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論文

High-density nanoprecipitates and phase reversion via maraging enable ultrastrong yet strain-hardenable medium-entropy alloy

Kwon, H.*; Sathiyamoorthi, P.*; Gangaraju, M. K.*; Zargaran, A.*; Wang, J.*; Heo, Y.-U.*; Harjo, S.; Gong, W.; Lee, B.-J.*; Kim, H. S.*

Acta Materialia, 248, p.118810_1 - 118810_12, 2023/04

https://doi.org/10.1016/j.actamat.2023.118810
 被引用回数：33 パーセンタイル：99.25(Materials Science, Multidisciplinary)

Maraging steels, known for ultrahigh strength and good fracture toughness, derive their superior properties from lath martensite structure with high-density nanoprecipitates. In this work, we designed a novel Fe-based medium-entropy alloy with a chemical composition of Fe$$_{60}$$Co$$_{25}$$Ni$$_{10}$$Mo$$_5$$ in atomic% by utilizing the characteristics of the maraging steels. By a single-step aging of only 10 min at 650 $$^{circ}$$C, the alloy showed microstructures consisting of a very high number density of (Fe, Co, Ni)$$_7$$Mo$$_6$$-type nanoprecipitates in lath martensite structure and reverted FCC phase, which led to ultrahigh yield strength higher than 2 GPa. This work demonstrates a novel direction to produce strong and ductile materials by expanding the horizons of material design with the aid of high-entropy concept and overcoming the limits of conventional materials.

論文

Work hardening behavior of hot-rolled metastable Fe$$_{50}$$Co$$_{25}$$Ni$$_{10}$$Al$$_{5}$$Ti$$_{5}$$Mo$$_{5}$$ medium-entropy alloy; In situ neutron diffraction analysis

Kwon, H.*; Harjo, S.; 川崎 卓郎; Gong, W.; Jeong, S. G.*; Kim, E. S.*; Sathiyamoorthi, P.*; 加藤 秀実*; Kim, H. S.*

Science and Technology of Advanced Materials, 23(1), p.579 - 586, 2022/00

https://doi.org/10.1080/14686996.2022.2122868
 被引用回数：6 パーセンタイル：47.37(Materials Science, Multidisciplinary)

Metastability engineering is a strategy to enhance the strength and ductility of alloys via deliberately lowering phase stability and prompting deformation-induced martensitic transformation. In this work, the martensitic transformation and its effect on the mechanical response of a Fe$$_{50}$$Co$$_{25}$$Ni$$_{10}$$Al$$_{5}$$Ti$$_{5}$$Mo$$_{5}$$ medium-entropy alloy (MEA) were studied by in situ neutron diffraction under tensile loading. This work shows how great a role FCC to BCC martensitic transformation can play in enhancing the mechanical properties of ferrous MEAs.

論文

${it In situ}$ neutron diffraction study of phase stress evolution in a ferrous medium-entropy alloy under low-temperature tensile loading

Bae, J. W.*; Kim, J. G.*; Park, J. M.*; Woo, W.*; Harjo, S.; Kim, H. S.*

Scripta Materialia, 165, p.60 - 63, 2019/05

https://doi.org/10.1016/j.scriptamat.2019.02.027
 被引用回数：34 パーセンタイル：84.65(Nanoscience & Nanotechnology)

Phase stress evolution of face-centered cubic (FCC) and deformation-induced body-centered cubic (BCC) phases was measured in recently developed ferrous medium-entropy alloy. This was done during tensile deformation at -137$$^{circ}$$C using ${it in situ}$ neutron diffraction measurement for the quantitative interpretation of the role of martensitic transformation on the improved low-temperature tensile properties. The strain-hardening rate curve exhibits two-stage hardening behavior, and the phase stress and stress contribution from the BCC phase increases significantly while that from FCC phase decreases during plastic deformation. This is a direct demonstration that BCC phase contributes significantly to the increase in strength and strain hardening.

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