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Journal Articles

Effect of water activity on the mechanical glass transition and dynamical transition of bacteria-solute systems

Kawai, Kiyoshi*; Sogabe, Tomochika*; Nakagawa, Hiroshi; Yamada, Takeshi*; Koseki, Shigenobu*

Journal of Food Engineering, 375, p.112066_1 - 112066_9, 2024/08

 Times Cited Count:1 Percentile:0.00(Engineering, Chemical)

The purpose of this study was to clarify effect of glycerol and glucose on the mechanical glass transition and dynamical transition of freeze-dried bacteria at various water activity (aw)-conditions. From the water sorption isotherm, it was noted that the water content at each aw and monolayer water content were higher in the order of glycerol, glucose, non-added samples. Effect of temperature on the mean square displacement (MSD) of atoms in the samples was investigated by incoherent elastic neutron scattering. The MSD increased gradually with an increase in temperature depending on the aw and added solute. From the linear fitting, three dynamical transition temperatures (low-, middle- and high-Tds) were determined. The Couchman-Karasz model suggested that the added solute and bacteria were not completely miscible.

Journal Articles

Neutron reflectivity study on the adsorption layer of polyethylene grown on Si substrate

Shimokita, Keisuke*; Yamamoto, Katsuhiro*; Miyata, Noboru*; Shibata, Motoki*; Nakanishi, Yohei*; Arakawa, Masato*; Takenaka, Mikihito*; Kida, Takumitsu*; Tokumitsu, Katsuhisa*; Tanaka, Ryo*; et al.

Langmuir, 40(30), p.15758 - 15766, 2024/07

 Times Cited Count:0 Percentile:0.00(Chemistry, Multidisciplinary)

Journal Articles

Quasielastic neutron scattering probing H$$^{-}$$ dynamics in the H$$^{-}$$ conductors LaH$$_{3-2x}$$O$$_{x}$$

Tamatsukuri, Hiromu; Fukui, Keiga*; Iimura, Soshi*; Honda, Takashi*; Tada, Tomofumi*; Murakami, Yoichi*; Yamaura, Junichi*; Kuramoto, Yoshio*; Sagayama, Hajime*; Yamada, Takeshi*; et al.

Physical Review B, 107(18), p.184114_1 - 184114_8, 2023/05

 Times Cited Count:1 Percentile:18.74(Materials Science, Multidisciplinary)

Journal Articles

Cement solidification technology for waste

Haga, Kazuko*; Shibuya, Kazutoshi*; Osugi, Takeshi; Yamada, Kazuo*

Haikibutsu Shigen Junkan Gakkai-Shi, 33(6), p.435 - 447, 2022/11

Cement solidification technology has been widely applied to waste stabilization and treatment because cement is not only relatively stable in physical and chemical properties after hardening, but also an inexpensive and easy-to-handle solidification material and treatment facilities are simple and economical. As the current status of cement solidification treatment technologies for wastes, this paper describes a study on cement solidification of wastes from the Fukushima Daiichi Nuclear Power Plant accident, the current status of cement solidification treatment of low-level radioactive wastes, and cement solidification technology for incinerated ash, and review previous research results on immobilization and leaching mechanisms of heavy metals in cement solidified products.

Journal Articles

Effect of water activity on the mechanical glass transition and dynamical transition of bacteria

Sogabe, Tomochika*; Nakagawa, Hiroshi; Yamada, Takeshi*; Koseki, Shigenobu*; Kawai, Kiyoshi*

Biophysical Journal, 121(20), p.3874 - 3882, 2022/10

 Times Cited Count:3 Percentile:34.16(Biophysics)

The purpose of this study was to clarify the glass transition behavior of bacteria ($$Cronobacter sakazakii$$) as a function of water activity ($$a_{rm w}$$). Mechanical relaxation was investigated at 298 K, and the mechanical $$a_{rm wc}$$ ($$a_{rm w}$$ at which mechanical glass transition occurs at 298 K) was determined to be 0.667. Temperature-dependency of mean square displacement was investigated by inelastic neutron scattering. From the linear fitting, two dynamical transition temperatures (low and high-$$T_{rm ds}$$) were determined. There was a minor effect of $$a_{rm w}$$ on the low-$$T_{rm ds}$$ except for the anhydrous sample. The high-$$T_{rm ds}$$ largely increased with the decrease in $$a_{rm w}$$. The dynamical $$a_{rm wc}$$determined by high-$$T_{rm ds}$$ (0.688) was slightly higher than the mechanical $$a_{rm wc}$$ because of the difference in the measurement time-scale. The high-$$T_{rm ds}$$ was converted to the glass transition temperature ($$T_{rm g}$$), and anhydrous $$T_{rm g}$$ was estimated to be 411 K. Bacterial inactive-active transition was discussed according to the glass transition behavior.

Journal Articles

Rotation of complex ions with ninefold hydrogen coordination studied by quasielastic neutron scattering and first-principles molecular dynamics calculations

Omasa, Yoshinori*; Takagi, Shigeyuki*; Toshima, Kento*; Yokoyama, Kaito*; Endo, Wataru*; Orimo, Shinichi*; Saito, Hiroyuki*; Yamada, Takeshi*; Kawakita, Yukinobu; Ikeda, Kazutaka*; et al.

Physical Review Research (Internet), 4(3), p.033215_1 - 033215_9, 2022/09

Journal Articles

Revealing the ion dynamics in Li$$_{10}$$GeP$$_{2}$$S$$_{12}$$ by quasi-elastic neutron scattering measurements

Hori, Satoshi*; Kanno, Ryoji*; Kwon, O.*; Kato, Yuki*; Yamada, Takeshi*; Matsuura, Masato*; Yonemura, Masao*; Kamiyama, Takashi*; Shibata, Kaoru; Kawakita, Yukinobu

Journal of Physical Chemistry C, 126(22), p.9518 - 9527, 2022/06

 Times Cited Count:8 Percentile:56.77(Chemistry, Physical)

Journal Articles

Evaluation of sample cell materials for aqueous solutions used in quasi-elastic neutron scattering measurements

Tominaga, Taiki*; Sahara, Masae*; Kawakita, Yukinobu; Nakagawa, Hiroshi; Yamada, Takeshi*

Journal of Applied Crystallography, 54(6), p.1631 - 1640, 2021/12

 Times Cited Count:5 Percentile:54.32(Chemistry, Multidisciplinary)

Journal Articles

Structural changes in pH-responsive gelatin/hydroxypropyl methylcellulose phthalate blends aimed at drug-release systems

Nogami, Satoshi*; Kadota, Kazunori*; Uchiyama, Hiromasa*; Arima-Osonoi, Hiroshi*; Iwase, Hiroki*; Tominaga, Taiki*; Yamada, Takeshi*; Takata, Shinichi; Shibayama, Mitsuhiro*; Tozuka, Yuichi*

International Journal of Biological Macromolecules, 190, p.989 - 998, 2021/11

 Times Cited Count:9 Percentile:51.10(Biochemistry & Molecular Biology)

Journal Articles

Experimental analysis on dynamics of liquid molecules adjacent to particles in nanofluids

Hashimoto, Shunsuke*; Nakajima, Kenji; Kikuchi, Tatsuya*; Kamazawa, Kazuya*; Shibata, Kaoru; Yamada, Takeshi*

Journal of Molecular Liquids, 342, p.117580_1 - 117580_8, 2021/11

 Times Cited Count:3 Percentile:18.93(Chemistry, Physical)

Quasi-elastic neutron scattering (QENS) and pulsed-field-gradient nuclear magnetic resonance (PFGNMR) analyses of a nanofluid composed of silicon dioxide (SiO$$_{2}$$) nanoparticles and a base fluid of ethylene glycol aqueous solution were performed. The aim was to elucidate the mechanism increase in the thermal conductivity of the nanofluid above its theoretical value. The obtained experimental results indicate that SiO$$_{2}$$ particles may decrease the self-diffusion coefficient of the liquid molecules in the ethylene glycol aqueous solution because of their highly restricted motion around these nanoparticles. At a constant temperature, the thermal conductivity increases as the self-diffusion coefficient of the liquid molecules decreases in the SiO$$_{2}$$ nanofluids.

Journal Articles

Dynamics of water in a catalyst layer of a fuel cell by quasielastic neutron scattering

Ito, Kanae; Yamada, Takeshi*; Shinohara, Akihiro*; Takata, Shinichi; Kawakita, Yukinobu

Journal of Physical Chemistry C, 125(39), p.21645 - 21652, 2021/10

 Times Cited Count:8 Percentile:41.96(Chemistry, Physical)

Journal Articles

Dynamical response of transition-edge sensor microcalorimeters to a pulsed charged-particle beam

Okumura, Takuma*; Azuma, Toshiyuki*; Bennet, D. A.*; Caradonna, P.*; Chiu, I.-H.*; Doriese, W. B.*; Durkin, M. S.*; Fowler, J. W.*; Gard, J. D.*; Hashimoto, Tadashi; et al.

IEEE Transactions on Applied Superconductivity, 31(5), p.2101704_1 - 2101704_4, 2021/08

 Times Cited Count:1 Percentile:7.76(Engineering, Electrical & Electronic)

A superconducting transition-edge sensor (TES) microcalorimeter is an ideal X-ray detector for experiments at accelerator facilities because of good energy resolution and high efficiency. To study the performance of the TES detector with a high-intensity pulsed charged-particle beam, we measured X-ray spectra with a pulsed muon beam at the Japan Proton Accelerator Research Complex (J-PARC) in Japan. We found substantial temporal shifts of the X-ray energy correlated with the arrival time of the pulsed muon beam, which was reasonably explained by pulse pileup due to the incidence of energetic particles from the initial pulsed beam.

Journal Articles

Deexcitation dynamics of muonic atoms revealed by high-precision spectroscopy of electronic $$K$$ X rays

Okumura, Takuma*; Azuma, Toshiyuki*; Bennet, D. A.*; Caradonna, P.*; Chiu, I. H.*; Doriese, W. B.*; Durkin, M. S.*; Fowler, J. W.*; Gard, J. D.*; Hashimoto, Tadashi; et al.

Physical Review Letters, 127(5), p.053001_1 - 053001_7, 2021/07

 Times Cited Count:15 Percentile:77.46(Physics, Multidisciplinary)

We observed electronic $$K$$X rays emitted from muonic iron atoms using a superconducting transition-edge-type sensor microcalorimeter. The energy resolution of 5.2 eV in FWHM allowed us to observe the asymmetric broad profile of the electronic characteristic $$K$$$$alpha$$ and $$K$$$$beta$$ X rays together with the hypersatellite $$K$$$$alpha$$ X rays around 6 keV. This signature reflects the time-dependent screening of the nuclear charge by the negative muon and the $$L$$-shell electrons, accompanied by electron side-feeding. Assisted by a simulation, this data clearly reveals the electronic $$K$$- and $$L$$-shell hole production and their temporal evolution during the muon cascade process.

Journal Articles

Nonmagnetic-magnetic transition and magnetically ordered structure in SmS

Yoshida, Shogo*; Koyama, Takehide*; Yamada, Haruhiko*; Nakai, Yusuke*; Ueda, Koichi*; Mito, Takeshi*; Kitagawa, Kentaro*; Haga, Yoshinori

Physical Review B, 103(15), p.155153_1 - 155153_5, 2021/04

 Times Cited Count:1 Percentile:5.36(Materials Science, Multidisciplinary)

Journal Articles

Position dependency of the scattered intensity in the time-of-flight backscattering spectrometer DNA

Matsuura, Masato*; Yamada, Takeshi*; Tominaga, Taiki*; Kobayashi, Makoto*; Nakagawa, Hiroshi; Kawakita, Yukinobu

JPS Conference Proceedings (Internet), 33, p.011068_1 - 011068_6, 2021/03

The position dependence of the scattered intensity in the time-of-flight backscattering spectrometer DNA was investigated. A periodic structure for both vertical (pixel) and horizontal (PSD) directions was observed. The solar slit and over-bending of an analyzer crystal is discussed as a possible origin of the modulation in the intensity. We have developed software program for the systematic correction of the position-dependent intensity and offset energy for the elastic peak. This corrects the deviation from the true scattering intensity and improve the quality of the data, which includes the energy resolution.

Journal Articles

Quartz cell for a backscattering spectrometer

Tominaga, Taiki*; Kawakita, Yukinobu; Nakagawa, Hiroshi; Yamada, Takeshi*; Shibata, Kaoru

JPS Conference Proceedings (Internet), 33, p.011086_1 - 011086_5, 2021/03

BB2019-1956.pdf:0.78MB

We developed a quartz double cylindrical sample cell optimized for a backscattering neutron spectrometer, especially for BL02 (DNA), MLF in J-PARC. A quartz glass tube, with one end closed, is shaved to obtain a wall thickness of 0.55 mm. The inner tube is properly centered using a protrusion into the outer tube such that the interstice between the outer and inner tubes keeps constant. This quartz cell can be used for samples that should not be in contact with the aluminum surface. We verified cell's background effect between the quartz cell and Al cell by QENS measurements using D$$_{2}$$O buffer. The elastic intensity profiles of the buffer in a low Q region were identical between both quartz cell and Al cell (A1070). In a high Q region, however, the profiles were different caused by the first sharp diffraction peak of quartz glass. For this region the data should be analyzed by consideration of absorption correction and diffraction in individual thickness of quartz cell.

Journal Articles

Position-encoded automatic cell elevator for BL02, J-PARC MLF

Tominaga, Taiki*; Kobayashi, Makoto*; Yamada, Takeshi*; Matsuura, Masato*; Kawakita, Yukinobu; Kasai, Satoshi*

JPS Conference Proceedings (Internet), 33, p.011095_1 - 011095_5, 2021/03

BB2019-1955.pdf:1.33MB

A vertical movement type of sample changer for the neutron spectrometer BL02, J-PARC MLF was developed for our top-loading type cryostat. The sample changer, termed as "PEACE", can control reproducibility of the irradiated position using guides made of polyether ether ketone. The variation between the background scattering profiles of three sample positions was found to be less than plus minus 1.6%. This result is reasonable, considering the deviation of sample position of less than plus minus 0.3 mm from the vertical axis.

Journal Articles

Dating of buried wood logs and fragments for high resolution reconstruction of landslide histories; Case studies in the Japanese Alps region in the historical times

Yamada, Ryuji*; Kimura, Takashi*; Kariya, Yoshihiko*; Sano, Masaki*; Tsushima, Akane*; Li, Z.*; Nakatsuka, Takeshi*; Kokubu, Yoko; Inoue, Kimio*

Sabo Gakkai-Shi, 73(5), p.3 - 14, 2021/01

We discuss the applicability of dating methods for determining landslide chronologies in relation to the type of samples and the sampling location. Case studies are carried out with fossil wood samples buried in the colluvial soil of large-scale landslides occurred in two areas of the Japanese Alps region. Ages are determined by accelerator mass spectrometry radiocarbon dating and dendrochronological analysis using the oxygen isotope composition of tree ring cellulose. Most of ages for Dondokosawa rock avalanche are concordant with the period of AD 887 Ninna (Goki-Shichido) earthquake. Ages for Ohtsukigawa debris avalanche are not concentrated in a specific period. In order to obtain accurate age of large-scale landslide, utilizing buried large diameter tree trunk or branches with the good preservation condition has a lot of advantages because it allows us to compare the landslide chronology with historical records of heavy rainfall and large earthquakes.

Journal Articles

Structural investigation of sulfonated polyphenylene ionomers for the design of better performing proton-conductive membranes

Shiino, Keisuke*; Otomo, Toshiya; Yamada, Takeshi*; Arima, Hiroshi*; Hiroi, Kosuke; Takata, Shinichi; Miyake, Jumpei*; Miyatake, Kenji*

ACS Applied Polymer Materials (Internet), 2(12), p.5558 - 5565, 2020/11

 Times Cited Count:27 Percentile:76.66(Materials Science, Multidisciplinary)

Journal Articles

Nanoscale relaxation in "Water-in-Salt" and "Water-in-Bisalt" electrolytes

Gonzal$'e$z, M. A.*; Borodin, O.*; Kofu, Maiko; Shibata, Kaoru; Yamada, Takeshi*; Yamamuro, Osamu*; Xu, K.*; Price, D. L.*; Saboungi, M.-L.*

Journal of Physical Chemistry Letters (Internet), 11(17), p.7279 - 7284, 2020/09

 Times Cited Count:22 Percentile:79.54(Chemistry, Physical)

172 (Records 1-20 displayed on this page)