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Journal Articles

Quantification of radicals in aqueous solution by positronium lifetime; An Experiment using a clinical PET scanner

Takyu, Sodai*; Matsumoto, Kenichiro*; Hirade, Tetsuya; Nishikido, Fumihiko*; Akamatsu, Go*; Tashima, Hideaki*; Takahashi, Miwako*; Yamaya, Taiga*

Japanese Journal of Applied Physics, 63(8), p.086003_1 - 086003_8, 2024/08

Positrons and electrons sometimes exist as a bound state, positronium (Ps), in living organisms. The triplet Ps (ortho-Ps) annihilation time represents the ortho-Ps pick-off annihilation lifetime, and it varies depending on the surrounding electron density. The ortho-Ps lifetime may add new biological information to PET scan information. In order to discuss the feasibility of quantifying (free) radicals in vivo by the ortho-Ps lifetime, we used a clinical PET system to make ortho-Ps lifetime measurements in aqueous solutions containing radicals. The results suggested that differences in radical concentrations in aqueous solutions of the order of a few mM could be quantified by the ortho-Ps lifetime if the counting statistic of the positron annihilation events was more than 10$$^{8}$$ events. This concentration was higher than the radical concentration generated in the physiological functions of living organisms.

Journal Articles

Rearrangement of hydrogen bonds in dehydrated raffinose tetrahydrate; A Time-of-flight neutron diffraction study

Kawasaki, Takuro; Takahashi, Miwako*; Kiyanagi, Ryoji; Ohara, Takashi

Acta Crystallographica Section C; Structural Chemistry (Internet), 78(12), p.743 - 748, 2022/12

 Times Cited Count:0 Percentile:0.00(Chemistry, Multidisciplinary)

Journal Articles

SENJU; A New time-of-flight single-crystal neutron diffractometer at J-PARC

Ohara, Takashi; Kiyanagi, Ryoji; Oikawa, Kenichi; Kaneko, Koji; Kawasaki, Takuro; Tamura, Itaru; Nakao, Akiko*; Hanashima, Takayasu*; Munakata, Koji*; Moyoshi, Taketo*; et al.

Journal of Applied Crystallography, 49(1), p.120 - 127, 2016/02

 Times Cited Count:55 Percentile:95.88(Chemistry, Multidisciplinary)

Journal Articles

Instrument design and performance evaluation of a new single crystal neutron diffractometer SENJU at J-PARC

Oikawa, Kenichi; Kawasaki, Takuro; Ohara, Takashi; Kiyanagi, Ryoji; Kaneko, Koji; Tamura, Itaru; Nakamura, Tatsuya; Harada, Masahide; Nakao, Akiko*; Hanashima, Takayasu*; et al.

JPS Conference Proceedings (Internet), 1, p.014013_1 - 014013_5, 2014/03

A new single crystal time-of-flight neutron diffractometer has been installed at BL18 of the Materials and Life Science Experimental Facility of J-PARC. The diffractometer "SENJU" was designed for precise crystal and magnetic structure analyses using a small crystal less than 1.0 mm$$^3$$ under multiple extreme environments such as low-temperature and high-magnetic field. The first neutron beam was delivered to the sample position on March 5, 2012. Subsequently, the hardware and software of SENJU have been checked and confirmed that they worked fine. At the same time, diffraction experiments of several organic and inorganic crystals have been done using NaCl, C12A7, and so on. In these measurements, Bragg reflections in the high-Q region (d-spacing $$<$$ 0.5 ${AA}$) were clearly observed and analyzed successfully. In this presentation, we will show the instrument design and performance evaluation of SENJU in detail.

Journal Articles

Structure of morpholinium tribromoplumbate C$$_{4}$$H$$_{8}$$ONH$$_{2}$$PbBr$$_{3}$$ studied using single-crystal neutron diffraction

Kawasaki, Takuro; Takahashi, Miwako*; Ohara, Takashi*; Tanaka, Ichiro*; Kusaka, Katsuhiro*; Hosoya, Takaaki*; Yamada, Taro*; Kurihara, Kazuo

Journal of the Physical Society of Japan, 81(9), p.094602_1 - 094602_6, 2012/09

 Times Cited Count:7 Percentile:45.79(Physics, Multidisciplinary)

Journal Articles

Current status of a time-of-flight single crystal neutron diffractometer SENJU at J-PARC

Tamura, Itaru; Oikawa, Kenichi; Kawasaki, Takuro; Ohara, Takashi; Kaneko, Koji; Kiyanagi, Ryoji; Kimura, Hiroyuki*; Takahashi, Miwako; Kiyotani, Tamiko*; Arai, Masatoshi; et al.

Journal of Physics; Conference Series, 340, p.012040_1 - 012040_4, 2012/02

 Times Cited Count:11 Percentile:94.26(Physics, Condensed Matter)

Oral presentation

Current status of extreme environment single crystal neutron diffractometer SENJU

Kiyanagi, Ryoji; Ohara, Takashi*; Kawasaki, Takuro; Oikawa, Kenichi; Tamura, Itaru; Kaneko, Koji; Hanashima, Takayasu*; Nakao, Akiko*; Munakata, Koji*; Kimura, Hiroyuki*; et al.

no journal, , 

no abstracts in English

Oral presentation

Development of a new TOF single crystal diffractometer SENJU at J-PARC

Ohara, Takashi; Kiyanagi, Ryoji; Kawasaki, Takuro; Oikawa, Kenichi; Kaneko, Koji; Tamura, Itaru; Nakao, Akiko*; Hanashima, Takayasu*; Munakata, Koji*; Kimura, Hiroyuki*; et al.

no journal, , 

SENJU is a new single crystal time-of-flight neutron diffractometer installed at BL18 of J-PARC. SENJU is designed for precise crystal and magnetic structure analyses under multiple extreme environments such as low-temperature, high-pressure and high-magnetic field, and also designed for diffraction measurements of small single crystals less than 1.0 mm$$^{3}$$ in volume. We have successfully achieved structure analysis of a laboratory X-ray size (0.1 mm$$^{3}$$) single organic crystal, measurement and visualization of a complex-shape diffuse scattering pattern and measurement of higher order magnetic reflections in high-Q region (Q$$>$$16${AA}$ $$^{-1}$$) by using SENJU. Those results show that the performance of SENJU is as we expected.

Oral presentation

Installation of additional detectors and T0 chopper on the single crystal neutron diffractometer, SENJU

Kiyanagi, Ryoji; Ohara, Takashi; Kawasaki, Takuro; Oikawa, Kenichi; Kaneko, Koji; Tamura, Itaru; Nakao, Akiko*; Hanashima, Takayasu*; Munakata, Koji*; Moyoshi, Taketo*; et al.

no journal, , 

The single crystal diffractometer, SENJU, which just became open for users, is the instrument designed to perform structure analyses under multiple extreme conditions even with tiny samples. Additional six detectors and T0 chopper were installed in order to improve the data collection efficiency and the background noise arises from the burst neutron. The solid angle covarage increased by 1.2 with the six new detectors, and significant reduction of the background noises were confirmed especially on the detectors at highest and lowest angles.

Oral presentation

Crystal structures and phase transitions of the Methylammonium Tin Halide Perovskites

Fujihisa, Yui*; Takahashi, Miwako*; Hagihara, Masato; Torii, Shuki*; Kamiyama, Takashi*; Ohara, Takashi; Noda, Yukio*

no journal, , 

Oral presentation

Quantum PET; Positron lifetime measurement for biomedical engineering applications

Takyu, Sodai*; Matsumoto, Kenichiro*; Hirade, Tetsuya; Nishikido, Fumihiko*; Akamatsu, Go*; Tashima, Hideaki*; Takahashi, Miwako*; Yamaya, Taiga*

no journal, , 

no abstracts in English

Oral presentation

Single crystal neutron diffractometer under extreme condition

Tamura, Itaru; Oikawa, Kenichi; Takahashi, Miwako*; Kawasaki, Takuro*; Kimura, Hiroyuki*; Kiyanagi, Ryoji*; Ohara, Takashi; Kaneko, Koji; Kiyotani, Tamiko*; Arai, Masatoshi; et al.

no journal, , 

no abstracts in English

Oral presentation

A New single crystal neutron diffractometer SENJU at J-PARC

Oikawa, Kenichi; Kaneko, Koji; Tamura, Itaru; Ohara, Takashi; Kawasaki, Takuro; Kimura, Hiroyuki*; Noda, Yukio*; Takahashi, Miwako*; Kiyotani, Tamiko*; Kiyanagi, Ryoji*; et al.

no journal, , 

A new single crystal neutron diffractometer SENJU is now under construction at a high pace in MLF at J-PARC. SENJU will realize precise structure analysis under the combined extreme conditions such as high-magnetic field and low temperature. The construction will be completed at the end of 2010 fiscal year, and has aimed at the first beam acceptance before the summer of 2011. In the presentation, detailed instrument specs will be introduced, and a concrete sample environment etc. will be described.

Oral presentation

Crystal structure of C$$_{4}$$H$$_{8}$$ONH$$_{2}$$-PbBr$$_{3}$$ by neutron and X-ray diffraction experiments

Kawasaki, Takuro; Takahashi, Miwako; Ohara, Takashi*; Oshima, Kenichi*; Kusaka, Katsuhiro*; Tanaka, Ichiro*; Hosoya, Takaaki*; Yamada, Taro*; Kurihara, Kazuo; Niimura, Nobuo*

no journal, , 

Oral presentation

A New time-of-flight single crystal diffractometer SENJU at J-PARC

Oikawa, Kenichi; Ohara, Takashi*; Kiyanagi, Ryoji; Kawasaki, Takuro; Tamura, Itaru; Kaneko, Koji; Nakamura, Tatsuya; Sakasai, Kaoru; Nakao, Akiko*; Hanashima, Takayasu*; et al.

no journal, , 

SENJU, named after the thousand armed Goddess of Mercy, is a single crystal time-of-flight Laue diffractometer proposed to the MLF at J-PARC. The diffractometer is dedicated for precise crystal and magnetic structure analyses under the combined extreme conditions using a small sample less than 1 $$mm^3$$. TOF-Laue technique coupled with wide area 2D detectors enables the efficient measurements and improves the completeness of the data. A WLSF-type scintillator detector developed for iBIX was modified to meet the requirements of SENJU. Although the construction schedule has been delayed because of the earthquake, on-beam commissioning will start in 2012.

Oral presentation

Crystal and electronic structures of organic-inorganic hybrid material C$$_{4}$$H$$_{8}$$ONH$$_{2}$$-PbBr$$_{3}$$

Kawasaki, Takuro; Takahashi, Miwako*; Oshima, Kenichi*; Ohara, Takashi*; Tanaka, Ichiro*; Kusaka, Katsuhiro*; Hosoya, Takaaki*; Kurihara, Kazuo; Niimura, Nobuo*; Yamada, Taro*

no journal, , 

no abstracts in English

Oral presentation

Current status of a single crystal neutron diffractometer SENJU

Kawasaki, Takuro; Oikawa, Kenichi; Ohara, Takashi*; Kiyanagi, Ryoji; Tamura, Itaru; Kaneko, Koji; Nakamura, Tatsuya; Sakasai, Kaoru; Nakao, Akiko*; Hanashima, Takayasu*; et al.

no journal, , 

no abstracts in English

Oral presentation

Commissioning and current status of the extreme environment single crystal neutron diffractometer SENJU

Kiyanagi, Ryoji; Ohara, Takashi*; Kawasaki, Takuro; Oikawa, Kenichi; Tamura, Itaru; Kaneko, Koji; Hanashima, Takayasu*; Nakao, Akiko*; Munakata, Koji*; Kimura, Hiroyuki*; et al.

no journal, , 

no abstracts in English

Oral presentation

Crystal structure analysis of Raffinose-pentahydrate using single crystal neutron diffraction

Kawasaki, Takuro; Takahashi, Miwako*; Ohara, Takashi*; Kiyanagi, Ryoji; Oikawa, Kenichi; Tamura, Itaru; Kaneko, Koji; Nakao, Akiko*; Hanashima, Takayasu*; Munakata, Koji*

no journal, , 

no abstracts in English

Oral presentation

Current status of structure analyses on SENJU

Kiyanagi, Ryoji; Ohara, Takashi*; Kawasaki, Takuro; Oikawa, Kenichi; Tamura, Itaru; Kaneko, Koji; Nakao, Akiko*; Hanashima, Takayasu*; Munakata, Koji*; Kimura, Hiroyuki*; et al.

no journal, , 

no abstracts in English

27 (Records 1-20 displayed on this page)