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Kurihara, Momo*; Yasutaka, Tetsuo*; Aono, Tatsuo*; Ashikawa, Nobuo*; Ebina, Hiroyuki*; Iijima, Takeshi*; Ishimaru, Kei*; Kanai, Ramon*; Karube, Jinichi*; Konnai, Yae*; et al.
Journal of Radioanalytical and Nuclear Chemistry, 322(2), p.477 - 485, 2019/11
Times Cited Count：2 Percentile：21.58(Chemistry, Analytical)We assessed the repeatability and reproducibility of methods for determining low dissolved radiocesium concentrations in freshwater in Fukushima. Twenty-one laboratories pre-concentrated three of 10 L samples by five different pre-concentration methods (prussian-blue-impregnated filter cartridges, coprecipitation with ammonium phosphomolybdate, evaporation, solid-phase extraction disks, and ion-exchange resin columns), and activity of radiocesium was measured. The z-scores for all of the 
Cs results were within 
2, indicating that the methods were accurate. The relative standard deviations (RSDs) indicating the variability in the results from different laboratories were larger than the RSDs indicating the variability in the results from each separate laboratory.
Ohashi, Yusuke; Nakatsuka, Yoshiaki; Kawatsuma, Shinji; Hata, Haruhi; Tsunashima, Yasumichi; Murata, Masato; Tokizawa, Takayuki; Sugitsue, Noritake
no journal, ,
Sludge waste derived from research and discussion for uranium refining and conversion exclude much uranium. We must recover uranium from them from the point of view of use of resource and we dispose of residue generated by the process. We recovered uranium from real waste by water or hydrochloric acid. The dissolution rates of uranium from sludge from neutralization and NaF, filter medium, alumina, MgF
wastes were more than 99% by 2 hour 1N HCl treatment. The dissolution rate of uranium from bed material waste was more than 99% by 24h 1N HCl treatment and addition of hydrogen peroxide. The dissolution rates of NaF, filter medium waste by water treatment were 99% and 88%. From the results, we confirmed dissolution characteristics of real waste as basic data to study recovery process of uranium.
Tsunashima, Yasumichi; Nakatsuka, Yoshiaki; Kawatsuma, Shinji; Ohashi, Yusuke; Murata, Masato; Tokizawa, Takayuki; Sugitsue, Noritake; Hata, Haruhi
no journal, ,
The operation waste generated from the uranium handling facilities of the uranium conversion and uranium enrichment, etc. is called a sludge. They are assumed to be execution of the uranium collection if necessary, cement solidification, and disposal. Therefore, the examination that confirmed the range where cement solidifies was executed. The cement kind, the water cement ratio, and the sludge mixture rate were assumed to be a parameter and the solidification test was executed. The range of solidification was confirmed by the bleeding water after 24 hours had passed. The uniaxial compression was measured with cement in the solidification condition. A possibility miscible from 40wt% to about 60wt% was able to be confirmed from these examination results in the absorbent (NaF pellet and active alumina), the bed materials (no active alumina), Neutralizing precipitation.
