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Journal Articles

Effects of silicon, carbon and molybdenum additions on IASCC of neutron irradiated austenitic stainless steels

Nakano, Junichi; Miwa, Yukio; Koya, Toshio; Tsukada, Takashi

Journal of Nuclear Materials, 329-333(Part1), p.643 - 647, 2004/08

 Times Cited Count:7 Percentile:46.83(Materials Science, Multidisciplinary)

To study effects of minor elements on the irradiation assisted stress corrosion cracking (IASCC), high purity Type 304 and 316 stainless steels (SSs) were fabricated and added minor elements, Si or C. After neutron irradiation to 3.5$$times$$10$$^{25}$$n/m$$^{2}$$ (E$$>$$1MeV), the slow strain rate tests (SSRT) for the irradiated specimens was conducted in oxygeneted high purity water at 561 K. Fracture surface of the specimens was examined using the scanning electron microscope (SEM) after the SSRT. Fraction of intergranular stress corrosion cracking (IGSCC) on the fracture surface after the SSRT increased with netron fluence. Suppression of irradiation hardening and increase of peiod to SCC fracture as benefitical effects of the additional elements, Si or Mo, were not observed obviously. In high purity SS added C, fraction of IGSCC was the smallest in the all SSs, although irraidiation hardening level was the largest in the all SSs. Addition of C suppressed the susceptibility to IGSCC.

JAEA Reports

Development of facility for in-situ observation during slow strain rate test for irradiated materials

Nakano, Junichi; Tsukada, Takashi; Tsuji, Hirokazu; Terakado, Shogo; Koya, Toshio; Endo, Shinya

JAERI-Tech 2003-092, 54 Pages, 2004/01

JAERI-Tech-2003-092.pdf:14.05MB

Irradiation assisted stress corrosion cracking (IASCC) is a degradation phenomenon caused by synergy of neutron radiation, aqueous environment and stress on in-core materials, and it is an important issue in accordance with increase of aged light water reactors. Isolating crack initiation stage from crack growth stage is very useful for the evaluation of the IASCC behavior. Hence facility for in-situ observation during slow strain rate test (SSRT) for irradiated material was developed. As performance demonstrations of the facility, tensile test with in-situ observation and SSRT without observation were carried out using unirradiated type 304 stainless steel in 561 K water at 9 MPa. The following were confirmed from the results. (1) Handling, observation and recording of specimen can be operated using manipulators in the hot cell. (2) In-situ observation can be performed in pressurized high temperature water and flat sheet type specimen is suitable for the in-situ observation. (3) Test condition can be kept constantly and data can be obtained automatically for long test period.

Journal Articles

Irradiation Assisted Stress Corrosion Cracking (IASCC)

Tsukada, Takashi

Zairyo To Kankyo, 52(2), p.66 - 72, 2003/02

Irradiation assisted stress corrosion cracking (IASCC) is a potential failure mode suffered by the core-components of austenitic stainless steels in the aged light-water reactor (LWR), which is the intergranular type cracking caused by synergistic effects of neutron/gamma radiation and chemical environment. Effects of radiation on the materials and high-temperature water are discussed in this paper to understand IASCC phenomenon from a mechanistic viewpoint. It is essential to elucidate the radiation-induced microcompositional and microstructural changes in the alloy for mechanistic and predictive investigations of IASCC. Although grain boundary segregations of alloying and impurity elements are significant factors affecting IASCC, it has been considered that the radiation-induced microstructural and mechanical changes of materials play critical roles in IASCC. For mechanistic understanding of IASCC, further fundamental research works with experimental and theoretical approaches are needed. Efforts directed to the researches at the Japan Atomic Energy Research Institute are also described.

Journal Articles

Evaluation of corrosion behavior of ion irradiated stainless steel using atomic force microscope

Nemoto, Yoshiyuki; Miwa, Yukio; Tsuji, Hirokazu; Tsukada, Takashi

Dai-12-Kai MAGDA Konfarensu (Oita) Koen Rombunshu, p.191 - 196, 2003/00

Development and research about analytical method for the study of corrosion behavior of austenitic stainless steel after irradiation was conducted from the point of view for basic study of IASCC (Irradiation Assisted Stress Corrosion Cracking). Ion irradiations were conducted with several irradiation conditions these were irradiation temperature, radiation damage, the contents of helium (He) implantation. AFM (Atomic Force Microscope) was used to evaluate surface condition of irradiated specimens after corrosion procedure. Corrosion condition was developed to obtain good surface condition of irradiated specimens to evaluate corrosion behavior by AFM. It was succeeded and corrosion behavior at inside of grains and grain boundaries of irradiated specimens was obtained. EBSP (Electron Backscatter Diffraction Pattern) was used to evaluate relation of corrosion behavior with grain boundary character. Moreover, relations of corrosion behavior with irradiation condition were discussed.

JAEA Reports

Development of analytical method for microstructure observation of oxide film on stainless steel

Nemoto, Yoshiyuki; Miwa, Yukio; Tsukada, Takashi; Kikuchi, Masahiko; Tsuji, Hirokazu

JAERI-Tech 2001-079, 25 Pages, 2001/12

JAERI-Tech-2001-079.pdf:6.76MB

Development and research about analytical method for the study of oxide film on austenitic stainless steel had been conducted from the point of view for basic study of IASCC (Irradiation Assisted Stress Corrosion Cracking). Nickel plating and copper plating had been compared as the oxide film protection while the fabrication for cross sectional observation. And thin film specimens for microstructural observation were fabricated using FIB (Focused Ion Beam) technique. Microstructure of oxide film on stainless steel had been observed with FE-TEM (Field Emission gun - Transmission Electron Microscope), and the chemical composition was analyzed with EDS (Energy dispersed X-ray Spectrometer). The oxide film had been formed in high pressure (8MPa) and high temperature (288$$^{circ}C$$) water, contains saturated oxygen. The thickness of oxide film was about 1$$mu$$m as maximum. Micro grains of Fe oxide with 100nm in diameter were formed in the oxide film. On the boundary with alloy, there was about 10nm thickness of passive film formed with Cr oxide.

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