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Journal Articles

Neutron diffraction study of the crystal and magnetic structures of antiferromagnetic manganese deuteride at high temperatures and high pressures

Machida, Akihiko*; Saito, Hiroyuki*; Aoki, Katsutoshi*; Komatsu, Kazuki*; Hattori, Takanori; Sano, Asami; Funakoshi, Kenichi*; Machida, Shinichi*; Sato, Toyoto*; Orimo, Shinichi*

Physical Review B, 111(22), p.224413_1 - 224413_6, 2025/06

 Times Cited Count:1

The crystal and magnetic structures of antiferromagnetic Mn deuterides formed by hydrogenating Mn metal at high temperature and high pressure, fcc $$gamma$$-MnDx and hcp $$epsilon$$-MnDx, were investigated by in-situ neutron powder diffraction. Deuterium atoms partially occupied the octahedral interstitial positions of the fcc and hcp metal lattices. The site occupancies increased rapidly with decreasing temperature from $$sim$$700 to $$sim$$450 K and remained down to 300 K. N$'{e}$el temperature of 543(10) K was determined for $$gamma$$-MnD$$_{0.34}$$. For $$epsilon$$-MnD$$_{0.62}$$, saturation magnetic moment and N$'{e}$el temperature were determined to be 0.82(1) $$mu_B$$ and 347(3) K, respectively. The N$'{e}$el temperatures determined for $$gamma$$-MnD$$_{0.34}$$ and $$epsilon$$-MnD$$_{0.62}$$ are consistent with those predicted by the respective Slater-Pauling curves proposed in previous studies. The updated N$'{e}$el temperatures provide insights into the development of more accurate Slater-Pauling curves based on electronic band structure calculations.

Journal Articles

A New metal extraction method using fluorous solvents

Ueda, Yuki; Micheau, C.; Motokawa, Ryuhei

Fuain Kemikaru, 54(5), p.53 - 60, 2025/05

no abstracts in English

Journal Articles

None

Kumada, Takayuki; Iwahara, Daisuke*

Isotope News, (798), p.26 - 27, 2025/04

no abstracts in English

Journal Articles

Residual stress measurement and lifetime evaluation of railway axles by neutron scattering technology

Hu, F.-F.*; Qin, T.-Y.*; Ao, N.*; Xu, P. G.; Su, Y. H.; Parker, J. D.*; Shinohara, Takenao; Shobu, Takahisa; Kang, G.-Z.*; Ren, M.-M.; et al.

Journal of Traffic and Transportation Engineering, 25(2), p.75 - 93, 2025/04

Journal Articles

Ordered graphane nanoribbons synthesized via high-pressure diels-alder polymerization of 2,2'-bipyrazine

Li, F.*; Tang, X.*; Fei, Y.*; Zhang, J.*; Liu, J.*; Lang, P.*; Che, G.*; Zhao, Z.*; Zheng, Y.*; Fang, Y.*; et al.

Journal of the American Chemical Society, 147(17), p.14054 - 14059, 2025/04

 Times Cited Count:1 Percentile:0.00(Chemistry, Multidisciplinary)

We synthesized a crystalline graphane nanoribbon (GANR) via pressure-induced polymerization of 2,2'-bipyrazine (BPZ). By performing Rietveld refinement of in situ neutron diffraction data, nuclear magnetic resonance spectroscopy, infrared spectra, and theoretical calculation, we found that BPZ experienced Diels-Alder polymerization between the $$pi$$ $$cdots$$ $$pi$$ stacked aromatic rings, and formed extended boat-GANR structures with exceptional long-range order. The unreacted -C=N- groups bridge the two ends of the boat, and ready for further functionalization. The GANR has a bandgap of 2.25 eV, with booming photoelectric response ($$I_{rm on}$$/$$I_{rm off}$$ =18.8). Our work highlights that the high-pressure topochemical polymerization is a promising method for the precise synthesis of graphane with specific structure and desired properties.

Journal Articles

Neutron spectroscopy study on crystalline electric field excitations in NdB$$_4$$

Yamauchi, Hiroki; Metoki, Naoto; Watanuki, Ryuta*; Hong, T.*; Fernandez-Baca, J. A.*; Hagihara, Masato; Masuda, Takatsugu*; Yoshizawa, Hideki*; Ito, Shinichi*

Journal of the Physical Society of Japan, 94(5), p.054705_1 - 054705_8, 2025/04

Journal Articles

Simulation study on dose and LET of neutron irradiation for biological experiments using spallation, reactor, and compact neutron sources

Sweet, M.*; Mishima, Kenji*; Harada, Masahide; Kurita, Keisuke; Iikura, Hiroshi; Tasaki, Seiji*; Kikuchi, Norio*

Quantum Beam Science (Internet), 9(2), p.11_1 - 11_17, 2025/04

Neutron beam, being electrically neutral and highly penetrating, offers unique advantages for irradiation of biological species such as plants, seeds, and microorganisms. We comprehensively investigated the potential of neutron irradiation for inducing genetic mutations using simulations of J-PARC BL10, JRR-3 TNRF, and KUANS for spallation, reactor, and compact neutron sources.

Journal Articles

Evaluation of uranium-233 neutron capture cross section in keV region

Otsuka, Naohiko*; Tada, Kenichi; Cabellos, O.*; Iwamoto, Osamu

Annals of Nuclear Energy, 212, p.110977_1 - 110977_9, 2025/03

 Times Cited Count:2 Percentile:0.00(Nuclear Science & Technology)

The uranium-233 neutron capture cross section between 3 keV and 1 MeV was evaluated considering the recent new alpha-value measurement performed at the Los Alamos National Laboratory LANCE facility. The obtained capture cross section is systematically lower than the capture cross section in the JENDL-5 library and the reduction is close to 50% around 20 keV. The newly evaluated cross section was validated against 166 criticality experiments chosen from the ICSBEP handbook by performing Monte Carlo neutron transport calculation with the JENDL-5 library, and slight reduction of the chi-square value was achieved by adoption of the newly evaluated capture cross section.

Journal Articles

Magnetic and quadrupole coupling emerging in NdB$$_4$$ with geometrically frustrated orthogonal antiferromagnetic dimer

Metoki, Naoto; Yamauchi, Hiroki; Hagihara, Masato; Watanuki, Ryuta*; Kawamura, Seiko; Kofu, Maiko*; Nakajima, Kenji; Matsuda, Masaaki*

Physical Review B, 111(10), p.104424_1 - 104424_9, 2025/03

 Times Cited Count:0 Percentile:0.00(Materials Science, Multidisciplinary)

Inelastic neutron scattering experiments were carried out to understand the unusual successive order in NdB$$_4$$ with the frustrated Shatry-Sutherland (SS) lattice. The pseudo-quartet with $$|pm frac{5}{2}rangle$$ and $$|pm frac{7}{2}rangle$$ splits into four levels in the magnetically ordered states. The spectra can be explained with the on-site magnetic interaction $$langle J_x rangle J_x$$, the coupling of $$J_x$$ with quadrupole $$O_{zx}$$, and the uniaxial crystalline electric field. The $$f$$-electron states reproduce the temperature dependences of the in-plane moment $$m_perp=langle J_x rangle$$ which is the primary order parameter, and a weakly induced $$m_c=langle J_z rangle$$ as the secondary order parameter. The magnetic-quadrupole coupling emerges and play essential role under the geometrical frustration, where the Heisenberg interactions are cancelled out.

Journal Articles

Transverse asymmetry of individual $$gamma$$ rays in the $$^{139}$$La($$overrightarrow{n},gamma$$)$$^{140}$$La reaction

Okuizumi, Mao*; Auton, C. J.*; Endo, Shunsuke; Fujioka, Hiroyuki*; Hirota, Katsuya*; Ino, Takashi*; Ishizaki, Kohei*; Kimura, Atsushi; Kitaguchi, Masaaki*; Koga, Jun*; et al.

Physical Review C, 111(3), p.034611_1 - 034611_6, 2025/03

 Times Cited Count:0 Percentile:0.00(Physics, Nuclear)

Journal Articles

Neutron resonance absorption imaging fully utilizing neutron energies from 1 eV to 100 keV

Tsuchikawa, Yusuke; Kai, Tetsuya; Parker, J.*; Matsumoto, Yoshihiro*; Shinohara, Takenao

Scientific Reports (Internet), 15, p.7687_1 - 7687_8, 2025/03

 Times Cited Count:1 Percentile:85.83(Multidisciplinary Sciences)

A neutron resonance absorption imaging technique to visualize two-dimensional distributions with element discrimination has been developed at the Materials and Life Science Experimental Facility of the Japan Proton Accelerator Research Complex. We measured neutron transmission spectra from 1 eV to 100 keV while rotating a sample containing iron, zirconium, nickel, molybdenum, and aluminum rods. The distributions of hafnium (impurity of zirconium) and molybdenum were clearly obtained by a straightforward analysis using the most prominent resonances. Then an analysis using multiple resonances of each element simultaneously was performed finding that the accuracy of elemental identification was improved, and iron and nickel distributions became clearer. However, these analysis methods sometimes have difficulties in the case of overlapping materials since a resonance shape can be deteriorated by those of other materials. Such an example was demonstrated with the case of iron and nickel. To overcome the issue and aiming for further improvement, we proposed a method to fit the transmission spectrum in a wide range assuming the existence of possible elements, successfully visualizing both the distributions of the sample metals and those of hafnium and manganese (impurities of zirconium and iron). The newly introduced analysis technique will contribute to the establishment of a standard analytical procedure for general users of the facility.

Journal Articles

None

Nankawa, Takuya

Isotope News, (797), p.16 - 17, 2025/02

no abstracts in English

Journal Articles

Concurrent ${it operando}$ neutron imaging and diffraction analysis revealing spatial lithiation phase evolution in an ultra-thick graphite electrode

Strobl, M.*; Baur, M. E.*; Samothrakitis, S.*; Molamud, F.*; Zhang, X.*; Tung, P. K. M.*; Schmidt, S.*; Woracek, R.*; Lee, J.*; Kiyanagi, Ryoji; et al.

Advanced Energy Materials, p.2405238_1 - 2405238_9, 2025/01

 Times Cited Count:0

Journal Articles

J-PARC proton beam irradiation facility plan

Meigo, Shinichiro

Kasokuki, 21(4), p.333 - 344, 2025/01

For the study of material damage under the beam irradiation circumstance of accelerator-driven systems (ADS), the JAEA had planned to construct a TEF-T using J-PARC Linac 400-MeV proton beams and the LBE spallation target. The task force for evaluating partitioning and transmutation technology in the MEXT recommended that the facility be considered to maximize the advantages of using Linac to meet users' various needs. The proton irradiation facility, a successor of TEF-T, is planned to be constructed for 1) Material irradiation examinations, 2) Semiconductor soft-error examinations using spallation neutrons, 3) Medical RI production, and 4) Proton beam applications for space use. A user community was established in 2022 to incorporate user input as a more attractive facility. In this paper, the present design status of the facility is described.

Journal Articles

Theory of the spin Seebeck effect influenced by crystal-field excitations in Tb$$_3$$Fe$$_5$$O$$_{12}$$

Mori, Michiyasu; Tomasello, B.*; Ziman, T.*

Physical Review B, 111(1), p.014407_1 - 014407_12, 2025/01

 Times Cited Count:0 Percentile:0.00(Materials Science, Multidisciplinary)

Journal Articles

Multiple metamagnetic transitions in the helical antiferromagnet CeVGe$$_{3}$$

Jin, H.*; Choi, E. S.*; Wu, H.-C.*; Curro, N. J.*; Nawa, Kazuhiro*; Sato, Taku*; Kiyanagi, Ryoji; Ohara, Takashi; Klavins, P.*; Taufour, V.*

Physical Review B, 111(3), p.035103_1 - 035103_7, 2025/01

 Times Cited Count:0 Percentile:0.00(Materials Science, Multidisciplinary)

Journal Articles

Tensile properties of irradiated modified 316 stainless steel (PNC316) at slow strain rates

Yano, Yasuhide; Miyazawa, Takeshi; Tanno, Takashi; Akasaka, Naoaki; Yoshitake, Tsunemitsu; Kaito, Takeji; Otsuka, Satoshi

Journal of Nuclear Science and Technology, 8 Pages, 2025/00

 Times Cited Count:0 Percentile:0.00(Nuclear Science & Technology)

The effects of strain rate on tensile properties of irradiated modified 316 stainless steel (PNC316) claddings were investigated. PNC316 claddings were irradiated at the experimental fast reactor Joyo using CRT402 control rod assembly at 400$$^{circ}$$C up to 25 dpa. Post-irradiation ring tensile tests were carried out at strain rates of 3.3$$times$$10$$^{-6}$$, 3.3$$times$$10$$^{-7}$$ and 3.3$$times$$10$$^{-8}$$ s$$^{-1}$$ at a test temperature of 350$$^{circ}$$C. The results showed no obvious dependence of all strain rates on tensile properties, although a slight decrease in total elongation was observed at the slowest strain rate of 3.3$$times$$10$$^{-8}$$ s$$^{-1}$$. In addition, only a part of fracture surface at the slowest strain rate showed intergranular type region in the inner surface area, although the grain boundary separation occurred on inner surfaces near the fracture region at all strain rates. It is suggested that presence of a high content of helium near the inner surfaces would be related to the fracture behavior.

Journal Articles

Strong low-energy rattling modes enabled liquid-like ultralow thermal conductivity in a well-ordered solid

Liu, P.-F.*; Li, X.*; Li, J.*; Zhu, J.*; Tong, Z.*; Kofu, Maiko*; Nirei, Masami; Xu, J.*; Yin, W.*; Wang, F.*; et al.

National Science Review, 11(12), p.nwae216_1 - nwae216_10, 2024/12

 Times Cited Count:13 Percentile:94.32(Multidisciplinary Sciences)

Journal Articles

High-precision powder diffraction experiments under high pressure at the J-PARC PLANET beamline and recent results; Observation of hydrogen bond symmetrization in ice

Hattori, Takanori; Komatsu, Kazuki*

Nihon Genshiryoku Gakkai-Shi ATOMO$$Sigma$$, 66(12), p.618 - 622, 2024/12

The high-pressure neutron diffractometer PLANET is the first beamline dedicated to high-pressure neutron experiments in Japan. It was constructed at the Materials and Life Science Experimental Facility (MLF) in the Japan Proton Accelerator Research Complex (J-PARC) located at Tokai-mura in Ibaraki Prefecture. Energy-dispersive data measurement using pulsed neutrons, state-of-the-art optical instruments, and a high-pressure device enable us to analyze the structure of crystals, liquids, and glasses over a wide range of pressure and temperature with unprecedented accuracy. In this paper, we will show how this has been achieved and introduce the recently published results on the symmetrization of hydrogen bonds in ice.

Journal Articles

Tracer diffusion coefficient measurements on NASICON-type Lithium-ion conductor LAGP using neutron radiography between 25$$^{circ}$$C and 500$$^{circ}$$C

Takagi, Honoka*; Yabutsuka, Takeshi*; Hayashida, Hirotoshi*; Song, F.; Kai, Tetsuya; Shinohara, Takenao; Kurita, Keisuke; Iikura, Hiroshi; Yamamoto, Norio*; Nakajima, Minoru*; et al.

Solid State Ionics, 417, p.116716_1 - 116716_7, 2024/12

 Times Cited Count:2 Percentile:0.00(Chemistry, Physical)

3538 (Records 1-20 displayed on this page)