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Journal Articles

Correlation between locally deformed structure and oxide film properties in austenitic stainless steel irradiated with neutrons

Chimi, Yasuhiro; Kitsunai, Yuji*; Kasahara, Shigeki; Chatani, Kazuhiro*; Koshiishi, Masato*; Nishiyama, Yutaka

Journal of Nuclear Materials, 475, p.71 - 80, 2016/07

 Times Cited Count:11 Percentile:69.28(Materials Science, Multidisciplinary)

To elucidate the mechanism of irradiation-assisted stress corrosion cracking (IASCC) in high-temperature water for neutron-irradiated austenitic stainless steels (SSs), the locally deformed structures, the oxide films formed on the deformed areas, and their correlation were investigated. Tensile specimens made of irradiated 316L SSs were strained 0.1%-2% at room temperature or at 563 K, and the surface structures and crystal misorientation among grains were evaluated. The strained specimens were immersed in high-temperature water, and the microstructures of the oxide films on the locally deformed areas were observed. The appearance of visible step structures on the specimens' surface depended on the neutron dose and the applied strain. The surface oxides were observed to be prone to increase in thickness around grain boundaries (GBs) with increasing neutron dose and increasing local strain at the GBs. No penetrative oxidation was observed along GBs or along surface steps.

Oral presentation

Relationship between crack growth rates and locally deformed structures in irradiated 316L stainless steels

Chimi, Yasuhiro; Kasahara, Shigeki; Nishiyama, Yutaka; Seto, Hitoshi*; Kitsunai, Yuji*; Koshiishi, Masato*

no journal, , 

In order to understand irradiation-assisted stress corrosion cracking (IASCC) growth behavior, crack growth tests using compact tension (CT) specimens made of neutron-irradiated 316L stainless steels (SSs) were performed in simulated BWR environments (at $$sim$$288$$^{circ}$$C). Moreover, microstructures of deformed areas were observed by transmission electron microscope (TEM) after straining tensile specimens made of neutron-irradiated 316L SSs. As a result, for lower neutron dose than $$<sim$$1.9 dpa, the crack growth rates (CGRs) show effective environmental mitigation and the deformed structures show tangling of dislocations. On the other hand, for higher neutron dose than $$>sim$$2.7 dpa, the CGRs show small environmental mitigation and the deformed structures consist mainly of dislocation channels. From the relationship between CGRs and deformed structures, mechanisms on IASCC growth will be discussed.

Oral presentation

Evaluation of crack growth rates and microstructures near crack tip of neutron-irradiated 316L stainless steels in simulated BWR environment

Chimi, Yasuhiro; Kasahara, Shigeki*; Nishiyama, Yutaka; Seto, Hitoshi*; Chatani, Kazuhiro*; Kitsunai, Yuji*; Koshiishi, Masato*

no journal, , 

In order to understand irradiation-assisted stress corrosion cracking (IASCC) growth behavior, crack growth tests in simulated BWR water conditions (at $$sim$$563 K) were performed using neutron-irradiated specimens made of 316L stainless steels, and the oxide film properties and locally deformed structures near the crack tip have been investigated by transmission electron microscopy (TEM). When electrochemical corrosion potential (ECP) of the materials was lowered by deaeration and hydrogen injection into feed water, apparent suppression of oxidation inside the cracks was observed as well as suppression of the crack growth rate (CGR). In the presentation, the TEM results of the locally deformed structures along the cracks are also reported, and the relation among the CGR, oxide film properties, and locally deformed structures is discussed.

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