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Kinsho, Michikazu; Kamiya, Junichiro; Abe, Kazuhiko*; Nakamura, Tomaru*
Proceedings of 10th International Particle Accelerator Conference (IPAC '19) (Internet), p.4161 - 4163, 2019/06
Alumina ceramics vacuum chamber which is used for the 3GeV rapid-cycling synchrotron (RCS) in J-PARC is composed of alumina duct, titanium (Ti) flanges and Ti sleeves. Before brazing the alumina duct and the Ti sleeves, the Ti sleeves were treated with nitric hydrofluoric acid. The purpose of this study is to clear the effect of this treatment for titanium material. It was cleared by SEM observation that the roughness of the titanium material after the nitric hydrofluoric acid treatment becomes big. It was also measured that the thickness of oxide film on surface of the titanium material was 12.7 nm before treatment and 6.0 nm after treatment. It became clear that both the clearing of oxide layer on the alumina ceramics and the vacuum condition of the vacuum heating furnace were important for brazing between alumina ceramics and pure titanium.
Kinsho, Michikazu; Kamiya, Junichiro; Abe, Kazuhiko*; Nakamura, Tomaru*
Proceedings of 15th Annual Meeting of Particle Accelerator Society of Japan (Internet), p.1177 - 1179, 2018/08
Alumina ceramics vacuum Chamber which is used for the RCS in J-PARC is composed of alumina duct, titanium (Ti) flanges and Ti sleeves. Before brazing the alumina duct and the Ti sleeves, the Ti sleeves were treated with Nitric acid-Hydrofluoric acid. The purpose of this study is to clear the effect of this treatment for titanium material. It was cleared that the roughness of the titanium material after the Nitric acid-Hydrofluoric acid treatment becomes big for SEM observation. It was also measured that the thickness of oxide film on surface of the titanium material was 12.7 nm before treatment and 6.0 nm after treatment. As a result of measuring the wettability of the brazing material which was silver brazing filler metal (Ag:72%, Cu:28%) on the Ti surface and the diffusion of the Ti material into the brazing material, it became clear that the vacuum condition of the vacuum heating furnace was important for brazing between alumina ceramics and pure titanium.
Kinsho, Michikazu; Saito, Yoshio*; Kabeya, Zenzaburo*; Tajiri, Keisuke*; Nakamura, Tomaru*; Abe, Kazuhiko*; Nagayama, Taketoshi*; Nishizawa, Daiji*; Ogiwara, Norio
Vacuum, 73(2), p.187 - 193, 2004/03
Times Cited Count：17 Percentile：54.99(Materials Science, Multidisciplinary)Alimina ceramics vacuum duct has been developing at JAERI for the 3GeV-RCS of the J-PARC project. There are two type of the alumina ceramics vacuum ducts, one is a 1.5m-long duct with a circular cross section for use in the quadrupole magnet, the other is a 3.5m-long being bending 15 degree with an elliptical cross section for use in the dipole magnet.These ducts could be manufactured by brazed jointing several duct segments of 0.5-0.8 m long. Since some electrically conductive boundary is necessary to form on the ceramics duct in order to reduce the duct impedance, the alumina ceramics ducts have copper stripes on the outside surface of the ducts. This is called for rf shielding system. The copper stripes as rf shielding is produced by an electroforming method. In order to reduce emitting secondary electrons when primary protons or electrons impinge onto the surface, TiN film is coated inside surface of the alumina ceramics duct.
Kinsho, Michikazu; Kamiya, Junichiro; Abe, Kazuhiko*; Nakamura, Tomaru*
no journal, ,
Alumina ceramics vacuum Chamber which is used for the 3 GeV rapid-cycling synchrotron (RCS) in J-PARC is composed of alumina duct, Ti flanges and Ti sleeves. Before brazing the alumina duct and the Ti sleeves, the Ti sleeves were treated with Nitric acid-Hydrofluoric acid. The purpose of this study is to clear the effect of this treatment for titanium material. It was cleared that the roughness of the titanium material after the Nitric acid-Hydrofluoric acid treatment becomes big for SEM observation. It was also measured that the thickness of oxide film on surface of the titanium material was 12.7 nm before treatment and 6.0 nm after treatment.
