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Journal Articles

Extraction of Rh(III) from hydrochloric acid by protonated NTAamide(C6) and analogous compounds and understanding of extraction equilibria by using UV spectroscopy and DFT calculations

Sasaki, Yuji; Kaneko, Masashi; Ban, Yasutoshi; Kinoshita, Ryoma; Matsumiya, Masahiko*; Shinoku, Kota*; Shiroishi, Hidenobu*

Analytical Sciences, 39(9), p.1575 - 1583, 2023/09

 Times Cited Count:0 Percentile:0(Chemistry, Analytical)

Extraction of Rh from HCl can be performed by NTAamide(C6) (hexahexyl-nitrilotriacetamide) and other related compounds into n-dodecane. We use ion-pair extraction of anionic species of Rh-chloride and protonated extractant. Rh behave as anion in hydrochloric acid and the tertiary nitrogen atom in extractant may be protonated to produce the quaternary amine in acidic condition. From the present work, the maximum distribution ratio of Rh(III) is 16. The D(Rh) values are changeable during preparation of the aqueous solutions because different Rh-Cl-H$$_{2}$$O complexes are formed in HCl media and show the slow exchange rate between Cl and H$$_{2}$$O. Using the UV spectrum, Rh-chloride solution having the peak of spectrum at 504 nm can be extracted effectively, where RhCl$$_{4}$$(H$$_{2}$$O)$$^-$$ and RhCl$$_5$$(H$$_2$$O)$$^2$$$$^-$$ exist mainly from DFT calculation. Stoichiometry of one-one complex of Rh and NTAamide is obtained from slope analysis, and 85 mM of concentrated Rh ion can be extracted.

Journal Articles

Sodium-cooled Fast Reactors

Ohshima, Hiroyuki; Morishita, Masaki*; Aizawa, Kosuke; Ando, Masanori; Ashida, Takashi; Chikazawa, Yoshitaka; Doda, Norihiro; Enuma, Yasuhiro; Ezure, Toshiki; Fukano, Yoshitaka; et al.

Sodium-cooled Fast Reactors; JSME Series in Thermal and Nuclear Power Generation, Vol.3, 631 Pages, 2022/07

This book is a collection of the past experience of design, construction, and operation of two reactors, the latest knowledge and technology for SFR designs, and the future prospects of SFR development in Japan. It is intended to provide the perspective and the relevant knowledge to enable readers to become more familiar with SFR technology.

JAEA Reports

Analysis of the radioactivity concentrations in low-level radioactive waste generated from JRR-2, JRR-3 and hot laboratory facilities

Tobita, Minoru*; Haraga, Tomoko; Sasaki, Takayuki*; Seki, Kotaro*; Omori, Hiroyuki*; Kochiyama, Mami; Shimomura, Yusuke; Ishimori, Kenichiro; Kameo, Yutaka

JAEA-Data/Code 2019-016, 72 Pages, 2020/02

JAEA-Data-Code-2019-016.pdf:2.67MB

In the future, radioactive wastes which generated from research and testing reactors in Japan Atomic Energy Agency are planning to be buried for the near surface disposal. Therefore, it is required to establish the method to evaluate the radioactivity concentrations of radioactive wastes by the time it starts disposal. In order to contribute to this work, we collected and analyzed the samples generated from JRR-2, JRR-3 and Hot laboratory facilities. In this report, we summarized the radioactivity concentrations of 25 radionuclides ($$^{3}$$H, $$^{14}$$C, $$^{36}$$Cl, $$^{60}$$Co, $$^{63}$$Ni, $$^{90}$$Sr, $$^{94}$$Nb, $$^{93}$$Mo, $$^{99}$$Tc, $$^{108m}$$Ag, $$^{126}$$Sn, $$^{129}$$I, $$^{137}$$Cs, $$^{152}$$Eu, $$^{154}$$Eu, $$^{233}$$U, $$^{234}$$U, $$^{238}$$U, $$^{238}$$Pu, $$^{239}$$Pu, $$^{240}$$Pu, $$^{241}$$Pu, $$^{241}$$Am, $$^{243}$$Am, $$^{244}$$Cm) which were obtained from radiochemical analysis of those samples.

Journal Articles

Student and Young researcher's view of research on health physics and environment science

Miwa, Kazuji; Terasaka, Yuta; Ochi, Kotaro; Futemma, Akira; Sasaki, Miyuki; Hirouchi, Jun

Nihon Genshiryoku Gakkai-Shi ATOMO$$Sigma$$, 61(9), p.687 - 691, 2019/09

This report summarizes the contents of the session of the Health Physics and Environment Science Division, which was held in Atomic Energy Society of Japan 2019 Spring Meeting. In this session, six students and young researchers who engaged in the field of nuclear energy and radiation gave a lecture about health physics and environmental science research through their expertise. After the all presentations end, we took discussion time about the issues and future development in this field with all attendees. In this report, we summarized each lecture outline and discussion contents.

Journal Articles

Comparison of airborne and ground-based tools used for radiation measurement in the environment

Ochi, Kotaro; Sasaki, Miyuki; Ishida, Mutsushi*; Sanada, Yukihisa

Progress in Nuclear Science and Technology (Internet), 6, p.103 - 107, 2019/01

After the Fukushima Daiichi Nuclear Power Plant (FDNPP) accident, a large amount of radionuclides was spread out all over the world. In our previous study, we developed the aerial radiation monitoring technique using unmanned helicopter for investigating the dose rate derived deposited radionuclides over wide area. In addition, many monitoring techniques were developed for investigating the local distribution of radionuclides using unmanned aerial vehicle, handheld instrument and car within small area. Distinction of these methods depends on desirable position resolution of dose rate. However, the comparison method of the measurement result between different methods is not established. In this study, we attempted to evaluate the some methods of airborne and ground radiation measurement in same extended farm.

Journal Articles

Evaluation of ecological half-life of dose rate based on airborne radiation monitoring following the Fukushima Dai-ichi Nuclear Power Plant accident

Sanada, Yukihisa; Urabe, Yoshimi*; Sasaki, Miyuki; Ochi, Kotaro; Torii, Tatsuo

Journal of Environmental Radioactivity, 192, p.417 - 425, 2018/12

 Times Cited Count:26 Percentile:68.96(Environmental Sciences)

Journal Articles

Estimation of the vertical distribution of radiocesium in soil on the basis of the characteristics of $$gamma$$-ray spectra obtained via aerial radiation monitoring using an unmanned helicopter

Ochi, Kotaro; Sasaki, Miyuki; Ishida, Mutsushi*; Hamamoto, Shoichiro*; Nishimura, Taku*; Sanada, Yukihisa

International Journal of Environmental Research and Public Health, 14(8), p.926_1 - 926_14, 2017/08

 Times Cited Count:4 Percentile:22.93(Environmental Sciences)

After the Fukushima Daiichi Nuclear Power Plant accident, the vertical distribution of radiocesium in soil has been investigated to better understand the behavior of radiocesium in the environment. The typical method used for measuring the vertical distribution of radiocesium is troublesome because it requires collection and measurement of the activity of soil samples. In this study, we established a method of estimating the vertical distribution of radiocesium by focusing on the characteristics of $$gamma$$-ray spectra obtained via aerial radiation monitoring using an unmanned helicopter. In this method, the change in the ratio of direct $$gamma$$ rays to scattered $$gamma$$ rays at various depths in the soil was utilized to quantify the vertical distribution of radiocesium. The results show a positive correlation between the abovementioned and the actual vertical distributions of radiocesium measured in the soil samples.

Journal Articles

The Succession of bacterial community structure in groundwater from a 250-m gallery in the Horonobe Underground Research Laboratory

Ise, Kotaro; Sasaki, Yoshito; Amano, Yuki; Iwatsuki, Teruki; Nanjo, Isao*; Asano, Takahiro*; Yoshikawa, Hideki

Geomicrobiology Journal, 34(6), p.489 - 499, 2017/07

 Times Cited Count:4 Percentile:14.31(Environmental Sciences)

We investigated the change in bacterial community structure after drilling boreholes, 09-V250-M02 and 09-V250-M03 in the 250 m depth research gallery of Horonobe Underground Research Laboratory (URL). In 09-V250-M02, $$varepsilon$$-Proteobacteria was predominantly detected in the clone library analyses of the groundwater samples conducted immediately after drilling the borehole. All these $$varepsilon$$-Proteobacteria clones are closely related to ${{it Arcobacter spp}}$. which is known as sulfide oxidizing chemoautotrophic bacteria. After four years, the microbial structure was drastically changed and most detected OTUs were uncultured species such as candidate division OP9 and Chloroflexi relatives which are frequently detected in deep-sea sediments.

JAEA Reports

Study on radionuclide analysis of rubble and plants for decommissioning of Fukushima Daiichi Nuclear Power Station

Seki, Kotaro; Sasaki, Takayuki*; Akimoto, Yuji*; Tokunaga, Takahito; Tanaka, Kiwamu; Haraga, Tomoko; Ueno, Takashi; Ishimori, Kenichiro; Hoshi, Akiko; Kameo, Yutaka

JAEA-Technology 2016-013, 37 Pages, 2016/07

JAEA-Technology-2016-013.pdf:2.09MB

In this study, based on the simple and rapid analytical method established from the wastes from research facilities, we created analytical schemes which is applicable to rubble and plants collected at Fukushima Daiichi, then transported to Nuclear Science Research Institute of JAEA. We examined the applicability, and confirmed quantifiability of radioactivity concentration with high recovery rate without being affected by fission products such as $$^{90}$$Sr and $$^{137}$$Cs.

Journal Articles

Development of electromagnetic non-destructive testing method for the inspection of heat exchanger tubes of Japan Sodium-cooled Fast Reactor, 2; Detection of flaws on the inner surface using electromagnetic waves

Sasaki, Kota*; Yusa, Noritaka*; Wakai, Takashi; Hashizume, Hidetoshi*

Electromagnetic Nondestructive Evaluation (XVIII), p.244 - 251, 2015/06

 Times Cited Count:0 Percentile:0.05

Journal Articles

Radioactivity evaluation of the secondary sodium in DRACS of the Japan Sodium-cooled Fast Reactor

Sasaki, Kenji*; Naito, Katsuaki*; Oki, Shigeo; Okubo, Tsutomu; Kotake, Shoji*

Progress in Nuclear Science and Technology (Internet), 4, p.94 - 98, 2014/04

This paper evaluates the amount of activation of the secondary sodium in Direct Heat Exchanger (DHX) by neutrons leaked from the core, the radioactivity density, and the dose rate around the secondary sodium pipes in Direct Reactor Auxiliary Cooling System (DRACS) and confirms that the requirements in radioactivity free areas are satisfied by improving the exactness of calculation model with Monte Carlo Methodology.

Journal Articles

Observation of the laser-induced surface dynamics using the single-shot soft X-ray laser probe

Hasegawa, Noboru; Ochi, Yoshihiro; Kawachi, Tetsuya; Nishikino, Masaharu; Ishino, Masahiko; Imazono, Takashi; Kaihori, Takeshi; Morita, Toshimasa; Sasaki, Akira; Terakawa, Kota*; et al.

X-Ray Lasers 2012; Springer Proceedings in Physics, Vol.147, p.117 - 120, 2014/00

 Times Cited Count:0 Percentile:0

We have developed the femto-second laser pump and soft X-ray laser probe system in order to observe the dynamical processes of the femto-second laser ablation. By using this system, we succeed to obtain the temporal evolution of the soft X-ray reflectivity from the laser induced Pt surface. The results lead that the rate of decrease in the reflectivity of the probe beam has a non-linear relation with the pump laser fluence.

Journal Articles

Enhanced charge collection by single ion strike in AlGaN/GaN HEMTs

Onoda, Shinobu; Hasuike, Atsushi*; Nabeshima, Yoshiaki*; Sasaki, Hajime*; Yajima, Kotaro*; Sato, Shinichiro; Oshima, Takeshi

IEEE Transactions on Nuclear Science, 60(6), p.4446 - 4450, 2013/12

 Times Cited Count:38 Percentile:94.87(Engineering, Electrical & Electronic)

no abstracts in English

Journal Articles

Enhancement of microwave nondestructive testing method for the inspection of pipes by optimizing the microwave probe profile

Sasaki, Kota*; Yusa, Noritaka*; Wakai, Takashi; Hashizume, Hidetoshi*

Hozengaku, 12(1), p.81 - 86, 2013/04

This study reports the development of a new microwave probe for the nondestructive testing of a pipe. Three-dimensional finite element simulations are carried out to optimize the profile of a microwave probe, whose results show that a probe with elliptic profile enables smaller reflection at the probes as well as much better single-mode propagation inside the pipe than conventional ones. Experimental validations are carried out using a straight brass pipe with an inner diameter of 39 mm and a total length of 2 m. The results of the experiments clearly demonstrate that the new microwave probe provides clearer signals due to simulated rectangular wall thinning.

Journal Articles

Validation of surface-based hydrochemical investigation and the impact of underground facility construction at Horonobe URL

Amano, Yuki; Nanjo, Isao; Murakami, Hiroaki; Yabuuchi, Satoshi; Yokota, Hideharu; Sasaki, Yoshito; Iwatsuki, Teruki

Chikasui Gakkai-Shi, 54(4), p.207 - 228, 2012/11

We verified the surface-based hydrochemical investigation for deep underground at Horonobe Underground Research Laboratory (URL) at Horonobe, Hokkaido, Japan, and identified the hydrochemical changes during the URL construction. The evaluation of the relationship between the number of borehole and understanding of water chemistry suggests that three basic borehole investigations and additional borehole for high permeable geological structure (fault and fractured zone) are required to illustrate cross-sectional hydrochemical distribution including the uncertainty in kilometers scale survey line. The observation and numerical analysis of hydrochemical variation (salinity, pH, ORP) around URL indicate that the groundwater pressure and the salinity in the vicinity of high permeable geological zone are varying due to groundwater inflow into the drift. The variation was consistent with the prediction reported previously. These results are considered to be referred to the management during surface-based investigation and construction of underground facility at the other sedimentary rock area.

Journal Articles

Development on microwave nondestructive testing of a wall thinning inside a pipe by optimizing microwave probe and analyzing wall thinning profile

Sasaki, Kota*; Liu, L.*; Yusa, Noritaka*; Wakai, Takashi; Hashizume, Hidetoshi*

Proceedings of 1st International Conference on Maintenance Science and Technology for Nuclear Power Plants (ICMST-Tokyo 2012) (CD-ROM), 2 Pages, 2012/11

Journal Articles

Development of the X-ray interferometer and the method of spatial and temporal synchronization of XRL and optical pulse

Hasegawa, Noboru; Ochi, Yoshihiro; Kawachi, Tetsuya; Terakawa, Kota*; Tomita, Takuro*; Yamamoto, Minoru; Nishikino, Masaharu; Oba, Toshiyuki; Kaihori, Takeshi; Imazono, Takashi; et al.

X-Ray Lasers 2010; Springer Proceedings in Physics, Vol.136, p.353 - 358, 2011/12

The understanding of the dynamics of the initial process is important for the micro processing and welding by the ultra-short laser pulse. The X-ray laser is suitable for probing this initial process because it has short wavelength (Ni-like Ag, 13.9 nm) and short duration (7 ps). For this investigation, the origin of time of the pumping pulse is quite important. In this study, we used the scintillation plate and the plasma gate technique to realize the spatial and temporal synchronization of the pump and probe pulses. For the spatial alignment, a CsI scintillation plate that was set at the sample position was illuminated by both the X-ray laser pulse, and the fluorescence light were detected by the CCD camera. For the temporal synchronization, we set a thin foil at the sample position. We measured the transmission of the X-ray laser while changing a temporal delay of the pumping laser with respect to the time of X-ray laser pulse to obtain the origin of the irradiation time.

Journal Articles

Observation of the laser-induced surface dynamics by the single-shot X-ray laser interferometer

Hasegawa, Noboru; Ochi, Yoshihiro; Kawachi, Tetsuya; Nishikino, Masaharu; Ishino, Masahiko; Imazono, Takashi; Kaihori, Takeshi; Sasaki, Akira; Terakawa, Kota*; Minami, Yasuo*; et al.

Proceedings of SPIE, Vol.8140, p.81400G_1 - 81400G_8, 2011/10

 Times Cited Count:3 Percentile:82.27

We have developed a soft X-ray laser (SXRL) interferometer capable of the single-shot imaging of nano-scaled structure dynamics. The interferometer consisted of the reflection optics including double Lloyd's mirrors and focusing optics, and the interference fringes are produced on the detector surface. By using this interferometer, the initial stage ($$sim$$50 ps) of the ablation process of the Pt surface pumped by a 70 fs Ti:Sapphire laser pulse was observed. The expansion speed of the surface estimated from the result (34 nm/50 ps) indicated that the nano-bubble structures were formed in the initial stage of the ablation. In order to observe the detailed dynamics, the temporal synchronization between the pump and probe pulses was improved to be 3 ps by adopting a portion of the SXRL and pump beams as the time fiducials, to which the pump and probe timing was adjusted by using the X-ray streak camera.

Journal Articles

Recent progress in the energy recovery linac project in Japan

Sakanaka, Shogo*; Akemoto, Mitsuo*; Aoto, Tomohiro*; Arakawa, Dai*; Asaoka, Seiji*; Enomoto, Atsushi*; Fukuda, Shigeki*; Furukawa, Kazuro*; Furuya, Takaaki*; Haga, Kaiichi*; et al.

Proceedings of 1st International Particle Accelerator Conference (IPAC '10) (Internet), p.2338 - 2340, 2010/05

Future synchrotron light source using a 5-GeV energy recovery linac (ERL) is under proposal by our Japanese collaboration team, and we are conducting R&D efforts for that. We are developing high-brightness DC photocathode guns, two types of cryomodules for both injector and main superconducting (SC) linacs, and 1.3 GHz high CW-power RF sources. We are also constructing the Compact ERL (cERL) for demonstrating the recirculation of low-emittance, high-current beams using above-mentioned critical technologies.

Journal Articles

Progress in R&D efforts on the energy recovery linac in Japan

Sakanaka, Shogo*; Ago, Tomonori*; Enomoto, Atsushi*; Fukuda, Shigeki*; Furukawa, Kazuro*; Furuya, Takaaki*; Haga, Kaiichi*; Harada, Kentaro*; Hiramatsu, Shigenori*; Honda, Toru*; et al.

Proceedings of 11th European Particle Accelerator Conference (EPAC '08) (CD-ROM), p.205 - 207, 2008/06

Future synchrotron light sources based on the energy-recovery linacs (ERLs) are expected to be capable of producing super-brilliant and/or ultra-short pulses of synchrotron radiation. Our Japanese collaboration team is making efforts for realizing an ERL-based hard X-ray source. We report recent progress in our R&D efforts.

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