affects tensile properties. Tensile tests at various temperatures suggest that thermally activated slip systems may influence elongation, requiring further study. In situ neutron time-of-flight diffraction during tensile loading enables analysis of strain evolution and slip plane activity. A two-phase elastic-plastic self-consistent model was used to compare with experiments. Results show basal slip {0002} activated at 20$$^{circ}$$C, pyramidal slip {10-11} at 350$$^{circ}$$C, and $$beta$$ phase carrying higher stress than $$alpha$$ in the plastic regime.

論文

Structural behaviors of lead zirconate titanate-based ferroelectric ceramics during pyroelectric-power generation cycles

川崎 卓郎; 福田 竜生; 山中 暁*; 村山 一郎*; 加藤 孝典*; 馬場 将亮*; 橋本 英樹*; Harjo, S.; 相澤 一也; 田中 裕久*; et al.

Journal of Applied Physics, 137(9), p.094101_1 - 094101_7, 2025/03

 被引用回数:0 パーセンタイル:0.00(Physics, Applied)

Energy harvesting from waste heat can improve energy efficiency in society. This research investigated the structural behaviors of lead zirconate titanate-based ferroelectric ceramics using operando neutron diffraction measurements under the conditions of two energy-harvesting cycles that involve consideration of the temperature changes of automobile exhaust gas for achieving good harvesting efficiencies. Input and output electrical energies and neutron diffraction data were simultaneously collected. The obtained time-resolved neutron-diffraction intensity data indicate that the applied electric fields and temperature changes induced 90$$^{circ}$$ domain rotation and lattice strain. These structural changes and their variations depending on cycle conditions, such as temperature changes, applied electric fields, and circuit switching, provide insight into the origins of the differences in the behaviors of electrical input/output energies in the cycles.

論文

A Lightweight shape-memory alloy with superior temperature-fluctuation resistance

Song, Y.*; Xu, S.*; 佐藤 駿介*; Lee, I.*; Xu, X.*; 大森 俊洋*; 長迫 実*; 川崎 卓郎; 鬼柳 亮嗣; Harjo, S.; et al.

Nature, 638, p.965 - 971, 2025/02

 被引用回数:2 パーセンタイル:88.78(Multidisciplinary Sciences)

In advanced applications like aerospace and space exploration, materials must balance lightness, functionality, and extreme thermal fluctuation resistance. Shape-memory alloys show promise with strength, toughness, and substantial strain recovery due to superelasticity, but maintaining low mass and effective operation at cryogenic temperatures is challenging. We hereby introduce a novel shape-memory alloy that adheres to these stringent criteria. Predominantly composed of Ti and Al with a chemical composition of Ti$$_{75.25}$$Al$$_{20}$$Cr$$_{4.75}$$, this alloy 25 is characterized by a low density (4.36$$times$$10$$^{3}$$ kg/m$$^{3}$$) and a high specific strength (185$$times$$10$$^{3}$$ Pa$$cdot$$m$$^{3}$$/kg) at room temperature, while exhibiting excellent superelasticity. The superelasticity, owing to a reversible stress-induced phase transformation from an ordered body-centered cubic parent phase to an ordered orthorhombic martensite, allows for a recoverable strain exceeding 7%. Remarkably, this functionality persists across a broad range of temperatures, from deep cryogenic 4.2 K to above room temperature, arising from an unconventional temperature dependence of transformation stresses. Below a certain threshold during cooling, the critical transformation stress inversely correlates with temperature. We interpret this behavior from the perspective of a temperature-dependent anomalous lattice instability of the parent phase. This alloy holds potential in everyday appliances requiring flexible strain accommodations, as well as components designed for extreme environmental conditions such as deep space and liquefied gases.

論文

Role of retained austenite and deformation-induced martensite in 0.15C-5Mn steel monitored by ${it in situ}$ neutron diffraction measurement during tensile deformation

山下 享介*; 諸岡 聡; Gong, W.; 川崎 卓郎; Harjo, S.; 北條 智彦*; 興津 貴隆*; 藤井 英俊*

ISIJ International, 64(14), p.2051 - 2060, 2024/12

An Fe-0.15C-5Mn-0.5Si-0.05Nb steel annealed at 660$$^{circ}$$C and 685$$^{circ}$$C showed L$"u$ders deformation followed by high work hardening, with variations in L$"u$ders strain and hardening behavior. ${it In situ}$ neutron diffraction during tensile tests analyzed phase stresses, strength contributions, and austenite orientation. Deformation-induced martensite contributed $$sim$$1000 MPa to strength near tensile failure, while austenite mainly enhanced ductility via transformation-induced plasticity. Austenite transformed to martensite during L$"u$ders deformation regardless of orientation, though 311-oriented grains tended to remain along the tensile direction.

論文

Strain analysis by neutron diffraction on Nb$$_{3}$$Sn strands in ITER central solenoid conductors of short and long twist pitch

諏訪 友音*; 礒野 高明*; Harjo, S.; 川崎 卓郎; 相澤 一也

Superconductor Science and Technology, 38(1), p.015008_1 - 015008_8, 2024/12

 被引用回数:0 パーセンタイル:0.00(Physics, Applied)

The ITER central solenoid (CS) conductors are composed of Nb$$_{3}$$Sn superconducting cables and stainless steel jackets. Approximately 60,000 electromagnetic loading cycles will be applied to the Nb$$_{3}$$Sn strands in the CS conductor over the course of ITER tokamak operation, and the CS conductor is required to maintain the current sharing temperature ($$T_{rm cs}$$) for these electromagnetic loading cycles. However, in CS conductor prototypes, degradation of $$T_{rm cs}$$ was observed after electromagnetic loading cycles. Visual inspections of the tested CS conductors revealed large bending and buckling of the Nb$$_{3}$$Sn strands. These strand deformations were considered to be the cause of $$T_{rm cs}$$ degradation because even a small amount of strain markedly affects the critical current of Nb$$_{3}$$Sn strands. To prevent the strands from bending and buckling, the twist pitch of the cable was shortened to improve stiffness. The stiffer cables did prevent $$T_{rm cs}$$ from degrading after electromagnetic loading cycles owing to the shortened twist pitch of the conductors, but a slight increase of $$T_{rm cs}$$ was observed. Visual inspections revealed no significant bent or buckled strands, but small deformations cannot be investigated visually. Thus, internal strain was measured by neutron diffraction and the internal strain states of the prototype CS conductors having long twist pitches and the improved short-twist-pitch (STP) CS conductors were evaluated. The results indicated that, after electromagnetic loading cycles, bending of the strands in the STP CS conductor was limited and compressive strain was reduced. Therefore, we determined that this STP is not only effective to prevent degradation caused by bent strands but it also increases $$T_{rm cs}$$ by reducing compressive strain.

論文

Deformation behavior of ultrafine-grained TRIP steel observed by neutron diffraction

Harjo, S.; Mao, W.*; Gong, W.; 川崎 卓郎

Proceedings of the 7th International Symposium on Steel Science (ISSS 2024), p.205 - 208, 2024/11

This study aimed to elucidate the effect of grain size on the deformation behavior of TRIP steel. We prepared metastable austenitic Fe-24Ni-0.3C steel samples with average grain sizes of 35 ${textmu}$m (coarse grain: CG) and 0.5 ${textmu}$m (ultrafine-grain: UFG) for in situ neutron diffraction studies during tensile deformation at room temperature. Our observations revealed increases in dislocation density in both samples prior to DIMT, indicating that plastic deformation precedes DIMT regardless of grain size. In the UFG sample, a significant rise in dislocation density occurred just around the yielding point with minimal increases in macroscopic plastic strain. Additionally, the dislocations exhibited strong dipole arrangements.

論文

${it In situ}$ neutron diffraction study to elucidate hydrogen effect on the deformation mechanism in Type 310S austenitic stainless steel

伊東 達矢; 小川 祐平*; Gong, W.; Mao, W.*; 川崎 卓郎; 岡田 和歩*; 柴田 曉伸*; Harjo, S.

Proceedings of the 7th International Symposium on Steel Science (ISSS 2024), p.237 - 240, 2024/11

Hydrogen embrittlement has long been an obstacle to the development of safe infrastructure. However, in contrast to hydrogen's embrittling effect, recent research has revealed that the addition of hydrogen improves both the strength and uniform elongation of AISI Type 310S austenitic stainless steel. A detailed understanding of how hydrogen affects the deformation mechanism of this steel could pave the way for the development of more advanced materials with superior properties. In the present study, ${it in situ}$ neutron diffraction experiments were conducted on Type 310S steel with and without hydrogen-charged to investigate the effect of hydrogen on the deformation mechanism. In addition to the effect of solid-solution strengthening by hydrogen, the q-value, a parameter representing the proportion of edge and screw dislocations in the accumulated dislocations, was quantitatively evaluated using CMWP analysis on neutron diffraction patterns. The comparison of q-values between the hydrogen-charged and non-charged samples reveals that hydrogen has minimal effect on dislocation character in Type 310S steel.

論文

Martensitic transformation-governed Luders deformation enables large ductility and late-stage strain hardening in ultrafine-grained austenitic stainless steel at low temperatures

Mao, W.*; Gao, S.*; Gong, W.; 川崎 卓郎; 伊東 達矢; Harjo, S.; 辻 伸泰*

Acta Materialia, 278, p.120233_1 - 120233_13, 2024/10

 被引用回数:12 パーセンタイル:87.44(Materials Science, Multidisciplinary)

Using a hybrid method of in situ neutron diffraction and digital image correlation, we found that ultrafine-grained 304 stainless steel exhibits Luders deformation after yielding, in which the deformation behavior changes from a cooperation mechanism involving dislocation slip and martensitic transformation to one primarily governed by martensitic transformation, as the temperature decreases from 295 K to 77 K. Such martensitic transformation-governed Luders deformation delays the activation of plastic deformation in both the austenite parent and martensite product, resulting in delayed strain hardening. This preserves the strain-hardening capability for the later stage of deformation, thereby maintaining a remarkable elongation of 29% while achieving a high tensile strength of 1.87 GPa at 77 K.

論文

Polarized and unpolarized neutron scattering for magnetic materials at the triple-axis spectrometer PONTA in JRR-3

中島 多朗*; 齋藤 開*; 小林 尚暉*; 川崎 卓郎; 中村 龍也; 古川 はづき*; 浅井 晋一郎*; 益田 隆嗣*

Journal of the Physical Society of Japan, 93(9), p.091002_1 - 091002_5, 2024/09

 被引用回数:2 パーセンタイル:68.78(Physics, Multidisciplinary)

Neutron scattering is a powerful tool to study magnetic structures and cross-correlated phenomena originated from symmetry of the magnetic structures in matter. Among a number of neutron scattering techniques, polarized neutron scattering is quite sensitive to the orientations of the magnetic moments, which are essential to understand microscopic mechanisms of the spin-driven emergent phenomena. Here, we present POlarized Neutron Triple-Axis spectrometer PONTA in the Japan Research Reactor 3 (JRR-3), and show the present capabilities of polarized and unpolarized neutron scattering by introducing recent results from the instrument.

論文

Internal strain measurement by neutron diffraction under transverse compressive stress for Nb$$_{3}$$Sn wires with and without Cu-Nb reinforcement

中本 美緒*; 菅野 未知央*; 荻津 透*; 杉本 昌弘*; 谷口 諒*; 廣瀬 清慈*; 川崎 卓郎; Gong, W.; Harjo, S.; 淡路 智*; et al.

IEEE Transactions on Applied Superconductivity, 34(5), p.8400806_1 - 8400806_6, 2024/08

 被引用回数:0 パーセンタイル:0.00(Engineering, Electrical & Electronic)

For an accelerator magnet, a certain mechanical strength is required to sustain against a transverse compression stress due to Lorentz force. A bronze-route Nb$$_{3}$$Sn wire with Cu-Nb reinforcement was developed by Tohoku University and Furukawa Electric to enhance the strength against axial tension. The Cu-Nb reinforcement wire also exhibited some indication of strength improvement against transverse compression; however, the details of a reinforcement mechanism for the transverse compression stress have not been clarified. In this study, the internal strains of Nb$$_{3}$$Sn bronze-route wires with and without the Cu-Nb reinforcement under transverse compression stress were evaluated by neutron diffraction at BL19 (TAKUMI) in J-PARC. The samples were attached to jig with solder only at the ends and compression was applied at the center of the samples with 30-mm anvil with 5-mm wide and 8- to 15-mm high beam. Since a critical current, Ic of a superconducting wire depends on the three-dimensional strain, internal strain of Nb$$_{3}$$Sn along the axial and two orthogonal radial directions were evaluated at room temperature (RT). In the different setup, Ic measurements of the wires under transverse compression stresses were also performed at 4.2 K and 14.5 T. Using 3-mm wide anvil, the transverse compression was applied at 4.2 K or RT. The neutron diffraction results indicated no significant differences in the internal strains of Nb$$_{3}$$Sn under transverse compression between the samples with and without Cu-Nb reinforcement, while the Ic measurements showed potential increase in the irreversible stress ($$sigma$$$$_{irr}$$) for Cu-Nb reinforced wires. The reason for this discrepancy was discussed based on the difference in the experimental setups for each measurement.

論文

マルチモーダル化したマグネシウム合金の変形中の構成相・組織の挙動

Harjo, S.; Gong, W.; 相澤 一也; 山崎 倫昭*; 川崎 卓郎

日本材料学会第58回X線材料強度に関するシンポジウム講演論文集, p.58 - 60, 2024/07

The experiment and analysis procedures for a sample exhibiting multimodal structures were outlined. The sample, a Mg$$_{97}$$Zn$$_1$$Y$$_2$$ alloy, initially comprised two phases: the HCP $$alpha$$ matrix ($$alpha$$Mg) and the long-period stacking ordered phase (LPSO), constituting approximately 25% of the volume. Through hot extrusion at 623 K with an extrusion ratio (R) of 5.0, the alloy was rendered multimodal. Specifically, at an R value of 5.0, dynamic recrystallization occurred partially within the $$alpha$$Mg phase, resulting in a bimodal microstructure. This microstructure consisted of a deformed $$alpha$$Mg component and a recrystallized $$alpha$$Mg component. An analysis employing Electron Backscatter Diffraction (EBSD) data facilitated multimodal characterization, enabling successful determination of stresses within the individual $$alpha$$Mg components, as well as the LPSO phase stress.

論文

マルチピークを用いた応力評価

Harjo, S.; Gong, W.; 川崎 卓郎

日本材料学会第58回X線材料強度に関するシンポジウム講演論文集, p.51 - 54, 2024/07

In-situ neutron diffraction was used to study tensile deformation in an extruded AZ31 alloy. The aim was to validate existing methods and develop new ones for stress evaluation in magnesium alloys. Results showed varied increases in lattice strains among grains, posing challenges for conventional procedures. A new method, considering grain volume fraction and multiple orientations, proved highly accurate. When simultaneous hk.l peaks weren't available, the 12.1 peak was recommended for stress evaluation, showing a linear relationship with applied stress throughout deformation.

論文

Microscopic insights of the extraordinary work-hardening due to phase transformation

Ma, Y.*; Naeem, M.*; Zhu, L.*; He, H.*; Sun, X.*; Yang, Z.*; He, F.*; Harjo, S.; 川崎 卓郎; Wang, X.-L.*

Acta Materialia, 270, p.119822_1 - 119822_13, 2024/05

 被引用回数:9 パーセンタイル:95.42(Materials Science, Multidisciplinary)

We report an in situ neutron diffraction study of 316 L that reveals an extraordinary work-hardening rate (WHR) of $$sim$$7 GPa at 15 K. Detailed analyses show that the major contribution to the excellent strength and ductility comes from the transformation-induced plasticity (TRIP) effect, introduced by the austenite-to-martensite ($$gamma$$-to-$$alpha$$') phase transition. A dramatic increase in the WHR is observed along with the transformation; the WHR declined when the austenite phase is exhausted. During plastic deformation, the volume-fraction weighted phase stress and stress contribution from the $$alpha$$'-martensite increase significantly. The neutron diffraction data further suggest that the $$gamma$$-to-$$alpha$$' phase transformation was mediated by the $$varepsilon$$-martensite, as evidenced by the concurrent decline of the $$varepsilon$$ phase with the $$gamma$$ phase.

論文

In-situ neutron diffraction study of serration-involved ultra-cryogenic deformation behavior at 15 K

Kim, Y. S.*; Chae, H.*; Lee, D.-Y.*; Han, J. H.*; Hong, S.-K.*; Na, Y. S.*; Harjo, S.; 川崎 卓郎; Woo, W.*; Lee, S.-Y.*

Materials Science & Engineering A, 899, p.146453_1 - 146453_7, 2024/05

 被引用回数:4 パーセンタイル:63.37(Nanoscience & Nanotechnology)

This work focused on the mechanical properties and serration-involved deformation behavior of advanced alloys at 15 K. Evolution of stacking faults and $$varepsilon$$-martensite improved the mechanical performance of CoCrNi alloys, and significant strain-induced martensite transformation of DED-SS316L led to superior strength and strain hardening. A magnitude in stress drop was governed by dislocation density, phase type, and lattice defects, irrespective of processing method. FCC {200} notably was influenced recovery behavior after stress drop, and the contribution of strain energy density by serration on tensile toughness was the greatest for HR-CoCrNi.

論文

Mechanical stability of retained austenite and texture evolution in additively manufactured stainless steel

Chae, H.*; Huang, E.-W.*; Jain, J.*; Lee, D.-H.*; Harjo, S.; 川崎 卓郎; Lee, S. Y.*

Metals and Materials International, 30(5), p.1321 - 1330, 2024/05

 被引用回数:4 パーセンタイル:46.68(Materials Science, Multidisciplinary)

In situ neutron diffraction during tensile deformation was performed for the stainless steels prepared by the additive manufacturing (AM) processes with two strategies: vertically built and horizontally built. The AM steels were further aged without solid solution treatment. As the results, the retained austenite was found to be more stable because the chemical composition became homogeneous by aging, and the onset of deformation induced martensitic transformation was delayed.

論文

Recrystallization of bulk nanostructured magnesium alloy AZ31 after severe plastic deformation; An in situ diffraction study

Liss, K.-D.*; Han, J.-K.*; Blankenburg, M.*; Lienert, U.*; Harjo, S.; 川崎 卓郎; 徐 平光; 行武 栄太郎*; Kawasaki, M.*

Journal of Materials Science, 59(14), p.5831 - 5853, 2024/04

 被引用回数:4 パーセンタイル:69.57(Materials Science, Multidisciplinary)

The magnesium alloy AZ31, which has undergone high-pressure torsion processing, was subjected to in situ annealing micro-beam synchrotron high-energy X-ray diffraction and compared to the as-received rolled sheet material that was investigated through in situ neutron diffraction. While the latter only exhibits thermal expansion and minor recovery, the nanostructured specimen displays a complex evolution, including recovery, strong recrystallization, phase transformations, and various regimes of grain growth. Nanometer-scale grain sizes, determined using Williamson-Hall analysis, exhibit seamless growth, aligning with the transition to larger grains, as assessed through the occupancy of single grain reflections on the diffraction rings. The study uncovers strain anomalies resulting from thermal expansion, segregation of Al atoms, and the kinetics of vacancy creation and annihilation. Notably, a substantial number of excess vacancies were generated through high-pressure torsion, and maintained for driving the recrystallization and forming highly activated volumes for diffusion and phase precipitation during heating. The unsystematic scatter observed in the Williamson-Hall plot indicates high dislocation densities following severe plastic deformation, which significantly decreases during recrystallization. Subsequently, dislocations reappear during grain growth, likely in response to torque gradients in larger grains. It is worth noting that the characteristics of unsystematic scatter differ for dislocations created at high and low temperatures, underscoring the strong temperature dependence of slip system activation.

論文

${it In situ}$ neutron diffraction revealing the achievement of excellent combination of strength and ductility in metastable austenitic steel by grain refinement

Mao, W.; Gong, W.; Harjo, S.; 諸岡 聡; Gao, S.*; 川崎 卓郎; 辻 伸泰*

Journal of Materials Science & Technology, 176, p.69 - 82, 2024/03

 被引用回数:6 パーセンタイル:55.06(Materials Science, Multidisciplinary)

Fe-24Ni-0.3C(wt.%)準安定オーステナイト鋼の降伏応力は、平均結晶粒径が35$$mu$$m(粗粒[CG])から0.5$$mu$$m(超微細粒[UFG])に減少すると3.5倍(158$$rightarrow$$551MPa)に増加したが、引張伸びは大きく維持された(0.87$$rightarrow$$0.82)。結晶粒径が力学特性と変形機構に及ぼす影響を定量的に明らかにするため、室温での引張変形中にCGとUFG Fe-24Ni-0.3C鋼のその場中性子回折測定を行った。CGとUFG試料における塑性変形の初期段階は転位すべりによって支配され、変形後期には変形誘起マルテンサイト変態(DIMT)も生じた。結晶粒の微細化により、DIMTの開始応力が大きく増加し、ひずみに関するDIMTの速度が抑制されることがわかった。結果として、(i)結晶粒微細化によりオー ステナイトが安定化し、DIMTに対して最も安定な結晶粒である$$<$$111$$>$$//LD(LD:負荷方向)オーステナイト粒でのDIMTの開始が大幅に遅れた。その結果、UFG試験片の$$<$$111$$>$$//LDオーステナイト粒のほとんどはマルテンサイトに変態しなかった。(ii)結晶粒の微細化は、マルテンサイト変態の自己促進効果も抑制した。それにもかかわらず、UFG試験片の変態速度が低いDIMTは、CG試験片のより応力を増加させるのに効率がよく、変形中に均一な変形を維持するのに適していた。以上の現象は、UFG準安定オーステナイト鋼の優れた強度と延性の両立に相互に寄与している。

論文

Cryogenic deformation behavior of a dual-phase Mg-Li alloy investigated by in-situ neutron diffraction

Gong, W.; Gholizadeh, R.*; 川崎 卓郎; 相澤 一也; Harjo, S.

Magnesium Technology 2024, p.89 - 90, 2024/03

Mg and its alloys generally exist as a single hcp crystal structure at room temperature. It is widely recognized that the application of Mg alloys is hindered by their limited formability at room temperature, primarily attributable to the scarcity of readily activated deformation modes within the hcp phase. The addition of Li in Mg alloy can stable the bcc phase at room temperature, and these dual-phase (hcp+bcc) Mg-Li alloys exhibit excellent formability. The Li-enriched bcc phase has been frequently considered as the origin for improving formability. However, these Mg-Li alloys show poor work-hardening ability and the resultant low strength at room temperature. Considering that the dislocation recovery can be suppressed by decreasing the deformation temperature and the activity of deformation mode may be changed with temperature, we investigated the deformation behavior of a commercial LZ91 magnesium alloy at cryogenic temperatures using in-situ neutron diffraction.

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