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Journal Articles

Quantitatively evaluating respective contribution of austenite and deformation-induced martensite to flow stress, plastic strain, and strain hardening rate in tensile deformed TRIP steel

Mao, W.; Gao, S.*; Gong, W.; Bai, Y.*; Harjo, S.; Park, M.-H.*; Shibata, Akinobu*; Tsuji, Nobuhiro*

Acta Materialia, 256, p.119139_1 - 119139_16, 2023/09

 Times Cited Count:5 Percentile:90.35(Materials Science, Multidisciplinary)

Transformation-induced plasticity (TRIP)-assisted steels exhibit an excellent combination of strength and ductility due to enhanced strain hardening rate associated with deformation-induced martensitic transformation (DIMT). Quantitative evaluation on the role of DIMT in strain hardening behavior of TRIP-assisted steels and alloys can provide guidance for designing advanced materials with strength and ductility synergy, which is, however, difficult since the phase composition keeps changing and both stress and plastic strain are dynamically partitioned among constituent phases during deformation. In the present study, tensile deformation with ${it in situ}$ neutron diffraction measurement was performed on an Fe-24Ni-0.3C (wt.%) TRIP-assisted austenitic steel. The analysis method based on stress partitioning and phase fractions measured by neutron diffraction was proposed, by which the tensile flow stress and the strain hardening rate of the specimen were resolved into factors associated with each phase, i.e., the austenite matrix, deformation-induced martensite, and the transformation rate of DIMT after differentiation, and then the role of each factor in the global strain hardening behavior was discussed. In addition, the plastic strain partitioning between austenite and martensite was indirectly estimated using the dislocation density measured by diffraction profile analysis, which constructed the full picture of stress and strain partitioning between austenite and martensite in the material. The results suggested that both the transformation rate and the phase stress borne by the deformation-induced martensite played important roles in the global tensile properties of the material. The proposed decomposition analysis method could be widely applied to investigating mechanical behavior of multi-phase alloys exhibiting the TRIP phenomenon.

Journal Articles

Hyperfine splitting and nuclear spin polarization in NdPd$$_5$$Al$$_2$$ and Nd$$_3$$Pd$$_{20}$$Ge$$_6$$

Metoki, Naoto; Shibata, Kaoru; Matsuura, Masato*; Kitazawa, Hideaki*; Suzuki, Hiroyuki*; Yamauchi, Hiroki; Hagihara, Masato; Frontzek, M. D.*; Matsuda, Masaaki*

Journal of the Physical Society of Japan, 91(5), p.054710_1 - 054710_6, 2022/05

 Times Cited Count:0 Percentile:0(Physics, Multidisciplinary)

Hyperfine splitting of Nd nuclei in NdPd$$_5$$Al$$_2$$ has been studied by means of high-resolution neutron spectroscopy. We observed inelastic peaks at $$hbaromega =pm3;{mu}$$eV coming from the hyperfine splitting in the magnetically ordered phase due to the hyperfine interactions between Nd nuclei ($$I$$=7/2) and the 4$$f$$ electrons with $$Gamma_6$$ ground state composed of mainly $$|pm9/2rangle$$. At very low temperatures, nuclear spin of Nd is polarized with increasing occupation probability of low energy levels and contributes to the enhancement of the antiferromagnetic Bragg intensities: the elastic non-spin-flip channel is dominant. As an application of this phenomenon, we determined the Nd moment and hyperfine splitting from the temperature dependence of an antiferromagnetic Bragg intensities for Nd$$_3$$Pd$$_{20}$$Ge$$_6$$.

Journal Articles

Effective grain size refinement of an Fe-24Ni-0.3C metastable austenitic steel by a modified two-step cold rolling and annealing process utilizing the deformation-induced martensitic transformation and its reverse transformation

Mao, W.; Gao, S.*; Bai, Y.*; Park, M.-H.*; Shibata, Akinobu*; Tsuji, Nobuhiro*

Journal of Materials Research and Technology, 17, p.2690 - 2700, 2022/03

 Times Cited Count:9 Percentile:83.6(Materials Science, Multidisciplinary)

Metastable austenitic steels having ultrafine grained (UFG) microstructures can be fabricated by conventional cold rolling and annealing processes by utilizing the deformation-induced martensitic transformation during cold rolling and its reverse transformation to austenite upon annealing. However, such processes are not applicable when the austenite has high mechanical stability against deformation-induced martensitic transformation, since there is no sufficient amount of martensite formed during cold rolling. In the present study, a two-step cold rolling and annealing process was applied to an Fe-24Ni-0.3C metastable austenitic steel having high mechanical stability. Prior to the cold rolling, a repetitive subzero treatment and reverse annealing treatment were applied. Such a treatment dramatically decreased the mechanical stability of the austenite and greatly accelerated the formation of deformation-induced martensite during the following cold rolling processes. As a result, the grain refinement was significantly promoted, and a fully recrystallized specimen with a mean austenite grain size of 0.5 mm was successfully fabricated, which exhibited both high strength and high ductility.

Journal Articles

Nanoscale relaxation in "Water-in-Salt" and "Water-in-Bisalt" electrolytes

Gonzal$'e$z, M. A.*; Borodin, O.*; Kofu, Maiko; Shibata, Kaoru; Yamada, Takeshi*; Yamamuro, Osamu*; Xu, K.*; Price, D. L.*; Saboungi, M.-L.*

Journal of Physical Chemistry Letters (Internet), 11(17), p.7279 - 7284, 2020/09

 Times Cited Count:16 Percentile:77.33(Chemistry, Physical)

Journal Articles

${it In situ}$ neutron diffraction study on the deformation of a TRIP-assisted multi-phase steel composed of ferrite, austenite and martensite

Lavakumar, A.*; Park, M. H.*; Gao, S.*; Shibata, Akinobu*; Okitsu, Yoshitaka*; Gong, W.; Harjo, S.; Tsuji, Nobuhiro*

IOP Conference Series; Materials Science and Engineering, 580, p.012036_1 - 012036_6, 2019/09

 Times Cited Count:3 Percentile:83.68(Engineering, Mechanical)

Journal Articles

Nuclear moments of the low-lying isomeric $$1^+$$ state of $$^{34}$$Al; Investigation on the neutron $$1p1h$$ excitation across $$N=20$$ in the island of inversion

Xu, Z. Y.*; Heylen, H.*; Asahi, Koichiro*; Boulay, F.*; Daugas, J. M.*; de Groote, R. P.*; Gins, W.*; Kamalou, O.*; Koszor$'u$s, $'A$.*; Lykiardopoupou, M.*; et al.

Physics Letters B, 782, p.619 - 626, 2018/07

AA2018-0159.pdf:0.5MB

 Times Cited Count:7 Percentile:53.6(Astronomy & Astrophysics)

no abstracts in English

Journal Articles

Liquid-like thermal conduction in intercalated layered crystalline solids

Li, B.; Wang, H.*; Kawakita, Yukinobu; Zhang, Q.*; Feygenson, M.*; Yu, H. L.*; Wu, D.*; Ohara, Koji*; Kikuchi, Tatsuya*; Shibata, Kaoru; et al.

Nature Materials, 17(3), p.226 - 230, 2018/03

 Times Cited Count:121 Percentile:96.83(Chemistry, Physical)

Journal Articles

Observation of a $$gamma$$-decaying millisecond isomeric state in $$^{128}$$Cd$$_{80}$$

Jungclaus, A.*; Grawe, H.*; Nishimura, Shunji*; Doornenbal, P.*; Lorusso, G.*; Simpson, G. S.*; S$"o$derstr$"o$m, P.-A.*; Sumikama, Toshiyuki*; Taprogge, J.*; Xu, Z. Y.*; et al.

Physics Letters B, 772, p.483 - 488, 2017/09

 Times Cited Count:8 Percentile:55.37(Astronomy & Astrophysics)

Journal Articles

Polar rotor scattering as atomic-level origin of low mobility and thermal conductivity of perovskite CH$$_{3}$$NH$$_{3}$$PbI$$_{3}$$

Li, B.; Kawakita, Yukinobu; Liu, Y.*; Wang, M.*; Matsuura, Masato*; Shibata, Kaoru; Kawamura, Seiko; Yamada, Takeshi*; Lin, S.*; Nakajima, Kenji; et al.

Nature Communications (Internet), 8, p.16086_1 - 16086_9, 2017/06

 Times Cited Count:81 Percentile:91.64(Multidisciplinary Sciences)

Journal Articles

$$beta$$ decay of semi-magic $$^{130}$$Cd; Revision and extension of the level scheme of $$^{130}$$In

Jungclaus, A.*; Grawe, H.*; Nishimura, Shunji*; Doornenbal, P.*; Lorusso, G.*; Simpson, G. S.*; S$"o$derstr$"o$m, P. A.*; Sumikama, Toshiyuki*; Taprogge, J.*; Xu, Z. Y.*; et al.

Physical Review C, 94(2), p.024303_1 - 024303_8, 2016/08

 Times Cited Count:18 Percentile:77.39(Physics, Nuclear)

Journal Articles

First observation of $$gamma$$ rays emitted from excited states south-east of $$^{132}$$Sn; The $$pi$$ g$$_{9/2}^{-1}$$ $$ otimes$$ $$nu f_{7/2}$$ multiplet of $$^{132}$$In$$_{83}$$

Jungclaus, A.*; Gargano, A.*; Grawe, H.*; Taprogge, J.*; Nishimura, Shunji*; Doornenbal, P.*; Lorusso, G.*; Shimizu, Y.*; Simpson, G. S.*; S$"o$derstr$"o$m, P.-A.*; et al.

Physical Review C, 93(4), p.041301_1 - 041301_6, 2016/04

 Times Cited Count:18 Percentile:77.39(Physics, Nuclear)

Journal Articles

Toward advancement of nuclear data research in the resonance region

Kunieda, Satoshi; Shibata, Keiichi; Fukahori, Tokio; Kawano, Toshihiko*; Paris, M.*; Hale, G.*

JAEA-Conf 2015-003, p.33 - 38, 2016/03

We present recent progress of nuclear data evaluation method in the resolved resonance range. Our multi-channel R-matrix code now includes photon-channel and computational capability of charged-particle elastic scattering. We also present the physical constraint from the theory in the analysis of experimental data. Example analysis results are shown for $$^8$$Be and $$^{17}$$O compound system. Finally, perspectives are discussed toward the advancement of nuclear data in the resonance region including those for medium-heavy nuclei.

Journal Articles

$$beta$$ decay of $$^{129}$$Cd and excited states in $$^{129}$$In

Taprogge, J.*; Jungclaus, A.*; Grawe, H.*; Nishimura, Shunji*; Doornenbal, P.*; Lorusso, G.*; Simpson, G. S.*; S$"o$derstr$"o$m, P.-A.*; Sumikama, Toshiyuki*; Xu, Z. Y.*; et al.

Physical Review C, 91(5), p.054324_1 - 054324_11, 2015/05

 Times Cited Count:24 Percentile:82.61(Physics, Nuclear)

Journal Articles

Covariance of neutron cross sections for $$^{16}$$O through R-matrix analysis

Kunieda, Satoshi; Kawano, Toshihiko*; Paris, M.*; Hale, G. M.*; Shibata, Keiichi; Fukahori, Tokio

Nuclear Data Sheets, 123, p.159 - 164, 2015/01

 Times Cited Count:6 Percentile:42.02(Physics, Nuclear)

The collision matrix in the R-matrix theory is unitary, hence theory brings strong constraints to behavior of the parameters. An unitarity-imposed R-matrix analysis is carried out for $$^{17}$$O system to evaluate $$^{16}$$O neutron cross-sections in the resolved resonance range. Covariance matrices are also estimated both for the cross-sections and angular distributions with a deterministic method. Present results mirror the nature in the theory as well as experimental information.

Journal Articles

Identification of a millisecond isomeric state in $$^{129}$$Cd$$_{81}$$ via the detection of internal conversion and Compton electrons

Taprogge, J.*; Jungclaus, A.*; Grawe, H.*; Nishimura, Shunji*; Xu, Z. Y.*; Doornenbal, P.*; Lorusso, G.*; N$'a$cher, E.*; Simpson, G. S.*; S$"o$derstr$"o$m, P.-A.*; et al.

Physics Letters B, 738, p.223 - 227, 2014/11

 Times Cited Count:23 Percentile:80.23(Astronomy & Astrophysics)

Journal Articles

Measurements of the neutron activation cross sections for Bi and Co at 386 MeV

Yashima, Hiroshi*; Sekimoto, Shun*; Ninomiya, Kazuhiko*; Kasamatsu, Yoshitaka*; Shima, Tatsushi*; Takahashi, Naruto*; Shinohara, Atsushi*; Matsumura, Hiroshi*; Satoh, Daiki; Iwamoto, Yosuke; et al.

Radiation Protection Dosimetry, 161(1-4), p.139 - 143, 2014/10

 Times Cited Count:2 Percentile:16.44(Environmental Sciences)

The neutron activation cross sections up to GeV are important for the neutron dosimetry of the radiation field in high-energy and high-intensity accelerator facilities for a project of intense spallation neutron source. But the evaluation of neutron activation cross section data is not enough above 20 MeV because experimental data are still scarce. This study aimed to measure the neutron activation cross sections of Bi and Co by using a quasi-monoenergetic neutron field. In this symposium, we will present obtained experimental cross section data with the other experimental data (neutron-induced and proton-induced), the calculated data by PHITS code and the evaluated nuclear data.

Journal Articles

Yrast 6$$^+$$ seniority isomers of $$^{136,138}$$Sn

Simpson, G. S.*; Gey, G.*; Jungclaus, A.*; Taprogge, J.*; Nishimura, Shunji*; Sieja, K.*; Doornenbal, P.*; Lorusso, G.*; S$"o$derstr$"o$m, P.-A.*; Sumikama, Toshiyuki*; et al.

Physical Review Letters, 113(13), p.132502_1 - 132502_6, 2014/09

 Times Cited Count:68 Percentile:91.93(Physics, Multidisciplinary)

Journal Articles

"Relative rates method" for evaluating the effect of potential geological environmental change due to uplift/erosion to radionuclide migration of high-level radioactive waste

Ebashi, Takeshi; Kawamura, Makoto*; Inagaki, Manabu*; Koo, Shigeru*; Shibata, Masahiro; Itazu, Toru; Nakajima, Kunihiko*; Miyahara, Kaname; Apted, M. J.*

Materials Research Society Symposium Proceedings, Vol.1665, p.39 - 45, 2014/07

In Japan, the likelihood of uplift/erosion on repository performance and waste isolation can be typically greatly reduced or excluded by careful siting, however, the inability to completely exclude the uplift/erosion scenario may require an analysis of the consequences of such a scenario. For this purpose, an assessment approach has been developed to more realistically treat the effect of uplift/erosion for a hypothetical repository located in sedimentary host rock. A key advantage to this approach is the extrapolation of the geohistory of modern analogue sites to develop credible initial inputs for future volunteer sites that may be poorly characterized at the initial stages of site investigation. In addition, the approach provides a systematic basis for bounding the range of possible evolution in thermal-hydrological-mechanical-chemical conditions of a repository experiencing different uplift/ erosion rates.

Journal Articles

Estimation of neutron cross-sections for $$^{16}$$O up to 5.2 MeV through R-matrix analysis

Kunieda, Satoshi; Kawano, Toshihiko*; Paris, M.*; Hale, G. M.*; Shibata, Keiichi; Fukahori, Tokio

NEA/NSC/DOC(2014)13 (Internet), p.33 - 39, 2014/07

There still remain differences among measured data, which makes the evaluated cross-sections uncertain, and which consequently affects some integral calculation. $$^{16}$$O is one of the important nuclei in the nuclear application, but such kinds of issues appears in elastic-scattering and (n,$$alpha$$) reaction cross-sections. Purpose of this study is to solve those issues as they are common concerns in the world. We present estimated cross sections and their covariance data which are "physically" constrained by the R-matrix theory. The differences between the estimated and the measured cross-sections will be also discussed.

Journal Articles

R-matrix analysis for n + $$^{16}$$O cross-sections up to E$$_{rm n}$$ = 6.0 MeV with covariances

Kunieda, Satoshi; Kawano, Toshihiko*; Paris, M.*; Hale, G. M.*; Shibata, Keiichi; Fukahori, Tokio

Nuclear Data Sheets, 118, p.250 - 253, 2014/04

 Times Cited Count:12 Percentile:62.86(Physics, Nuclear)

Oxygen is one of the most important materials in nuclear applications. However, there are big discrepancies among experimental and evaluated data in $$^{16}$$O($$n,alpha$$) cross section. Also, there are increasing demands for giving uncertainties in evaluated cross section to estimate the margin of integral calculations. We analyzed experimental cross sections with R-matrix theory, and estimated cross sections with their uncertainties. In this analysis, not only the neutron but also an inverse reactions were included. The systematic uncertainties were also considered for each measurement. The resulting cross sections and uncertainties mirror both experimental and theoretical knowledges.

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