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Journal Articles

Separation technique using column chromatography for safeguards verification analysis of uranium and plutonium in highly-active liquid waste by isotope dilution mass spectrometry

Yamamoto, Masahiko; Taguchi, Shigeo; Horigome, Kazushi; Kuno, Takehiko

Proceeding IAEA Symposium on International Safeguards; Building Future Safeguards Capabilities (Internet), 8 Pages, 2018/11

In this study, the single-column extraction chromatographic separation has been developed for analysis of U and Pu in highly active liquid waste by isotope dilution mass spectrometry (IDMS). The commercially available TEVA$$^{textregistered}$$ resin is selected as an extraction chromatography resin. The U is chromatographically separated from fission products (FP) elements by nitric acid while Pu(IV) is adsorbed on the resin. After that, Pu is eluted by reducing to Pu(III). The method has been successfully achieved the separation with yielding the enough recovery and sufficient decontamination factors for subsequent IDMS analysis. The column dose rate after the FP removal is decreased to the background. The analytical results obtained by the developed method are in a good agreement with those of the conventional method. It provides simple and rapid separation and expected that the method can be applied to join IAEA/Japan on-site analytical laboratory.

Journal Articles

Preparation of solid phase extraction cartridges for trace analysis of radionuclides

Asai, Shiho; Saito, Kyoichi*

Biomedical Research on Trace Elements, 28(1), p.1 - 10, 2017/04

Radionuclides are commonly determined with radiometry and mass spectrometry. For $$gamma$$-emitting nuclides, the activities can be measured without chemical separation due to the strong penetration ability. In contrast, the measurements of alpha and beta-emitting nuclides are generally associated with tedious and time-consuming chemical separation procedures to remove concomitants. Thus, an adsorbent that achieves rapid separation is desirable to reduce separation time and workload. Our research team has developed compact cartridge-type solid phase extraction materials which enable to facilitate separation procedures. In this review, basic separation performances of the developed cartridges were overviewed along with two application examples to radionuclide-containing samples.

Oral presentation

Study on the analysis method for radioactive strontium in environmental samples by ICP-MS with online solid phase extraction

Yanagisawa, Kayo*; Kuwata, Haruka*; Hagiwara, Hiroki; Uezu, Yasuhiro

no journal, , 

no abstracts in English

Oral presentation

Application of the rapid analytical method for $$^{90}$$Sr to environmental samples with online solid phase extraction/ICP-MS

Hagiwara, Hiroki; Yanagisawa, Kayo*; Kuwata, Haruka*; Tanabe, Tsutomu; Uezu, Yasuhiro

no journal, , 

no abstracts in English

Oral presentation

Quantitative analysis of humic substances dissolved in sedimentary groundwater in Japanese coastal areas

Terashima, Motoki; Endo, Takashi*; Kimuro, Shingo; Miyakawa, Kazuya

no journal, , 

no abstracts in English

Oral presentation

Development of the desalting method for total alpha activity determination, 1; Introduction and overview of the desalting performance test by solid-phase extraction

Hosokawa, Tomoaki*; Fujiwara, Hideki*; Kamoshida, Shuichi*; Anzai, Kiyoshi*; Nakano, Masanao; Koike, Yuko; Yamada, Ryohei; Nagaoka, Mika

no journal, , 

no abstracts in English

Oral presentation

Development of the desalting method for total alpha activity determination, 2; Result of the desalting performance test by solid-phase extraction

Nakano, Masanao; Koike, Yuko; Yamada, Ryohei; Nagaoka, Mika; Hosokawa, Tomoaki*; Fujiwara, Hideki*; Kamoshida, Shuichi*; Anzai, Kiyoshi*

no journal, , 

no abstracts in English

Oral presentation

Development of simultaneous analytical method for $$^{93}$$Zr and $$^{93}$$Mo based on solid phase extraction combined with ICP-MS/MS, 1; Sequential chemical separation of Zr and Mo from Nb

Furuse, Takahiro; Do, V. K.; Aita, Rena; Ota, Yuki; Murakami, Erina; Tomitsuka, Tomohiro; Sano, Yuichi; Akimoto, Yuji*; Endo, Tsubasa*; Katayama, Atsushi; et al.

no journal, , 

In order to simplify the analysis of $$^{93}$$Zr and $$^{93}$$Mo in radioactive waste from conventional radiation measurement, we have considered analysis method combining solid-phase extraction and ICP-MS/MS. In this presentation, we report the results of a study on sequential chemical separation of Zr and Mo from Nb and sample matrix using ZR resin as a solid-phase extraction resin.

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