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Journal Articles

New antiferromagnetic order with pressure-induced superconductivity in EuFe$$_2$$As$$_2$$

Ikeda, Shugo*; Tsuchiya, Yu*; Zhang, X.-W.*; Kishimoto, Shunji*; Kikegawa, Takumi*; Yoda, Yoshitaka*; Nakamura, Hiroki; Machida, Masahiko; Glasbrenner, J.*; Kobayashi, Hisao*

Physical Review B, 98(10), p.100502_1 - 100502_6, 2018/09

 Times Cited Count:6 Percentile:25.82(Materials Science, Multidisciplinary)

The interplay between magnetism and superconductivity is one of important subjects to investigate the pairing mechanism in novel superconductors. We have found new coexistence between an antiferromagnetic order in the Fe sublattice and superconductivity of the FeAs-based EuFe$$_2$$As$$_2$$ superconductor in the pressure range from 2.4 to 3.0 GPa by $$^{57}$$Fe nuclear forward scattering (NFS) using a single crystal sample. The magnetic state in the Fe sublattice changes to a new antiferromagnetic one with superconductivity from a stripe-type antiferromagnetic one observed in normal conducting state at 2.7 GPa. Below the superconducting transition temperature, the temperature dependence of $$^{57}$$Fe NFS spectra reveals that the new antiferromagnetic order develops with the superconductivity. This non-trivial coupling of two ordered states in EuFe$$_2$$As$$_2$$ under pressure demonstrates a new and intriguing relationship between magnetism and superconductivity in Fe-based superconductors.

Journal Articles

Construction of a magnetic bottle spectrometer and its application to pulse duration measurement of X-ray laser using a pump-probe method

Namba, Shinichi*; Hasegawa, Noboru; Kishimoto, Maki; Nishikino, Masaharu; Ishino, Masahiko; Kawachi, Tetsuya

AIP Advances (Internet), 5(11), p.117101_1 - 117101_10, 2015/11

 Times Cited Count:3 Percentile:13.89(Nanoscience & Nanotechnology)

To characterize the temporal evolution of ultrashort X-ray pulses emitted by laser plasmas using a pump-probe method, a magnetic bottle time-of-flight electron spectrometer is constructed. The design is determined by numerical calculations of a mirror magnetic field and of the electron trajectory in a flight tube. The performance of the spectrometer is characterized by measuring the electron spectra of xenon atoms irradiated with a laser-driven plasma X-ray pulse. In addition, as a preliminary experiment, two-color above-threshold ionization (ATI) is conducted, in which xenon atoms are simultaneously irradiated with an X-ray laser pump and an IR laser probe. The correlation in the intensity of the Auger sideband spectra and in the time delay of the two laser pulses yields an X-ray pulse width of 5.7 ps, in good agreement with the value obtained using an X-ray streak camera.

Journal Articles

Effects of ultra-intense laser driven proton beam on the hydriding property of palladium

Abe, Hiroshi; Orimo, Satoshi; Kishimoto, Masahiko*; Aone, Shigeo*; Uchida, Hirohisa*; Daido, Hiroyuki; Oshima, Takeshi

Nuclear Instruments and Methods in Physics Research B, 307, p.218 - 220, 2013/07

 Times Cited Count:1 Percentile:11.54(Instruments & Instrumentation)

We investigated the structure changes of a hydrogen storage alloy by ion irradiations, and its absorption property in order to obtain basic data and to elucidate relevant mechanisms of hydrogen absorption by the influence of the irradiation. In previous studies, the induction of vacancies in a hydrogen absorption alloy was found to be effective to increase in the hydrogen absorption rate. As well known, the rate of hydrogen absorption strongly depends upon the surface state of a hydrogen storage alloy because the dissociation of hydrogen molecules or water molecules needs electron change with the surface in the H$$_{2}$$ gas or electrochemical reaction process. In this study, ion irradiations were made at a room temperature using the laser driven proton beam method, at Kansai Photon Science Institute, Japan Atomic Energy Agency. The beam treatment has several unique properties such as short pulse duration, high peak current, low transverse emittance, and wide energy range from KeV to MeV. The irradiation was used to modify the alloy surface using this equipment. From obtained results, the initial hydrogen absorption rate was found improved by the laser driven proton beam rather more effectively than a mono-energetic proton beam. Discussion is made on the correlation among proton irradiation (laser driven proton or mono-energetic proton) and the initial hydrogen absorption rate of the alloy. We argue about the usefulness of an energy spread beam.

Journal Articles

Development of single shot soft X-ray contact microscopy system for nano-scale dynamics measurement of living biological specimen

Kishimoto, Maki; Kado, Masataka; Ishino, Masahiko; Tamotsu, Satoshi*; Yasuda, Keiko*; Shinohara, Kunio*

AIP Conference Proceedings 1465, p.43 - 47, 2012/07

 Times Cited Count:9 Percentile:94.44(Physics, Applied)

We have been developing a picosecond single shot soft X-ray contact microscopy system for observing the nanometer-scale inner structure of the living biological specimen in a hydrated condition. The microscopy system consists of an intense IR pump laser system for generating soft X-rays and X-ray microscope chamber. The pump laser system employs OPCPA technique to generate water-window X-rays effectively. The X-ray microscope chamber is composed of a vacuum chamber, a focusing lens, a metal film target, an in-vacuum type sample holder. The soft X-rays from the laser-induced plasma generated by pump laser pulse illuminates bio-specimens on the PMMA photo resist set in the in-vacuum sample holder. The photo resist is developed and the X-ray transmission imageis read out by AFM. We took X-ray images of hydrated Leydig cells from mouse testicle and demonstrated that the developed X-ray microscopy system has a spatial resolution of about 100 nm.

Journal Articles

Observation of organelle by a laser plasma X-ray microscope

Kado, Masataka; Kishimoto, Maki; Ishino, Masahiko; Tamotsu, Satoshi*; Yasuda, Keiko*; Shinohara, Kunio*

AIP Conference Proceedings 1465, p.246 - 250, 2012/07

 Times Cited Count:5 Percentile:84.86(Physics, Applied)

Contact X-ray microscopy has a potential to image wet biological specimens in natural condition. It is very important to identify obtained features in the X-ray images, since X-ray microscopes have potential to image features that have not been visualized yet. We have proposed to compare the X-ray images of the biological specimens with the fluorescence images and to identify the features found in the X-ray images based on the features found in the fluorescence images. Comparing the X-ray images to the fluorescence images of the set biological cells, fine structures of the mitochondria in the X-ray images have been able to be identified.

Journal Articles

Source development and novel applications of laser-driven plasma X-ray lasers in JAEA

Kawachi, Tetsuya; Hasegawa, Noboru; Nishikino, Masaharu; Ishino, Masahiko; Imazono, Takashi; Oba, Toshiyuki; Kaihori, Takeshi; Kishimoto, Maki; Ochi, Yoshihiro; Tanaka, Momoko; et al.

X-Ray Lasers 2010; Springer Proceedings in Physics, Vol.136, p.15 - 24, 2011/12

This paper reviews recent improvement in the source development of laser-driven X-ray lasers and the applications in the research fields of material science, laser processing, X-ray imaging, and radiation damage in biological cells. In the application for material science, we have firstly observed temporal correlation between the domain structures of ferro-electric substance under the Curie temperature. In the laser processing, new X-ray laser interferometer reveals us the nano-scale surface distortion of substance pumped by a femto-second optical pulse. In the X-ray diffraction image, we have taken several static images of micro-structure of samples: now we are trying to extend the objective to nano-scale dynamics using pump and probe method. In the radiation damage of biological cells, we observed double strand break in DNA using X-ray laser exposure; this results are compared with the case using incoherent several KeV X-ray exposure.

Journal Articles

Development of the X-ray interferometer and the method of spatial and temporal synchronization of XRL and optical pulse

Hasegawa, Noboru; Ochi, Yoshihiro; Kawachi, Tetsuya; Terakawa, Kota*; Tomita, Takuro*; Yamamoto, Minoru; Nishikino, Masaharu; Oba, Toshiyuki; Kaihori, Takeshi; Imazono, Takashi; et al.

X-Ray Lasers 2010; Springer Proceedings in Physics, Vol.136, p.353 - 358, 2011/12

The understanding of the dynamics of the initial process is important for the micro processing and welding by the ultra-short laser pulse. The X-ray laser is suitable for probing this initial process because it has short wavelength (Ni-like Ag, 13.9 nm) and short duration (7 ps). For this investigation, the origin of time of the pumping pulse is quite important. In this study, we used the scintillation plate and the plasma gate technique to realize the spatial and temporal synchronization of the pump and probe pulses. For the spatial alignment, a CsI scintillation plate that was set at the sample position was illuminated by both the X-ray laser pulse, and the fluorescence light were detected by the CCD camera. For the temporal synchronization, we set a thin foil at the sample position. We measured the transmission of the X-ray laser while changing a temporal delay of the pumping laser with respect to the time of X-ray laser pulse to obtain the origin of the irradiation time.

Journal Articles

Observation of organelles in Leydig cells by contact soft X-ray microscopy with a laser plasma X-ray source

Kado, Masataka; Ishino, Masahiko; Tamotsu, Satoshi*; Yasuda, Keiko*; Kishimoto, Maki; Nishikino, Masaharu; Kinjo, Yasuhito*; Shinohara, Kunio*

AIP Conference Proceedings 1365, p.391 - 394, 2011/09

 Times Cited Count:7 Percentile:89.93(Microscopy)

Contact X-ray microscopy has achieved a single-shot imaging of wet biological specimens in natural condition and succeeded in imaging live mouse macrophages with hair-like structures, which was not observed before. It is very important to identify obtained features in the X-ray images, since X-ray microscopes have potential to image features that have not been visualized yet. Here, we demonstrate to image the same biological specimens both by confocal laser microscopy and soft X-ray microscopy. Staining biological specimens with well-established techniques makes easy to identify features in the fluorescence images obtained with confocal laser microscope. Comparing the X-ray images of the specimens with the fluorescence images, features found in the fluorescence images could also be identified in the X-ray images. Comparing the X-ray images to the fluorescence images, fine structures of the actin filaments in the X-ray images were identified.

Journal Articles

Development of a specimen holder combined with ultra thin film laser plasma X-ray source for compact contact-type soft X-ray microscope to observe hydrated living biologocal cells

Ishino, Masahiko; Kado, Masataka; Shinohara, Kunio*; Yamamoto, Yoshimasa*; Hirai, Itaru*; Kishimoto, Maki; Nishikino, Masaharu; Hasegawa, Noboru; Tamotsu, Satoshi*; Yasuda, Keiko*; et al.

Proceedings of SPIE Europe Optics + Optoelectronics 2011, Vol.8139, p.81390R_1 - 81390R_8, 2011/09

 Times Cited Count:0 Percentile:0.01(Optics)

Ultra thin gold films are favorable laser plasma targets for a soft X-ray microscopy, because the thin films emit intense soft X-rays at the wavelength of water window region. Using rear side emissions, the distance between the X-ray source and the specimens can be reduced so that the X-ray flux on specimens increases. The microscope system can be designed to be compact when the specimen holder and X-ray source are combined in one piece. The biological specimen holder combined with an ultra thin film target has been developed. This X-ray microscope system needs not any X-ray optics which causes a decrease in X-ray photons for imaging. X-ray images of hydrated living cells have been obtained successfully by use of the newly developed specimen holder. Specimen holder combined with plasma X-ray source will be a key component of a compact soft X-ray microscope using in a laboratory.

Journal Articles

Flash imaging of fine structures of cellular organelles by contact X-ray microscopy with a high intensity laser plasma X-ray source

Kado, Masataka; Ishino, Masahiko; Kishimoto, Maki; Tamotsu, Satoshi*; Yasuda, Keiko*; Kinjo, Yasuhito*; Shinohara, Kunio*

Proceedings of SPIE Europe Optics + Optoelectronics 2011, Vol.8139, p.81390O_1 - 81390O_7, 2011/09

Laser plasma X-ray sources have high intensity and short pulse duration, and are suitable for X-ray microscopy in biology. They make wet live biological specimens possible to be imaged with a single shot X-ray exposure and several works have been done to image them. However there were no reports on the imaging of fine structures of cellular organelles in a live biological cell since higher X-ray intensity is needed for it. We have developed a high intensity laser plasma X-ray source, cooperating it with contact X-ray microscopy, and observed fine structures of cellular organelles in a wet biological cells. Comparing the X-ray images and the fluorescence images of cellular organelles such as actin filaments and mitochondria we have been clearly able to identify organelles in the X-ray images and observed fine structures.

Journal Articles

Ablation of insulators under the action of short pulses of X-ray plasma lasers and free-electron lasers

Inogamov, N. A.*; Anisimov, S. I.*; Petrov, Y. V.*; Khokhlov, V. A.*; Zhakhovskii, V. V.*; Faenov, A. Ya.*; Pikuz, T.; Fortov, V. E.*; Skobelev, I. Y.*; Kato, Yoshiaki*; et al.

Journal of Optical Technology, 78(8), p.473 - 480, 2011/08

 Times Cited Count:6 Percentile:32.94(Optics)

Journal Articles

Spallative ablation of dielectrics by X-ray laser

Inogamov, N. A.*; Zhakhovsky, V. V.*; Faenov, A. Ya.*; Khokhlov, V. A.*; Shepelev, V. V.*; Skobelev, I. Y.*; Kato, Yoshiaki*; Tanaka, Momoko; Pikuz, T. A.*; Kishimoto, Maki; et al.

Applied Physics A, 101(1), p.87 - 96, 2010/10

 Times Cited Count:34 Percentile:76.6(Materials Science, Multidisciplinary)

Journal Articles

Observation of actin filaments in Leydig cells with a contact-type soft X-ray microscope with laser plasma X-ray source

Kado, Masataka; Ishino, Masahiko; Tamotsu, Satoshi*; Yasuda, Keiko*; Kishimoto, Maki; Nishikino, Masaharu; Kinjo, Yasuhito*; Shinohara, Kunio*

Denki Gakkai Rombunshi, C, 130(10), p.1774 - 1778, 2010/10

Actin filaments in Leydig cells from mouse testes have been observed with a contact-type soft X-ray microscope with laser plasma X-ray source. The Leydig cells were fixed with paraformaldehyde, stained with Phalloidin, and observed with a confocal laser microscope prior to the observation with X-ray microscope. Obtained images by both of the confocal laser microscopy and the X-ray microscopy were directly compared and revealed that not only position of actin filaments but also the shapes can be identified each other. The actin filaments in the X-ray images were clearly recognized and their structures were obtained in more detail compared to those in the confocal laser microscope images.

Journal Articles

Interaction of short laser pulses in wavelength range from infrared to X-ray with metals, semiconductors, and dielectrics

Inogamov, N. A.*; Faenov, A. Ya.*; Zhakhovskii, V. V.*; Skobelev, I. Y.*; Khokhlov, V. A.*; Kato, Yoshiaki*; Tanaka, Momoko; Pikuz, T. A.*; Kishimoto, Maki; Ishino, Masahiko; et al.

Contributions to Plasma Physics, 51(4), p.361 - 366, 2010/05

 Times Cited Count:19 Percentile:62.41(Physics, Fluids & Plasmas)

Journal Articles

Observations of the intense soft X-ray emissions from ultra thin Au films irradiated with high contrast laser pulses

Ishino, Masahiko; Kado, Masataka; Nishikino, Masaharu; Shinohara, Kunio*; Tamotsu, Satoshi*; Yasuda, Keiko*; Hasegawa, Noboru; Kishimoto, Maki; Oba, Toshiyuki; Kawachi, Tetsuya

Proceedings of SPIE, Vol.7589, p.75891B_1 - 75891B_8, 2010/02

 Times Cited Count:2 Percentile:72.8(Engineering, Biomedical)

Soft X-ray microscopes operating in the water window are capable of imaging living hydrated biological specimens. Laser produced plasmas are attractive soft X-ray sources, because of their short duration time. Based on the minimum dose calculation, soft X-ray photons more than 10$$^{5}$$ photons/$$mu$$m$$^{2}$$ at the sample surface are needed to acquire an image of the biological specimens with spatial resolution up to 100 nm. The observations of soft X-ray emissions from laser produced plasmas using ultra thin film targets have been carried out. Au thin films were irradiated by a high contrast Nd:glass laser pulses. The spectral properties of emitted soft X-rays were monitored by an X-ray spectrograph from the rear side with respect to the surface of laser irradiation. The observed emission intensities had an obvious dependence on the film thickness, and the most intense emissions were obtained at the thickness of 28 nm. The experimental results have suggested that the most of the laser energy irradiated is absorbed by the film target, and it is resulted an efficient energy deposition from laser to X-rays.

Journal Articles

Low-threshold ablation of dielectrics irradiated by picosecond soft X-ray laser pulses

Faenov, A. Y.; Inogamov, N. A.*; Zhakhovskii, V. V.*; Khokhlov, V. A.*; Nishihara, Katsunobu*; Kato, Yoshiaki*; Tanaka, Momoko; Pikuz, T. A.*; Kishimoto, Maki; Ishino, Masahiko; et al.

Applied Physics Letters, 94(23), p.231107_1 - 231107_3, 2009/06

 Times Cited Count:44 Percentile:82.04(Physics, Applied)

Journal Articles

Demonstration of a fully spatial coherent X-ray laser at 13.9 nm

Nishikino, Masaharu; Tanaka, Momoko; Ochi, Yoshihiro; Kishimoto, Maki; Ishino, Masahiko; Hasegawa, Noboru; Kado, Masataka; Sukegawa, Kota*; Kawachi, Tetsuya; Nagashima, Keisuke

IEEE Journal of Selected Topics in Quantum Electronics, 10(6), p.1382 - 1387, 2004/11

 Times Cited Count:9 Percentile:45.8(Engineering, Electrical & Electronic)

no abstracts in English

Oral presentation

Recent progress in X-ray laser research in JAEA

Kawachi, Tetsuya; Kishimoto, Maki; Kado, Masataka; Tanaka, Momoko; Hasegawa, Noboru; Ochi, Yoshihiro; Nishikino, Masaharu; Ishino, Masahiko; Imazono, Takashi; Kunieda, Yuichi; et al.

no journal, , 

Recent progress in X-ray laser research in Japan Atomic Energy Agency is reviewed. Using the nickel-like silver soft X-ray laser at the wavelength of 13.9 nm, the application experiments have been conducted in the research fields such as material science, high-density plasma diagnostics, XRL ablation, XRL imaging using single-shot holography and atomic physics. The repetition rate of the XRL beam has been improved from each 10-20 minutes to 0.1 Hz by using new driver laser system with Nd: glass zigzag slab amplifier, and we are now constructing new beam line for the pump-probe measurement of the surface phase-transition by the method of X-ray laser interferometer. In the research activity on the extension of the wavelength region of the X-ray lasers, firstly, the demonstration of novel coherent X-ray generation by "flying mirror" technique is reported. The second is theoretical investigation of the resonance photo-pumping scheme toward water-window region.

Oral presentation

Development of imaging and quality assessment of X-ray laser focal spot and investigations of LiF crystals colorization thresholds

Faenov, A. Y.; Fukuda, Yuji; Pikuz, T.*; Bulanov, S. V.; Tanaka, Momoko; Kishimoto, Maki; Ishino, Masahiko; Kato, Yoshiaki*; Kawachi, Tetsuya

no journal, , 

Oral presentation

Development of imaging and quality assessment of X-ray laser focal spot and investigations of LiF crystals colorization thresholds

Faenov, A. Y.; Fukuda, Yuji; Pikuz, T. A.*; Bulanov, S. V.; Tanaka, Momoko; Kishimoto, Maki; Ishino, Masahiko; Kato, Yoshiaki*; Kawachi, Tetsuya

no journal, , 

51 (Records 1-20 displayed on this page)