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Nagata, Takashi; Mizuta, Shunji; Nagura, Fuminori
Enerugi Rebyu, 29(5), p.11 - 14, 2009/05
no abstracts in English
Kaito, Takeji; Otsuka, Satoshi; Inoue, Masaki; Asayama, Tai; Uwaba, Tomoyuki; Mizuta, Shunji; Ukai, Shigeharu*; Furukawa, Tomohiro; Ito, Chikara; Kagota, Eiichi; et al.
Journal of Nuclear Materials, 386-388, p.294 - 298, 2009/04
Times Cited Count:32 Percentile:88.55(Materials Science, Multidisciplinary)In order to examine irradiation effect on creep rupture strength of Oxide Dispersion Strengthened (ODS) steel claddings, the in-pile creep rupture test was conducted using Material Testing Rig with Temperature Control (MARICO)-2 in the experimental fast reactor JOYO. Fourteen creep rupture events were successfully detected by the temperature change in each capsule and the -ray spectrometry of the cover gas. Time to creep ruptures of six ODS steel specimens were identified by means of Laser Resonance Ionization Mass Spectrometry (RIMS), and no irradiation effect on creep rupture strength was confirmed within the irradiation condition in the MARICO-2 test.
Nagata, Takashi; Ichimiya, Masakazu; Funasaka, Hideyuki; Mizuta, Shunji; Nagura, Fuminori
Nihon Genshiryoku Gakkai-Shi ATOMO, 51(4), p.234 - 238, 2009/04
no abstracts in English
Mizuta, Shunji; Chikazawa, Yoshitaka; Washiya, Tadahiro; Suzuki, Masahiro
Nihon Genshiryoku Gakkai-Shi ATOMO, 50(10), p.624 - 629, 2008/10
no abstracts in English
Kaito, Takeji; Mizuta, Shunji; Uwaba, Tomoyuki; Otsuka, Satoshi; Ukai, Shigeharu
JNC TN9400 2005-015, 126 Pages, 2005/02
Oxide Dispersion Strengthened (ODS) ferritic steel has excellent swelling resistance and improved high-temperature strength, which are important properties for fast reactor fuel cladding tube. In feasibility study (FS) which is advanced by Japan Nuclear Cycle Development Institute (JNC), ODS ferritic steel is noticed as a prospective candidate material for commercialized fast reactor (FR) fuel cladding tube. JNC has developed a microstructure control procedure to disperse nano-sized oxide particles in equiaxed crystal grain and succeeded in producing high performance ODS ferritic steel tube, which has adequate mechanical properties. For the purpose of getting irradiation data base and evaluating applicability of ODS ferritic steel, fuel pin irradiation test of ODS ferritic steel cladding in FR such as JOYO is in the planning stage.This report describes a summary of the tentative materials strength standard of ODS ferritic steels for designing of FR fuel pin.
Hatakeyama, Koichi; Mizuta, Shunji; Fujiwara, Masayuki;
JNC TN9400 2001-110, 87 Pages, 2001/12
For the purpose of urgently discerning the applicability of ODS cladding tube to the long life core of the fast reactors, the irradiation test using Russian fast reactor BOR-60 is planned. In this irradiation test, TIG welding or laser welding will be applied as welding method of ODS cladding with end plug. In this report, applicability of alternative weldin9 method, i.e., TIG welding, laser welding, and also electron beam welding and 3 kinds of brazing diffusion bonding technique was evaluated. In addition, bending test and internal creep rupture test of the samples which were welded by laser and TIG welding were carried out. Following results were obtained in this study. (1) Tensile strength of laser welding test specimens with the highest energy density is most excellent in the welding process (over 90% of the base metal strength). (2) In the brazing filler metal, the tensile strength of the nickel brazing was most excellent (over 84% of the base metal strength). (3) In the bending test of laser and TIG welded test specimens, the crack was generated in circumferential direction of weld zone, which relatively corresponds to small bending angle. (4) As result of internal creep rupture test at 700C, cladding itself was ruptured in the high stress region, whereas, weld zone was ruptured in the low stress level.
Mizuta, Shunji; Fujiwara, Masayuki;
JNC TN9400 2001-103, 139 Pages, 2001/09
Oxide dispersion strengthened (ODS) ferritic steels have been developing as a long life fuel claddings, because they are expected to be superior structure stability and high temperature strength up to high neutron dose. In order to improve a strength anisotropy induced by an elongated grain structure along rolling direction, the effects of manufacturing process and added elements have been studied by means of recrystallization technique. The feasibility study was also conducted for economical manufacturing process with capable of large scale production. Following results were obtained in this study. (1)From cold rolling manufacturing study as a parameter of Ti and YO contents, claddings have been successfully manufactured through softening by recrystallization heat treatment. The grains tend to elongate along rolling direction with increasing Ti and YO contents. (2)The ring tensile tests show the improved strength with increasing Ti and YO contents: 0.3Ti-0.23YO has the highest strength. The uniform elongation and ductility in circumferential direction is maintained at entire temperature range. (3)The internal creep rupture strength is also improved by finely distributed YO-TiO complex oxides. The manufactured cladding with 0.3Ti-0.23YO is expected to attain the target strength (120MPa at 700C for 10,000h). (4)At the cladding manufacturing test with four times rolling, recrystallization structure was realized at the final heat treatment by suppressing heat treatment temperature up to recovery stage at intermediate heat treatment.
Tsai, H.*; Allen, T. R.*; Cole, J. I.*; Strain, R. V.*; Yoshitake, Tsunemitsu; Donomae, Takako; Akasaka, Naoaki; Mizuta, Shunji; Ukai, Shigeharu; Miyakawa, Shunichi
JNC TY9400 2001-025, 117 Pages, 2001/07
None
Otsuka, Satoshi; Uwaba, Tomoyuki; ; Mizuta, Shunji
JNC TN9400 2001-038, 40 Pages, 2001/03
14Cr-25Ni advanced austenitic steels (14Cr-25Ni steel) was developed in order to improve the swelling resistance of modified 15Cr-20Ni base austenitic steels(PNC1520). This steel is planned to be utilized as back-up material for Monju advanced core component. Seven types of cladding tubes with different amounts of alloying elements of Ti, Nb, V and P had been fabricated and the out-of-pile testing of these cladding tubes has been conducted. Among out of piles properties, tensile property and creep property of 14Cr-25Ni steels were evaluated in this study. The results can be summarized as follows. (1)Tensile properties (0.2% yield stress, ultimate tensile strength, uniform elongation, ultimate elongation) of 14Cr-25Ni steels were almost equivalent to those of PNC316 steel and PNC1520 steel in the temperature range from room temp. to 900C. (2)The creep strength of 14Cr-25Ni steels was between PNC316 and PNC1520. It was shown that the long term creep strength at 750C was remarkably improved by the Ti, Nb and V addition. (3)It is suspected that the improvement of creep strength of V-added-steel would be caused by stabilization of dislocation microstructure due to finely distributed carbo-nitride [Ti, Nb, V(C, N)] precipitates.
; ; Mizuta, Shunji
Effects of Radiation on Materials: 20th International Symposium (ASTM STP 1405), p.487 - 499, 2001/00
None
Yoshitake, Tsunemitsu; Donomae, Takako; Mizuta, Shunji; James J.Co*
Progtams and Abstrac, p.469 - 486, 2001/00
None
; Mizuta, Shunji; Yoshitake, Tsunemitsu; *
The Sixth Japan-China Symposium on Materials for Advanced Energy Systems and Fission & Fusion Engine, 0 Pages, 2001/00
None
; Mizuta, Shunji;
JNC TN9400 2000-104, 132 Pages, 2000/10
Ferritic/Martensitic steel (PNC-FMS) with superior resistance to swelling is being developed as wrapper tube for the long-life core of large-scale fast breeder reacor. If the ferrite phase would be formed at heat affected zone(HAZ)in welding between PNC-FMS wrapper tube and SUS316 steel,and thus toughness degradation would be suspected due to ferrite formation. In this study, the formation of the ferrite in applying TIG welding and EB welding are investigated using base metal of 3 types, which are Ni max./Cr min., Ni min./Cr max. and the center of chemical composition in the specification. The effect of the amount of the ferrite formation and characteristics of toughness change with thermal aging were evaluated. The results are summarized as follows. (1)The ferrite generation can be suppressed in the combination of welding process and chemical composition. (a)In case of specification center, the ferrite formation can be suppressed about 1% by EB welding. (b)In case of Ni max./Cr min. in the specification, the ferrite formation can be perfectly suppressed even in TIG welding or EB welding.
Fujiwara, Masayuki; Mizuta, Shunji;
JNC TN9400 2000-050, 19 Pages, 2000/04
For evaluating the fast reactor system technology, it is important to evaluate the practical feasibility of ODS ferritic cdaddings, which is the most promising matelials to attain the goal of high coolant temperature and more than 150 GWd/t. Based on the results of their technology development, mass production process with highly economically benefit as well as manufacturing cost estimation of ODS ferritic claddings were preliminarily conducted. From the view point of future utility scale, the cost for manufacturig mother tubes has a dominant factor in the total manufacturing cost. The method to reduce the cost of mother tube manufacturing was also preliminarily investigated.
Mizuta, Shunji; ;
JNC TN9400 2000-048, 28 Pages, 2000/04
ODS (Oxide Dispersion Strengthened) ferritic-martainsitic steels are one of the most prospective cladding materials for advanced fast breeder reactors, since they are expected to have excellent swelling resistance and superior high temperature strength due to the finely distributed stable oxide particles(YO). Properties and the tentative strength equations for ODS ferritic-martainsitic were proposed on the basis of the latest data to apply to the feasibility study of the sodium coolant MOX fuel plant. The items of equations are follows. (1)creep rupture strength (2)correction factor of creep rupture strength (in Na and in reactor) (3)outer surface eorrosion (Na) (4)inner surface corrosion (in MOX fuel pin) (5)thermal conductivity
; ; Mizuta, Shunji
JNC TN9400 2000-040, 41 Pages, 2000/03
The corrosion behavior of ferritic stainless steels applied to core components under C0 gas environment was investigated in order to be helpful to fuel design in C0 gas cooled reactor as the feasibility study for fast breeder reactor. The dependence of the corrosion behavior, before a breakaway occurs, on C0 gas temperature, Si and Cr contents of ferritic steels was determined quantitatively. The following correlations to calculate the metal loss thickness was established. X = 4.4w w = √(kt) k = exp( - 5.45[Si]) exp( - 1.09[Cr]) exp( - 11253/T) = 1.65 104.40 10 X : metal loss thickness[ml, w : corrosion weight gain [mg/cm] k : parabola constant [(mg/cm)/hr], t : time [hr], : constant [Si] : Si content[wt.%], [Cr] : Cr content [wt.%], T : temperature [K]
Mizuta, Shunji; ;
JNC TN9400 2000-032, 38 Pages, 2000/03
lt is necessary for feasibility study of fast reactor to evaluate the oxidation of the austenitic stainless steels in the case of using for core material in carbon dioxide gas-cooled reactor. The properties for oxidation of austenitic stainless steels in carbon dioxide were surveyed in literatures and the data were selected after evaluation of factors for oxidation in carbon dioxide. The equation of oxidation in carbon dioxide for PE16, 20Cr/25Ni/Nb, 18Cr-8Ni and JNC Cladding materials were proposed. The equation for oxidation of austenitic stainless steels were expressed as upper limit for the equation according to parabolic law. The equation for JNC cladding materials (PNC316, PNC1520, 14Cr-25Ni) was proposed based the oxidation behavior of 18Cr-8Ni which is same oxidation region for weight gain in three-component system of Fe-Cr-Ni, in addition to evaluate of effect for silicon content. The oxidation equation of 20Cr/25Ni/Nb was applied to the high Ni alloy of JNC cladding material. The obtained equation is as follows, X = 4.4W1000, W = , kp = exp(-Q/(RT)), X: oxide thickness[m], W : weight gain[gcm], kp : parabolic rate constant[gcm s], t :time[sec] : constant[gcmS], Q : activation energy[J・mol], R : gas constant[8.314J K mol], T : temperature[K] (1) PE16 : kp = 1.09010 exp(-192,500/(RD)), (2) 20Cr/25Ni/Nb : kp = 1.65110 exp(-201,300/(RT)) High Ni alloy (JNC), (3)18Cr-8Ni : kp = 1.50310 exp(-60,000/(RT)), (4) PNC316, PNC1520 : kp = 1.50310 exp(-60,000/(RT))0.62 14Cr-25Ni(JNC) The weight gain is (3)(4)(2)(1) in order.
Uwaba, Tomoyuki; Mizuta, Shunji;
JNC TN9400 2000-028, 41 Pages, 2000/03
14Cr-25Ni optimized advanced austenic steels have been developed to improve the swelling resistance of 15Cr-20Ni austenic stainless steels used for FBR fuel cladding. ln this improvement, Ti,Nb,V and P were dissolved into 14Cr-25Ni marix by means of the high-temperature solution treatment to make finely distributed and stabilized precipitates in the operation. Furthermore, at the final stage of cold-working, cold-working level increased and residual stress was reduced. ln this study, as fablicated microstructure observation, solubility of alloying elements and grain size test in the manufacturing process were evaluated. Following results were obtained. (1)Spherical precipitates were observed in the grain. Most of them were identified as conjugated carbo-nitride [Ti,Nb(C,N)] by EDX analysis. (2)The dissolved percentages of Ti and Ni in the matrix were about 70% and 30% respectively. Undissoved Ti and Nb may react with undissolved carbon and precipitate as MC carbides. (3)High-temperature solution treatment is effective for the sufficient solubility of alloying elements, but it is likely to induce very large grains, which is the cause of defective signal in the ultrasonic alloy testing. The results of the grain size test showed that the large grain size is reduced in low Nb (0.1wt%) alloy compared with the standard alloy (0.2wt%Nb), and the effectiveness for the grain size control by reducing the Nb content was confirmed. Also, it was suggested that the intermediate heat treatment and cold work conditions would possibly avoid the occurrence of the large grain at the final heat treatment.
; ; Mizuta, Shunji
JNC TN9400 2000-023, 126 Pages, 2000/02
Modified 316 and 15Cr-20Ni base austenitic stainless steels had been developed by Japan Nuclear Cycle Development lnstitute as the candidate materials for Monju and Demonstration fast breeder reactor. Previously, irradiation creep correlation of modified 316 and 15Cr-20Ni had been evaluated using pressurized tubes irradiated in FFTF/MOTA. 0n the other hand, for other austenitic S.S. developed abroad, it was reported that irradiation creep behavior of fuel pin could not be sufficiently described using results of pressurized tube experiments. ln this study, irradiation creep properties of modified 316 and 15Cr-20Ni fuel pins (MFA-I, 2) irradiated in FFTF were evaluated. And irradiation deformation of MFA-1, 2 fuel pins were estimated using the irradiation creep correlation based on MOTA data. The results are summarized as follows : (1)Irradiation creep compliance B calculated from MFA-I, 2 data are 5.6 15.010 [(I0n/m, E>0.1Mev)(MPa)], Which are larger than B based on MOTA data of 2.26.410 and are within the range of B of other austenitic S.S. abroad. (2)Creep-swelling coupling coefficient D derived from MFA-1, 2 data tend to decrease with increasing swelling rate. And the range of D based on MFA-1, 2 data include values calculated from MOTA data of 3.88.210 [(MPa)] and for other austenitic S.S. abroad. (3)As the result that irradiation creep deformation of MFA-1, 2 fuel pins could be appropriately estimated using the irradiation creep correlation derived from MOTA data, it is considered that the creep, correlation based on MOTA data can be applied to estimation of fuel pin deformation.
Ukai, Shigeharu; Mizuta, Shunji; Kaito, Takeji; Okada, Y.*
Journal of Nuclear Materials, 278, p.320 - 327, 2000/00
Times Cited Count:17 Percentile:72(Materials Science, Multidisciplinary)None