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Journal Articles

Advanced analysis technology for new material and product development

Sasaki, Hirokazu*; Nishikubo, Hideo*; Nishida, Shinsuke*; Yamazaki, Satoshi*; Nakasaki, Ryusuke*; Isomatsu, Takemi*; Minato, Ryuichiro*; Kinugawa, Kohei*; Imamura, Akihiro*; Otomo, Shinya*; et al.

Furukawa Denko Jiho, (138), p.2 - 10, 2019/02

no abstracts in English

Journal Articles

Materials and Life Science Experimental Facility (MLF) at the Japan Proton Accelerator Research Complex, 2; Neutron scattering instruments

Nakajima, Kenji; Kawakita, Yukinobu; Ito, Shinichi*; Abe, Jun*; Aizawa, Kazuya; Aoki, Hiroyuki; Endo, Hitoshi*; Fujita, Masaki*; Funakoshi, Kenichi*; Gong, W.*; et al.

Quantum Beam Science (Internet), 1(3), p.9_1 - 9_59, 2017/12

The neutron instruments suite, installed at the spallation neutron source of the Materials and Life Science Experimental Facility (MLF) at the Japan Proton Accelerator Research Complex (J-PARC), is reviewed. MLF has 23 neutron beam ports and 21 instruments are in operation for user programs or are under commissioning. A unique and challenging instrumental suite in MLF has been realized via combination of a high-performance neutron source, optimized for neutron scattering, and unique instruments using cutting-edge technologies. All instruments are/will serve in world-leading investigations in a broad range of fields, from fundamental physics to industrial applications. In this review, overviews, characteristic features, and typical applications of the individual instruments are mentioned.

JAEA Reports

Potassium-Argon (K-Ar) dating for fault gouge samples in the Tono Geoscience Center

Tamura, Hajimu*; Shibata, Kenji*; Takahashi, Naoya; Niwa, Masakazu

JAEA-Testing 2017-001, 52 Pages, 2017/03


It is essential to understand the activity of faults in and around a target area to assess the long-term geosphere stability for geological isolation. Potassium-Argon (K-Ar) dating of fault gouge has been conducted in Tono Geoscience Center as one of the dating technique for faulting. This report includes methods for sample preparation, analyses, and age calculation on the K-Ar dating. This can contribute to an evaluation of calculated K-Ar ages.

Journal Articles

Nitric acid concentration dependence of dicesium plutonium(IV) nitrate formation during solution growth of uranyl nitrate hexahydrate

Nakahara, Masaumi; Kaji, Naoya; Yano, Kimihiko; Shibata, Atsuhiro; Takeuchi, Masayuki; Okano, Masanori; Kuno, Takehiko

Journal of Chemical Engineering of Japan, 46(1), p.56 - 62, 2013/01

 Times Cited Count:1 Percentile:7.24(Engineering, Chemical)

The influence of HNO$$_{3}$$ concentration in the solution on the formation of Cs$$_{2}$$Pu(NO$$_{3}$$)$$_{6}$$ was evaluated in the U crystallization process. The solubility of Cs$$_{2}$$Pu(NO$$_{3}$$)$$_{6}$$ in a uranyl nitrate solution was found to decrease with increasing HNO$$_{3}$$ concentration in the solution. In the U crystallization experiments with the dissolver solution of irradiated fast reactor fuel, Cs$$_{2}$$Pu(NO$$_{3}$$)$$_{6}$$ formed with 6.5 mol/dm$$^{3}$$ HNO$$_{3}$$ concentration in the mother liquor, and the decontamination factor of Cs for the uranyl nitrate hexahydrate crystals was low. Meanwhile, Cs$$_{2}$$Pu(NO$$_{3}$$)$$_{6}$$ did not precipitate with uranyl nitrate hexahydrate crystals under the condition of 4.0 mol/dm$$^{3}$$ HNO$$_{3}$$ concentration in the mother liquor, and Cs could be separated from the uranyl nitrate hexahydrate crystals.

Journal Articles

Salt-free technique for solvent washing process in NEXT process

Sano, Yuichi; Kaji, Naoya; Shibata, Atsuhiro; Takeuchi, Masayuki; Washiya, Tadahiro

Proceedings of International Conference on Toward and Over the Fukushima Daiichi Accident (GLOBAL 2011) (CD-ROM), 7 Pages, 2011/12

Journal Articles

Current status on research and development of uranium crystallization system in advanced aqueous reprocessing of FaCT project

Shibata, Atsuhiro; Kaji, Naoya; Nakahara, Masaumi; Yano, Kimihiko; Tayama, Toshimitsu; Nakamura, Kazuhito; Washiya, Tadahiro; Myochin, Munetaka; Chikazawa, Takahiro*; Kikuchi, Toshiaki*

Proceedings of International Conference on Advanced Nuclear Fuel Cycle; Sustainable Options & Industrial Perspectives (Global 2009) (CD-ROM), p.151 - 157, 2009/09

As a part of FaCT project, Japan Atomic Energy Agency has been developing a U crystallization process for advanced aqueous reprocessing technology in collaboration with Mitsubishi Materials Corporation. We have carried out experimental studies and obtained fundamental data. Continuous operation tests were also carried out by an engineering-scale crystallizer to confirm productivity of the equipment and to investigate non-steady state conditions. The requirements for the U crystallization process in the FaCT project could be achieved except DF of Cs. More detail investigation is under way to settle the process condition without Pu-Cs double salt formation.

Oral presentation

Fundamental test of crystallization process; Evaluation of U solubility in solution of irradiated fuel

Kaji, Naoya; Nakahara, Masaumi; Nakamura, Kazuhito; Shibata, Atsuhiro; Tomita, Yutaka; Washiya, Tadahiro; Kitajima, Takafumi; Koizumi, Tsutomu

no journal, , 

Solubility obtained from the latest crystallization tests using irradiated fuel and the tests implemented before using U or Pu/U are compared with the data showed by Hart. Based on the result, availability of the data to estimate crystallization ratio is considered.

Oral presentation

Fundamental test of crystallization process; Experience on behavior of FPs in crystallization process by using irradiated MOX fuel

Kaji, Naoya; Nakamura, Kazuhito; Nomura, Kazunori; Shibata, Atsuhiro; Yano, Kimihiko; Washiya, Tadahiro; Kitajima, Takafumi; Koizumi, Tsutomu

no journal, , 

For the purpose of obtaining DFs of the short-life FPs by $$gamma$$ analysis in the hot experiment, fundamental test of crystallization process was carried out using Fast Experimental Reactor "JOYO" irradiated fuel. In this experiment, DFs of nuclides analyzed by $$gamma$$ analysis except Cs (Such as Ru-106, Ce-144, Pr-144) and Pu were evaluated to be about 100. It was suggested that there is the condition in which Pu-Cs double salt does not be formed, although DF of Cs had been very low in the past experiments because of forming Pu-Cs double salt.

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