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Journal Articles

Outlining zircon growth in a granitic pluton using 3D cathodoluminescence patterns, U-Pb age, titanium concentration, and Th/U; Implications for the magma chamber process of Okueyama granite, Kyushu, Japan

Yuguchi, Takashi*; Ito, Daichi*; Yokoyama, Tatsunori; Sakata, Shuhei*; Suzuki, Satoshi*; Ogita, Yasuhiro; Yagi, Koshi*; Imura, Takumi*; Motai, Satoko*; Ono, Takeshi*

Lithos, 440-441, p.107026_1 - 107026_14, 2023/03

 Times Cited Count:0 Percentile:0.02(Geochemistry & Geophysics)

We propose a new method for elucidating zircon growth in granitic plutons, based on variations in three-dimensional 3D cathodoluminescence (CL) patterns, U-Pb ages, titanium concentration, and Th/U ratios. We focused on the zircon growth processes in the Okueyama granite (OKG) in central Kyushu, Japan, to obtain interpretations of magma chamber processes that result in the formation of granitic plutons. The OKG consists of three lithofacies: biotite granite (BG), hornblende granite (HG), and hornblende granodiorite (HGD). To determine the 3D internal structure and growth pattern of a zircon crystal, we performed CL observations for multi-sections of the samples. Simultaneously, we also determined the zircon U-Pb age and titanium concentration of the center sections of the samples. The 3D distribution of the oscillatory zoning can be used to determine the crystal nucleus. The simultaneous determination of zircon U-Pb ages and Ti concentrations of the granite samples indicates the time-temperature (t-T) history of granitic magma before its solidification. The t-T histories of the BG, HG, and HGD represented similar cooling behaviors within the magma chamber: rapid cooling from the zircon crystallization temperature to the closure temperature of the biotite K-Ar system between 16 Ma and 10 Ma. The variations in the Th/U ratios against temperature also demonstrate a different trend at the boundary of approximately 670 $$^{circ}$$C. Fractional crystallization in the magma chamber progressed significantly at temperatures above 670 $$^{circ}$$C; below 670 $$^{circ}$$C, crystallization progressed slowly, indicating only minimal changes in the magma composition. The variations in the Th/U ratio against temperature in the BG, HG, and HGD portrayed common tendencies, indicating the same behavior in the progression of fractional crystallization among the three lithofacies, which in turn, represented the same behavior within the entire magma chamber.

Journal Articles

Evaluation of suitability of zircon as standard materials based on thermal history; Example of the Wassogatake Formation in Ishikawa Prefecture

Nagata, Mitsuhiro; Nakajima, Toru; Fukuda, Shoma; Sueoka, Shigeru; Yagi, Koshi*; Yokoyama, Tatsunori

Fisshion, Torakku Nyusureta, (36), p.9 - 13, 2023/00

Zircon U-Pb and fission track (FT) dating and moonstone (sanidine) K-Ar dating of the Wassogatake Formation in the southern part of Hakusan City, Ishikawa Prefecture were carried out as part of the search for zircon standard materials for dating. The weighted average U-Pb dates obtained from the three samples are ca. 21.9-21.7 Ma, overlapping within the uncertainty range. Zircon FT and moonstone K-Ar dates were obtained younger ages from some samples. In addition, the track lengths of the three samples are short. Based on the above results, the zircons of the Wassogatake Formation are effective for the high closure temperature dating method (e.g., U-Pb dating), but are not suitable for the low closure temperature dating method (e.g., FT dating).

Journal Articles

K-Ar geochronology for hydrothermal K-feldspar within plagioclase in a granitic pluton; Constraints on timing and thermal condition for hydrothermal alteration

Yuguchi, Takashi*; Yagi, Koshi*; Sasao, Eiji; Nishiyama, Tadao*

Heliyon (Internet), 7(4), p.e06750_1 - e06750_9, 2021/04

 Times Cited Count:1 Percentile:10.87(Multidisciplinary Sciences)

Our methodology and interpretations provide new insight for K-Ar geochronology in hydrothermal microcline within altered plagioclase in a granitic pluton. Our methodology employs a two-step separation process consisting of (1) plagioclase extraction from the rock sample and (2) separation of the hydrothermal microcline from the plagioclase, giving precise determination of microcline powders in K-Ar geochronology. This tighter constraint should provide the ability to better unravel thermal and age histories in granite subject to multi-step alteration processes and complex thermal histories.

Journal Articles

Simultaneous determination of zircon U-Pb age and titanium concentration using LA-ICP-MS for crystallization age and temperature

Yuguchi, Takashi*; Ishibashi, Kozue*; Sakata, Shuhei*; Yokoyama, Tatsunori; Ito, Daichi*; Ogita, Yasuhiro; Yagi, Koshi*; Ono, Takeshi*

Lithos, 372-373, p.105682_1 - 105682_9, 2020/11

 Times Cited Count:3 Percentile:14.2(Geochemistry & Geophysics)

Simultaneous determination of zircon U-Pb age and titanium concentration for a single analysis spot gives both the crystallization age and temperature. The crystallization age and temperature pairs in granitic zircons map the time-temperature ($$t-T$$) path of granitic magma before its solidification. In laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) analysis, it is challenging to quantitatively analyse a low level of titanium concentration. This study employed two approaches using a Quadrupole mass spectrometer equipped with a collision/reaction cell (CRC). The methods were applied to zircon samples of the Kurobegawa granite (KRG), the Okueyama granite (OKG), the Toki granite (TKG), and the Tono plutonic complex (TPC) and provided U-Pb ages and titanium concentrations consistent with previous studies. The crystallization ages and temperatures collected from individual analysis spots of zircon samples in the KRG, OKG, TKG, and TPC are plotted in the $$t-T$$ diagrams and enable us to characterize the rapid cooling paths at thermal conditions of zircon crystallization at the sampling sites.

Journal Articles

K-Ar ages of an andesitic parallel dike swarm in the Takane area, Takayama City, Gifu Prefecture, Central Japan

Niwa, Masakazu; Ueki, Tadamasa*; Hoshi, Hiroyuki*; Sugisaki, Yuichi*; Yagi, Koshi*; Tozawa, Terumasa

Chishitsugaku Zasshi, 126(9), p.543 - 548, 2020/09

A large number of paleomagnetic and chronological studies have contributed to the elucidation of the early Miocene clockwise rotation of Southwest Japan associated with the major opening of back-arc basins of the Japan Sea. Paleomagnetic data from an andesitic parallel dike swarm in the Takane area, Takayama City, Gifu Prefecture, Central Japan, were previously reported, showing the easterly deflection of the observed magnetization direction compared to an early Miocene expected paleomagnetic direction. This must represent the clockwise rotation during the opening of the Japan Sea, if the dike swarm was intruded before the opening event. Here, we report new K-Ar hornblende ages from an andesite dike of the dike swarm. These ages are statistically indistinguishable, indicating emplacement of the dike swarm before the clockwise rotation.

Journal Articles

Role of micropores, mass transfer, and reaction rate in the hydrothermal alteration process of plagioclase in a granitic pluton

Yuguchi, Takashi*; Shobuzawa, Kaho*; Ogita, Yasuhiro*; Yagi, Koshi*; Ishibashi, Masayuki; Sasao, Eiji; Nishiyama, Tadao*

American Mineralogist, 104(4), p.536 - 556, 2019/04

 Times Cited Count:17 Percentile:72.93(Geochemistry & Geophysics)

This study describes the plagioclase alteration process with a focus on the role of micropores, mass transfer and reaction rate in the Toki granitic pluton, central Japan. The plagioclase alteration process involves albitization, K-feldspathization, and the formation of illite, calcite, fluorite and epidote. Such secondary minerals of hydrothermal origin in plagioclase within granitic rocks record the chemical characteristics of the hydrothermal fluid. Our results highlight (1) the nature of micropores such as distribution and volume in plagioclase, (2) the reaction nature of plagioclase alteration inferred by petrography and chemistry, (3) the physical conditions including alteration age and temperature, (4) the sequential variations of the fluid chemistry and (5) the mass transfer rate and reaction rate in the plagioclase alteration.

Journal Articles

Formation age and cooling history of Kojaku granite

Sueoka, Shigeru; Shimada, Koji; Ishimaru, Tsuneari; Danhara, Toru*; Iwano, Hideki*; Yagi, Koshi*

Chigaku Zasshi, 127(6), p.795 - 803, 2018/12

no abstracts in English

Journal Articles

Cooling and denudation history of the Tsuruga body of Kojaku granite, southwest Japan, constrained from multi-system thermochronology

Sueoka, Shigeru; Umeda, Koji; Yasue, Kenichi; Niwa, Masakazu; Shimada, Koji; Ishimaru, Tsuneari; Danhara, Toru*; Iwano, Hideki*; Yagi, Koshi*

Chigaku Zasshi, 125(2), p.201 - 219, 2016/04

We applied multi-system thermochronology to the Tsuruga body of the Kojaku granite to constrain the cooling/denudation history of the Tsuruga area. Based on the thermochronometric results and other data, we reconstructed the cooling and denudation histories of the Tsuruga body as below: (1) the Tsuruga body intruded at c.a. 68 Ma at the depth of 4-5 km, (2) rapidly cooled down to c.a. 200$$^{circ}$$C by heat conduction within a few million years or less, and (3) slowly cooled due to peneplanation during the Cenozoic. This cooling/denudation history is consistent with the observations that cataclasite and fault gouge are dominant in the crush zones of the Tsuruga body, that similar slow cooling histories over the Cenozoic are estimated in the surrounding areas based on thermochronometric ages, and that the amount of denudation in the last few million years in the Tsuruga area is inferred at less than several hundred meters from the elevations of the uplifted peneplains.

Journal Articles

High pressure high temperature experiments using multi-anvil device; Method and facility

Utsumi, Wataru; Funakoshi, Kenichi*; Yagi, Naoto*; Urakawa, Satoru*; Otaka, Osamu*; Katsura, Tomoo*; Irifune, Tetsuo*; Inoue, Toru*; Uchida, Takeyuki*

Ganseki Kobutsu Kagaku, 30(2), p.100 - 101, 2001/03

no abstracts in English

Oral presentation

Role of micropores, mass transfer and reaction rate in hydrothermal alteration process of plagioclase in a granite

Yuguchi, Takashi*; Shobuzawa, Kaho*; Ogita, Yasuhiro*; Yagi, Koshi*; Ishibashi, Masayuki; Sasao, Eiji; Nishiyama, Tadao*

no journal, , 

This study presents the plagioclase alteration process with a focus on the role of micropores, mass transfer and reaction rate in the Toki granitic pluton, central Japan. The plagioclase alteration process involves an albitization, K-feldspathization and the formation of illite, calcite, fluorite and epidote. Such secondary minerals of hydrothermal origin in plagioclase within granitic rocks record the chemical characteristics of the hydrothermal fluid. Our results highlight (1) the nature of micropores such as distribution and volume in plagioclase, (2) the reaction nature of plagioclase alteration inferred by petrography and chemistry, (3) the physical conditions including alteration age and temperature, (4) the sequential variations of the fluid chemistry and (5) the mass transfer rate and reaction rate in the plagioclase alteration.

Oral presentation

Simultaneous determination of zircon U-Pb age and titanium concentration using LA-ICP-MS; Case studies of the Kurobegawa granite, the Toki granite and the Tono plutonic complex

Ishibashi, Kozue*; Sakata, Shuhei*; Yokoyama, Tatsunori; Ito, Daichi*; Ogita, Yasuhiro; Yagi, Koshi*; Ono, Takeshi*; Yuguchi, Takashi*

no journal, , 

no abstracts in English

Oral presentation

Simultaneous determination of zircon U-Pb age and titanium concentration using LA-ICP-MS; A Case study of the Okueyama granite, Kyusyu, Japan

Ito, Daichi*; Ishibashi, Kozue*; Sakata, Shuhei*; Yokoyama, Tatsunori; Ogita, Yasuhiro; Yagi, Koshi*; Ono, Takeshi*; Yuguchi, Takashi*

no journal, , 

no abstracts in English

Oral presentation

Zircon growth process in granitic pluton by 3D cathodoluminescence patterns, U-Pb ages, titanium concentration, and Th/U ratios; Case study of the Okueyama granite, Kyushu, Japan

Yuguchi, Takashi*; Ito, Daichi*; Yokoyama, Tatsunori; Sakata, Shuhei*; Suzuki, Satoshi*; Ogita, Yasuhiro; Yagi, Koshi*; Imura, Takumi*; Motai, Satoko*; Ono, Takeshi*

no journal, , 

This study proposes a new method for elucidating zircon growth processes in the Okueyama granitic pluton, Kyushu, Japan. Our method, which combines 3D growth patterns, U-Pb ages, titanium concentration, and Th/U ratios, contributes to the petrology and mineralogy to understand the growth of zircon crystals within a magma chamber. Simultaneous determination of zircon U-Pb ages and titanium concentrations for the granite gives the variations in the temporal and thermal conditions during zircon growth, thus, developing a t-T history of the granitic magma before its solidification. The simultaneous determination of zircon U-Pb ages and Ti concentrations in the granite also enable us to associate the Th/U ratio with the crystallization temperature. Therefore, the decrease in zircon Th/U ratios as decreasing the temperature indicates the progression of fractional crystallization as the cooling of the magma chamber.

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