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論文

Visualization of phase distribution in lead-bismuth eutectic during one-dimensional solidification process

伊藤 大介*; 佐藤 博隆*; 齊藤 泰司*; Parker, J. D.*; 篠原 武尚; 甲斐 哲也

Journal of Visualization, 22(5), p.889 - 895, 2019/06

 被引用回数:1 パーセンタイル:7.22(Computer Science, Interdisciplinary Applications)

Solidification process of lead-bismuth eutectic (LBE) is one of the key phenomena to prevent flow channel blockage accident in an LBE-cooled accelerator-driven system. However, the solidification of liquid metal cannot be observed optically and it is difficult to detect noninvasively. In this study, the one-dimensional solidification process of the LBE was visualized by pulsed neutron transmission imaging. Neutrons have higher transmittivity to the LBE than X-ray and neutron transmission spectrum of the LBE sample can be obtained by pulsed neutron imaging technique. The solid and liquid phases of the LBE were identified during the solidification process by the presence or absence of Bragg edge in the measured neutron transmission spectrum, and the transient behavior of the solid-liquid interface could be visualized. In addition, the characteristic spatial distribution of the crystalline structure was found in Bragg-edge transmission image after the solidification.

論文

中性子透過率スペクトル測定を利用した新しい中性子散乱実験

大場 洋次郎*; 諸岡 聡; 佐藤 博隆*; 佐藤 信浩*; 井上 倫太郎*; 杉山 正明*

波紋, 26(4), p.170 - 173, 2016/11

Based on the time-of-light (TOF) technique, new generation pulsed neutron sources enable novel neutron scattering experiments. Using small-angle neutron scattering (SANS) at the pulsed neutron sources, simultaneous measurements of SANS and Bragg edge transmission can be performed. From the SANS profiles, the precipitates and inclusions in metals and alloys are characterized, while the Bragg edge transmission spectra give crystallographic information about the matrix. This is a powerful tool for quantitative characterization of the microstructures in the metals and alloys. The neutron transmission experiments have potential for further development. Magnetic Bragg edge transmission analysis will be useful for magnetic materials. These new neutron scattering techniques enhance the usability and flexibility of neutron scattering experiments.

論文

Magnetic scattering in the simultaneous measurement of small-angle neutron scattering and Bragg edge transmission from steel

大場 洋次郎*; 諸岡 聡; 大石 一城*; 佐藤 信浩*; 井上 倫太郎*; 足立 望*; 鈴木 淳市*; 土山 聡宏*; Gilbert, E. P.*; 杉山 正明*

Journal of Applied Crystallography, 49(5), p.1659 - 1664, 2016/10

 被引用回数:13 パーセンタイル:66.23(Chemistry, Multidisciplinary)

Pulsed neutron sources enable the simultaneous measurement of small-angle neutron scattering (SANS) and Bragg edge transmission. This simultaneous measurement is useful for microstructural characterization in steel. Since most steels are ferromagnetic, magnetic scattering contributions should be considered in both SANS and Bragg edge transmission analyses. An expression for the magnetic scattering contribution to Bragg edge transmission analysis has been derived. The analysis using this expression was applied to Cu steel. The ferrite crystallite size estimated from this Bragg edge transmission analysis with the magnetic scattering contribution was larger than that estimated using conventional expressions. This result indicates that magnetic scattering has to be taken into account for quantitative Bragg edge transmission analysis. In the SANS analysis, the ratio of magnetic to nuclear scattering contributions revealed that the precipitates consist of body-centered cubic Cu$$_{0.7}$$Fe$$_{0.3}$$ and pure Cu, which probably has 9R structure including elastic strain and vacancies. These results show that effective use of the magnetic scattering contribution allows detailed analyses of steel microstructure.

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