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Journal Articles

Oxidation behaviour of P122 and a 9Cr-2W ODS steel at 550$$^{circ}$$C in oxygen-containing flowing lead-bismuth eutectic

Schroer, C.*; Konys, J.*; Furukawa, Tomohiro; Aoto, Kazumi

Journal of Nuclear Materials, 398(1-3), p.109 - 115, 2010/03

 Times Cited Count:52 Percentile:95.38(Materials Science, Multidisciplinary)

The long-term performance of P122 and ODS steel was tested in oxygen-containing flowing lead-bismuth eutectic at 550 $$^{circ}$$C and a flow velocity of 2 m/s by means of exposure experiments in the CORRIDA loop of FZK. The target for the enrichment of dissolved oxygen was a concentration, c$$_{o}$$, of 10$$^{-6}$$mass%. Owing to initial problems in controlling c$$_{o}$$, some of the exposed specimens experienced varying conditions, which allowed for investigating the influence of temporarily low c$$_{o}$$ (down to 10$$^{-9}$$mass%), in addition to constantly high c$$_{o}$$ (averaging 1.6$$times$$10$$^{-6}$$mass%). Maximum exposure times at constantly high c$$_{o}$$ were 10,000 and 20,000 h for P122 and the ODS steel, respectively. Under the testing conditions, both steels were affected by moderate oxidation resulting in the formation of a compact layer of a spinel-type oxide on the surface and a more or less pronounced internal oxidation zone. The thickness of the oxide scale was quantified and used for determining the material loss. For c$$_{o}$$ = 10$$^{-6}$$mass%, logarithmic and power rate laws were fitted to the obtained data as a basis for predicting the metal recession at times exceeding the experimental exposure times.

JAEA Reports

Study on Pb-Bi Corrosion of Structural and Fuel Cladding Materials for Nuclear Applications; Part VI. Results of Exposure Experiments in Oxygen Containing Flowing LBE at 550$$^{circ}$$C for 10,000h

Schroer, C.*; Voss, Z.*; Wedemeyer, O.*; Novotny, J.*; Konys, J.*; Heinzel, A.*; Weisenburger, A.*; M$"u$ller, G.*; Furukawa, Tomohiro; Aoto, Kazumi

JNC TY9400 2005-020, 45 Pages, 2005/08

JNC-TY9400-2005-020.pdf:5.26MB

This report summarises the results of exposure experiments on the behaviour of 12Cr-2W steel P122 and an 9Cr-2W ODS-steel in oxygen-containing flowing lead-bismuth eutectic (LBE) at 550$$^{circ}$$C, which were performed in the CORRIDA loop at the Karlsruhe Lead Laboratory (KALLA) as part of the collaboration between the Japan Nuclear Cycle Development Institute and the Karlsruhe Research Centre. The duration of these experiments was nominally 800, 2000, 5000 and 10,000 h. Both steels were tested after surface-finishing by turning and after surface alloying with aluminium in the GESA-facility. Owing to initial problems with the enrichment of oxygen in the flowing LBE, the oxygen content considerably varied during most of these experiments, so that the influence of temporary changes in the oxygen content of the LBE could also be investigated. The behaviour of P122 and ODS at permanently high oxygen content was deduced from an experiment for 4990 h at 550$$^{circ}$$C and (c$$_{O}$$ $$approx$$ 5$$times$$10$$^{-7}$$ mass-% or a$$_{PbO}$$ $$approx$$ 10$$^{-3}$$). The results are compared with the findings of exposures to stagnant LBE at 550$$^{circ}$$C and c$$_{O}$$=10$$^{-6}$$ mass-% (COSTA-experiments).

JAEA Reports

Study on Pb-Bi Corrosion of Structural and Fuel Cladding Materials for Nuclear Applications (2); Part II. Exposure of Weld P122 in Oxygen Containing Flowing LBE at 550$$^{circ}$$C for 5,000h

Schroer, C.*; Voss, Z.*; Wedemeyer, O.*; Novotny, J.*; Konys, J.*; Heinzel, A.*; Weisenburger, A.*; M$"u$ller, G.*; Furukawa, Tomohiro; Aoto, Kazumi

JNC TY9400 2005-019, 26 Pages, 2005/08

JNC-TY9400-2005-019.pdf:5.04MB

This report summarises the results of exposure experiments on the behaviour of 12Cr-2W steel P122 joined by multi-run TIG welding in oxygen-containing flowing lead-bismuth eutectic (LBE) at 550$$^{circ}$$C for nominally 800, 2000 and 5000 h. The flow velocity of the LBE and the mean oxygen content were 2 m/s and 5$$times$$10-7 mass-% (aPbO = 10-3), respectively. The influence of surface-alloying with aluminium (GESA-treatment) was also investigated in an exposure experiment for nominally 5000 h. The behaviour of the welded joint is generally comparable to that of P122 (after the standard heat-treatment), both qualitatively and quantitatively. Only few exceptions were observed which probably result from local peculiarities of the specific sample material. After surface alloying with aluminium, no significant oxidation and no liquid metal corrosion occurred in the centre of the specimens (including the weld seam), where the desired high quality of the aluminised layer was achieved.

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