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Journal Articles

${it In situ}$ neutron diffraction revealing the achievement of excellent combination of strength and ductility in metastable austenitic steel by grain refinement

Mao, W.; Gong, W.; Harjo, S.; Morooka, Satoshi; Gao, S.*; Kawasaki, Takuro; Tsuji, Nobuhiro*

Journal of Materials Science & Technology, 176, p.69 - 82, 2024/03

The yield stress of Fe-24Ni-0.3C (wt.%) metastable austenitic steel increased 3.5 times (158 $$rightarrow$$ 551 MPa) when the average grain size decreased from 35 $$mu$$m (coarse-grained [CG]) to 0.5 $$mu$$m (ultrafine-grained [UFG]), whereas the tensile elongation was kept large (0.87 $$rightarrow$$ 0.82). ${it In situ}$ neutron diffraction measurements of the CG and UFG Fe-24Ni-0.3C steels were performed during tensile deformation at room temperature to quantitatively elucidate the influence of grain size on the mechanical properties and deformation mechanisms. The initial stages of plastic deformation in the CG and UFG samples were dominated by dislocation slip, with deformation-induced martensitic transformation (DIMT) also occurring in the later stage of deformation. Results show that grain refinement increases the initiation stress of DIMT largely and suppresses the rate of DIMT concerning the strain, which is attributed to the following effects. (i) Grain refinement increased the stabilization of austenite and considerably delayed the initiation of DIMT in the $$<$$111$$>$$//LD (LD: loading direction) austenite grains, which were the most stable grains for DIMT. As a result, most of the $$<$$111$$>$$//LD austenite grains in the UFG specimens failed to transform into martensite. (ii) Grain refinement also suppressed the autocatalytic effect of the martensitic transformation. Nevertheless, the DIMT with the low transformation rate in the UFG specimen was more efficient in increasing the flow stress and more appropriate to maintain uniform deformation than that in the CG specimen during deformation. The above phenomena mutually contributed to the excellent combination of strength and ductility of the UFG metastable austenitic steel.

Journal Articles

Martensitic transformation behavior of Fe-Ni-C alloys monitored by ${it in-situ}$ neutron diffraction during cryogenic cooling

Yamashita, Takayuki*; Harjo, S.; Kawasaki, Takuro; Morooka, Satoshi; Gong, W.; Fujii, Hidetoshi*; Tomota, Yo*

ISIJ International, 64(2), p.192 - 201, 2024/01

Journal Articles

Probing deformation behavior of a refractory high-entropy alloy using ${it in situ}$ neutron diffraction

Zhou, Y.*; Song, W.*; Zhang, F.*; Wu, Y.*; Lei, Z.*; Jiao, M.*; Zhang, X.*; Dong, J.*; Zhang, Y.*; Yang, M.*; et al.

Journal of Alloys and Compounds, 971, p.172635_1 - 172635_7, 2024/01

Journal Articles

Recrystallization of bulk nanostructured magnesium alloy AZ31 after severe plastic deformation; An in situ diffraction study

Liss, K.-D.*; Han, J.-K.*; Blankenburg, M.*; Lienert, U.*; Harjo, S.; Kawasaki, Takuro; Xu, P. G.; Yukutake, Eitaro*; Kawasaki, M.*

Journal of Materials Science, 23 Pages, 2024/00

Journal Articles

Stress evaluation method by neutron diffraction for HCP-structured magnesium alloy

Harjo, S.; Gong, W.; Kawasaki, Takuro

Quantum Beam Science (Internet), 7(4), p.32_1 - 32_13, 2023/12

Journal Articles

Effects of dislocation arrangement and character on the work hardening of lath martensitic steels

Dannoshita, Hiroyuki*; Hasegawa, Hiroshi*; Higuchi, Sho*; Matsuda, Hiroshi*; Gong, W.; Kawasaki, Takuro; Harjo, S.; Umezawa, Osamu*

Scripta Materialia, 236, p.115648_1 - 115648_5, 2023/11

 Times Cited Count:0 Percentile:0

Journal Articles

Measurement of mechanical behavior of $$^{11}$$B-enriched MgB$$_{2}$$ wire using a pulsed neutron source

Machiya, Shutaro*; Osamura, Kozo*; Hishinuma, Yoshimitsu*; Taniguchi, Hiroyasu*; Harjo, S.; Kawasaki, Takuro

Quantum Beam Science (Internet), 7(4), p.34_1 - 34_17, 2023/10

Journal Articles

Quantitatively evaluating the huge L$"u$ders band deformation in an ultrafine grain stainless steel by combining ${it in situ}$ neutron diffraction and digital image correlation analysis

Mao, W.; Gao, S.*; Gong, W.; Harjo, S.; Kawasaki, Takuro; Tsuji, Nobuhiro*

Scripta Materialia, 235, p.115642_1 - 115642_6, 2023/10

 Times Cited Count:0 Percentile:0

In the present study, a hybrid ${it in situ}$ neutron diffraction and digital image correlation measurement was performed on tensile deformation of an ultrafine grain (UFG) stainless steel exhibiting a huge L$"u$ders band deformation to evaluate the individual contribution of the austenite matrix and the deformation-induced martensite to the strain hardening during the propagation of the band. Quantitative analysis revealed that the strain hardening of the austenite matrix was insufficient to maintain a uniform deformation when the flow stress was greatly enhanced by the UFG structure. The strain hardening required for the L$"u$ders band to propagate was mostly provided by the formation of martensite and the high internal stress within it.

Journal Articles

Strengthening of $$alpha$$Mg and long-period stacking ordered phases in a Mg-Zn-Y alloy by hot-extrusion with low extrusion ratio

Harjo, S.; Gong, W.; Aizawa, Kazuya; Kawasaki, Takuro; Yamasaki, Michiaki*

Acta Materialia, 255, p.119029_1 - 119029_12, 2023/08

 Times Cited Count:1 Percentile:94.84(Materials Science, Multidisciplinary)

Journal Articles

${it In situ}$ neutron diffraction study on the deformation behavior of the plastic inorganic semiconductor Ag$$_{2}$$S

Wang, Y.*; Gong, W.; Kawasaki, Takuro; Harjo, S.; Zhang, K.*; Zhang, Z. D.*; Li, B.*

Applied Physics Letters, 123(1), p.011903_1 - 011903_6, 2023/07

 Times Cited Count:0 Percentile:59.51

Journal Articles

Lattice parameters of austenite and martensite during transformation for Fe-18Ni alloy investigated through ${it in situ}$ neutron diffraction

Gong, W.; Harjo, S.; Tomota, Yo*; Morooka, Satoshi; Kawasaki, Takuro; Shibata, Akinobu*; Tsuji, Nobuhiro*

Acta Materialia, 250, p.118860_1 - 118860_16, 2023/05

 Times Cited Count:0 Percentile:77.63(Materials Science, Multidisciplinary)

Journal Articles

Competitive strengthening between dislocation slip and twinning in cast-wrought and additively manufactured CrCoNi medium entropy alloys

Woo, W.*; Kim, Y. S.*; Chae, H. B.*; Lee, S. Y.*; Jeong, J. S.*; Lee, C. M.*; Won, J. W.*; Na, Y. S.*; Kawasaki, Takuro; Harjo, S.; et al.

Acta Materialia, 246, p.118699_1 - 118699_13, 2023/03

 Times Cited Count:4 Percentile:97.51(Materials Science, Multidisciplinary)

Journal Articles

Neutron stress measurement of W/Ti composite in cryogenic temperatures using time-of-flight method

Nishida, Masayuki*; Harjo, S.; Kawasaki, Takuro; Yamashita, Takayuki*; Gong, W.

Quantum Beam Science (Internet), 7(1), p.8_1 - 8_15, 2023/03

Journal Articles

Compressive deformation behavior of AZ31 alloy at 21K; An ${it In situ}$ neutron diffraction study

Gong, W.; Kawasaki, Takuro; Zheng, R.*; Mayama, Tsuyoshi*; Sun, B.*; Aizawa, Kazuya; Harjo, S.; Tsuji, Nobuhiro*

Scripta Materialia, 225, p.115161_1 - 115161_5, 2023/03

 Times Cited Count:2 Percentile:48.15(Nanoscience & Nanotechnology)

Journal Articles

Tensile overload-induced texture effects on the fatigue resistance of a CoCrFeMnNi high-entropy alloy

Lam, T.-N.*; Chin, H.-H.*; Zhang, X.*; Feng, R.*; Wang, H.*; Chiang, C.-Y.*; Lee, S. Y.*; Kawasaki, Takuro; Harjo, S.; Liaw, P. K.*; et al.

Acta Materialia, 245, p.118585_1 - 118585_9, 2023/02

 Times Cited Count:2 Percentile:73.49(Materials Science, Multidisciplinary)

Journal Articles

Effect of extrusion ratio in hot-extrusion on kink deformation during compressive deformation in an $$alpha$$Mg/LPSO dual-phase magnesium alloy monitored by ${it in situ}$ neutron diffraction

Harjo, S.; Gong, W.; Aizawa, Kazuya; Kawasaki, Takuro; Yamasaki, Michiaki*; Mayama, Tsuyoshi*; Kawamura, Yoshihito*

Materials Transactions, 64(4), p.766 - 773, 2023/02

 Times Cited Count:1 Percentile:87.31(Materials Science, Multidisciplinary)

Journal Articles

Stress partitioning between bcc and cementite phases discussed from phase stress and dislocation density in martensite steels

Tsuchida, Noriyuki*; Ueji, Rintaro*; Gong, W.; Kawasaki, Takuro; Harjo, S.

Scripta Materialia, 222, p.115002_1 - 115002_6, 2023/01

 Times Cited Count:4 Percentile:67.13(Nanoscience & Nanotechnology)

Journal Articles

Rearrangement of hydrogen bonds in dehydrated raffinose tetrahydrate; A Time-of-flight neutron diffraction study

Kawasaki, Takuro; Takahashi, Miwako*; Kiyanagi, Ryoji; Ohara, Takashi

Acta Crystallographica Section C; Structural Chemistry (Internet), 78(12), p.743 - 748, 2022/12

 Times Cited Count:0 Percentile:0.01(Chemistry, Multidisciplinary)

Journal Articles

Si-addition contributes to overcoming the strength-ductility trade-off in high-entropy alloys

Wei, D.*; Gong, W.; Tsuru, Tomohito; Lobzenko, I.; Li, X.*; Harjo, S.; Kawasaki, Takuro; Do, H.-S.*; Bae, J. W.*; Wagner, C.*; et al.

International Journal of Plasticity, 159, p.103443_1 - 103443_18, 2022/12

 Times Cited Count:12 Percentile:98.45(Engineering, Mechanical)

Journal Articles

${it In situ}$ observation of twinning and detwinning in AZ31 alloy

Gong, W.; Zheng, R.*; Harjo, S.; Kawasaki, Takuro; Aizawa, Kazuya; Tsuji, Nobuhiro*

Journal of Magnesium and Alloys (Internet), 10(12), p.3418 - 3432, 2022/12

 Times Cited Count:12 Percentile:93.63(Metallurgy & Metallurgical Engineering)

293 (Records 1-20 displayed on this page)