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論文

Temperature-dependent deformation behavior of dual-phase medium-entropy alloy; In-situ neutron diffraction study

Gu, G. H.*; Jeong, S. G.*; Heo, Y.-U.*; Harjo, S.; Gong, W.; Cho, J.*; Kim, H. S.*; 他4名*

Journal of Materials Science & Technology, 223, p.308 - 324, 2025/07

https://doi.org/10.1016/j.jmst.2024.11.057
 被引用回数：0 パーセンタイル：0.00(Materials Science, Multidisciplinary)

Face-centered cubic (FCC) equi-atomic multi-principal element alloys (MPEAs) exhibit excellent mechanical properties from cryogenic to room temperatures. At room temperature, deformation is dominated by dislocation slip, while at cryogenic temperatures (CTs), reduced stacking fault energy enhances strain hardening with twinning. This study uses in-situ neutron diffraction to analyze the temperature-dependent deformation behavior of Al$$_{7}$$(CoNiV)$$_{93}$$, a dual-phase (FCC/BCC) medium-entropy alloy (MEA). At liquid nitrogen temperature (LNT), deformation twinning in the FCC matrix leads to additional strain hardening through the dynamic Hall-Petch effect, giving the appearance of improved strengthening at LNT. In contrast, BCC precipitates show dislocation slip at both 77 K and 298 K, with temperature-dependent lattice friction stress playing a significant role in strengthening. The study enhances understanding of deformation behaviors and provides insights for future alloy design.

論文

Numerical investigation of the accuracy of a conductance-type wire-mesh sensor for a single spherical bubble and bubbly flow

上澤 伸一郎; 小野 綾子; 永武 拓; 山下 晋; 吉田 啓之

Journal of Nuclear Science and Technology, 62(5), p.432 - 456, 2025/05

https://doi.org/10.1080/00223131.2024.2447366
 被引用回数：0 パーセンタイル：0.00(Nuclear Science & Technology)

ワイヤメッシュセンサ(WMS)の精度を明らかにするため、単一の球形気泡と気泡流に対してWMSの静電場シミュレーションを実施した。単一気泡の静電場シミュレーションでは、様々な気泡位置における電流密度分布と、送信ワイヤから受信ワイヤまでの電流経路を示した。その結果、WMS周囲の不均一な電流密度分布に基づく系統的誤差があることを明らかにした。また、数値流体解析コードJAEA Utility Program for Interdisciplinary Thermal-hydraulics Engineering and Research (JUPITER)で得られた気泡流結果に対して静電場シミュレーションを実施したところ、線形近似やMaxwellの式などの、WMS信号からボイド率への既存の変換方法では0と1の間の瞬間ボイド率の中間値を定量的に推定できなかった。また、WMS信号に対してボイド率$$pm$$0.2という大きなばらつきがあり、瞬間ボイド率を定量的に計測することが困難であることがわかった。一方で、時間平均ボイド率においては、流路の中心付近のボイド率は線形近似を使用して推定でき、流路壁面近くのボイド率はMaxwellの式を使用して推定できることがわかった。

論文

Role of solute hydrogen on mechanical property enhancement in Fe-24Cr-19Ni austenitic steel; An ${it in situ}$ neutron diffraction study

伊東 達矢; 小川 祐平*; Gong, W.; Mao, W.*; 川崎 卓郎; 岡田 和歩*; 柴田 曉伸*; Harjo, S.

Acta Materialia, 287, p.120767_1 - 120767_16, 2025/04

https://doi.org/10.1016/j.actamat.2025.120767
 被引用回数：0 パーセンタイル：0.00(Materials Science, Multidisciplinary)

Incorporating solute hydrogen into Fe-Cr-Ni-based austenitic stainless steels enhances both strength and ductility, providing a promising solution to hydrogen embrittlement by causing solid-solution strengthening and assisting deformation twinning. However, its impacts on the relevant lattice defects evolution (${it i.e.}$, dislocations, stacking faults, and twins) during deformation remains unclear. This study compared the tensile deformation behavior in an Fe-24Cr-19Ni (mass%) austenitic steel with 7600 atom ppm hydrogen-charged (H-charged) and without hydrogen-charged (non-charged) using ${it in situ}$ neutron diffraction. Hydrogen effects on the lattice expansion, solid-solution strengthening, stacking fault probability, stacking fault energy, dislocation density, and strain/stress for twin evolution were quantitatively evaluated to link them with the macroscale mechanical properties. The H-charged sample showed improvements in yield stress, flow stress, and uniform elongation, consistent with earlier findings. However, solute hydrogen exhibited minimal influences on the evolution of dislocation and stacking fault. This fact contradicts the previous reports on hydrogen-enhanced dislocation and stacking fault evolutions, the latter of which can be responsible for the enhancement of twinning. The strain for twin evolution was smaller in the H-charged sample compared to the non-charged one. Nevertheless, when evaluated as the onset stress for twin evolution, there was minimal change between the two samples. These findings suggest that the increase in flow stress due to the solid-solution strengthening by hydrogen is a root cause of accelerated deformation twinning at a smaller strain, leading to an enhanced work-hardening rate and improved uniform elongation.

報告書

1次元熱計算コードGENGTCの計算手法の改良

冬島 拓実; 佐谷戸 夏紀; 大塚 薫; 遠藤 泰一; 飛田 正浩*; 竹本 紀之

JAEA-Testing 2024-008, 38 Pages, 2025/03

JAEA-Testing-2024-008.pdf:2.37MB

材料試験炉(Japan Materials Testing Reactor: JMTR)では燃料試料及び材料試料を照射するため、キャプセルに試料を装荷して照射試験を行ってきた。照射試験では、多種多様な照射試料を目標とする温度で照射するため、キャプセルの熱計算が重要である。令和3年3月にJMTRは廃止措置計画が認可され、環境技術開発部では現在、JMTRの代替としての海外の試験研究炉を用いた照射試験を実施している。海外の試験研究炉を用いた照射試験に向けてキャプセルの設計・検討に必要な熱計算を行う際、米国のオークリッジ国立研究所で開発された1次元熱計算コードGENGTCを用いている。GENGTCはこれまでパソコン性能の向上に伴って改良・拡張が繰り返されてきたが、従来のGENGTCを用いたプログラムには機能の一部に不良事象箇所が確認されていた。そこで、その原因を究明してプログラムを修正するとともに、FORTRAN77言語のプログラムからExcelのマクロ計算機能を使用したVisual Basic言語のプログラムに変更した。また、当該コードをさらに利用しやすくするためのプログラムの整備を行った。本稿はそれらの改良箇所について報告を行うものである。

論文

Reduction and phase transformation of Ce-doped zirconolites

林崎 康平; 廣岡 瞬; 山田 忠久*; 砂押 剛雄*; 村上 龍敏; 齋藤 浩介

Ceramics (Internet), 8(1), p.24_1 - 24_12, 2025/03

https://doi.org/10.3390/ceramics8010024

Zirconolite is a wasteform that can immobilize Pu. Herein, zirconolites comprising Ce as a Pu simulant and Al as a charge compensator of Ce/Pu were synthesized by sintering raw CaO, ZrO$$_{2}$$, TiO$$_{2}$$, CeO$$_{2}$$, and Al$$_{2}$$O$$_{3}$$ powder mixtures at 1400$$^{circ}$$C in static air. The reduction behavior and phase transformation of zirconolites during their heat treatment in an Ar-H$$_{2}$$ gas flow were investigated. All zirconolite compositions first underwent reduction at $$sim$$ 1050$$^{circ}$$C by forming a small domain of perovskite phase. Ce-Al co-doped zirconolite showed a smaller fraction of phase transformation in perovskite than Ce-doped zirconolite, indicating the advantage of using a charge compensator to prevent perovskite formation.

論文

Comparative analysis of primary variables selection in modeling non-isothermal two-phase flow; Insights from EBS experiment at Horonobe URL

Kim, M.*; Lee, C.*; 杉田 裕; Kim, J.-S.*; Jeon, M.-K.*

Geomechanics for Energy and the Environment, 41, p.100628_1 - 100628_9, 2025/03

https://doi.org/10.1016/j.gete.2024.100628
 被引用回数：0 パーセンタイル：0.00(Energy & Fuels)

この研究では、DECOVALEX-2023プロジェクトの一環として幌延の地下研究施設で実施された実規模大の人工バリア試験の数値解析を使用して、非等温二相流のモデリングに対する主要変数の選択の影響を調査した。検証済みの数値モデルを使用して、人工バリアシステム内の不均質多孔質媒体の熱-水連成挙動を解析した。支配方程式を離散化する際の2つの異なる主要変数スキームを比較したところ、結果に大きな違いがあることが明らかになった。

論文

Measurements of neutron capture cross-section for nuclides of interest in decommissioning (II); $$^{58}$$Fe(n,$$gamma$$)$$^{59}$$Fe

中村 詔司; 芝原 雄司*; 遠藤 駿典; Rovira Leveroni, G.; 木村 敦

Journal of Nuclear Science and Technology, 62(3), p.300 - 307, 2025/03

https://doi.org/10.1080/00223131.2024.2427244
 被引用回数：0 パーセンタイル：0.00(Nuclear Science & Technology)

As nuclear facilities are dismantled in decommissioning, large amount of various waste is generated. Even more inconveniently, waste is radioactive due to neutron activation. Thus, the neutron capture cross-sections of nuclides targeted in decommissioning are required to evaluate the radioactivity produced. In this work, $$^{58}$$Fe nuclide was selected among objective nuclides for decommissioning, and its thermal-neutron capture cross-section was measured by a neutron activation method at the graphite thermal column of Kyoto University Research Reactor in 5-MW operation. The thermal-neutron capture cross-section was derived using ${it Westcott'}$s convention. The present work obtained 1.36$$pm$$0.03 barns for the $$^{58}$$Fe(n,$$gamma$$)$$^{59}$$Fe reaction. The present result supports the JENDL-5 evaluation within 2$$sigma$$. If updated with currently recommended nuclear data, some of the reported past data would support the present result.

論文

Stress and plastic strain partitioning behaviors and those contributions to martensitic transformation of retained austenite in medium manganese and transformation-induced plasticity-aided bainitic ferrite steels

北條 智彦*; 小山 元道*; 熊井 麦弥*; Zhou, Y.*; 柴山 由樹; 城 鮎美*; 菖蒲 敬久; 齋藤 寛之*; 味戸 沙耶*; 秋山 英二*

ISIJ International, 65(2), p.284 - 296, 2025/02

https://doi.org/10.2355/isijinternational.ISIJINT-2024-268

Stress and plastic strain distributions and those partitioning behaviors of ferrite and retained austenite were investigated in the medium manganese (Mn) and the transformation-induced plasticity-aided bainitic ferrite (TBF) steels, and the martensitic transformation behaviors of retained austenite during Luders elongation and work hardening were analyzed using synchrotron X-ray diffraction at SPring-8. The stress and plastic strain of retained austenite and volume fraction of retained austenite were remarkably changed during Luders deformation in the medium Mn steel, implying that the medium Mn steel possessed inhomogeneous deformation at the parallel part of the tensile specimen. On the other hand, the distributions of the stress, plastic strain and volume fraction of retained austenite were homogeneous and the homogeneous deformation occurred at the parallel part of the tensile specimen at the plastic deformation regime with work hardening in the medium Mn and TBF steels. The martensitic transformation of retained austenite at uders deformation in the medium Mn steel was possessed owing to the application of high stress and preferential deformation at retained austenite, resulting in a significant increase in the plastic deformation and reduction of stress in the retained austenite. The martensitic transformation of retained austenite at the plastic deformation regime with work hardening was induced by the high dislocation density and newly applied plastic deformation in retained austenite in the medium Mn steel whereas the TBF steel possessed gradual transformation of retained austenite which is applied high tensile stress and moderate plastic deformation.

論文

Unusual low-temperature ductility increase mediated by dislocations alone

Naeem, M.*; Ma, Y.*; Tian, J.*; Kong, H.*; Romero-Resendiz, L.*; Fan, Z.*; Jiang, F.*; Gong, W.; Harjo, S.; Wu, Z.*; et al.

Materials Science & Engineering A, 924, p.147819_1 - 147819_10, 2025/02

https://doi.org/10.1016/j.msea.2025.147819
 被引用回数：0 パーセンタイル：0.00(Nanoscience & Nanotechnology)

Face-centered cubic (fcc) medium-/high-entropy alloys (M/HEAs) typically enhance strength and ductility at cryogenic temperatures via stacking faults, twinning, or martensitic transformation. However, in-situ neutron diffraction on VCoNi MEA at 15 K reveals that strain hardening is driven solely by rapid dislocation accumulation, without these mechanisms. This results in increased yield strength, strain hardening, and fracture strain. The behavior, explained by the Orowan equation, challenges conventional views on cryogenic strengthening in fcc M/HEAs and highlights the role of dislocation-mediated plasticity at low temperatures.

論文

Measurements of neutron capture cross-section for nuclides of interest in decommissioning (III); $$^{170}$$Er(n,$$gamma$$)$$^{171}$$Er and $$^{180}$$Hf(n,$$gamma$$)$$^{181}$$Hf reactions

中村 詔司; 芝原 雄司*; 遠藤 駿典; Rovira Leveroni, G.; 木村 敦

Journal of Nuclear Science and Technology, 14 Pages, 2025/00

https://doi.org/10.1080/00223131.2025.2457589
 被引用回数：0 パーセンタイル：0.00(Nuclear Science & Technology)

In the decommissioning of nuclear facilities, large amounts of radioactive waste are generated due to neutron activation. In that case, neutron capture cross-sections of nuclides targeted in decommissioning are required to evaluate their radioactivities produced. The present study selected two nuclides, $$^{171}$$Er and $$^{181}$$Hf, among objective ones for decommissioning, and thermal-neutron capture cross-sections for their parent nuclides were measured by the neutron activation method at the Kyoto University Research Reactor under 1-MW operation. The thermal-neutron capture cross-sections were derived on the basis of Westcott's convention. The present study obtained the results as follows: 8.19$$pm$$0.35 barns for the $$^{170}$$Er(n,$$gamma$$)$$^{171}$$Er reaction and 13.57$$pm$$0.14 barns for the $$^{180}$$Hf(n,$$gamma$$)$$^{181}$$Hf reaction. As a by-product, the measurements of the Hf sample also yielded 0.427$$pm$$0.006 barns for the $$^{179}$$Hf(n,$$gamma$$)$$^{180m}$$Hf reaction. This study revealed that some experimental and data evaluations differ from the present results by more than the experimental uncertainties.

論文

Martensitic transformation and shape memory effect in Mn-rich Cu-Mn-Al alloys

伊東 達矢; Xu, S.*; Xu, X.*; 大森 俊洋*; 貝沼 亮介*

Shape Memory and Superelasticity, 9 Pages, 2025/00

https://doi.org/10.1007/s40830-025-00519-y

The microstructure, crystal structures, cold workability, and martensitic transformation temperatures of several Cu$$_{100-{it x}-{it y}}$$Mn$$_{it x}$$Al$$_{it y}$$ (40 $$leq$$ ${it x}$ $$leq$$ 55; 10 $$leq$$ ${it y}$ $$leq$$ 13; at%) alloys were analyzed. For the first time, martensitic transformation was revealed Mn-rich Cu-Mn-Al alloys. The surface relief of the martensite phase reversibly appeared and disappeared during cooling and heating, along with small thermal hysteresis, implying a thermoelastic transformation. The crystal structures of the parent and martensite phases are B2 and 2M(BCT), respectively, with c$/a being approximately 1.35. Cold workability improves with decreasing Al content, exhibiting a trend similar to that observed for previously reported Cu-rich Cu-Al-Mn shape memory alloys. The martensitic transformation temperatures decrease with increasing Al content and increase with increasing Mn content. These results are consistent with the stability trends of the parent body-centered cubic phase in the phase diagram at high temperature. The shape memory effect with a recovery strain of 1.3% was observed in a 5.0% pre-stretched Cu$_{39}$$Mn$$_{50}$$Al$$_{11}$$ (at%) sample. This alloy demonstrates moderate cold workability and cost-effectiveness, exhibiting potential as an alternative for conventional shape memory alloys in various applications.

論文

幌延国際共同プロジェクトの現状と今後の展開,4; タスクC: 実規模の人工バリアシステムの解体試験

大野 宏和

原子力バックエンド研究(CD-ROM), 31(2), p.140 - 143, 2024/12

https://nuce.aesj.or.jp/jnuce/vol31/jnuce-vol31-2-p140-143.pdf

高レベル放射性廃物の地層処分において、人工バリア定置後のニアフィールドにおいては、廃棄体の発熱、地下水の浸潤とそれに伴う緩衝材の膨潤応力の発生、間隙水の化学的特性の変化、オーバーパックの腐食など複数の現象が相互に影響し合った複雑な系となることが予想される。地層処分の安全評価においては、このような熱-水-応力-化学連成現象(THMC連成現象)を予測するための解析コードの整備が重要となる。幌延深地層研究センターの地下施設(幌延URL)の深度350m調査坑道では、処分孔竪置き方式の実規模大の人工バリアを堆積岩に定置し、坑道の一部を埋め戻した人工バリア性能確認試験を実施し、ニアフィールドの過渡期状態変遷の評価に必要なデータを緩衝材や埋め戻し材中に設置したセンサーで取得している。幌延国際共同プロジェクトのタスクCは、それらのデータに加えて、人工バリア性能確認試験の解体試験で取得されるデータを用いて、連成現象の理解や解析コードの検証を国際共同プロジェクトとして実施するものである。

論文

Role of retained austenite and deformation-induced martensite in 0.15C-5Mn steel monitored by ${it in situ}$ neutron diffraction measurement during tensile deformation

山下 享介*; 諸岡 聡; Gong, W.; 川崎 卓郎; Harjo, S.; 北條 智彦*; 興津 貴隆*; 藤井 英俊*

ISIJ International, 64(14), p.2051 - 2060, 2024/12

https://doi.org/10.2355/isijinternational.ISIJINT-2024-196

An Fe-0.15C-5Mn-0.5Si-0.05Nb steel annealed at 660$$^{circ}$$C and 685$$^{circ}$$C showed L$"u$ders deformation followed by high work hardening, with variations in L$"u$ders strain and hardening behavior. ${it In situ}$ neutron diffraction during tensile tests analyzed phase stresses, strength contributions, and austenite orientation. Deformation-induced martensite contributed $$sim$$1000 MPa to strength near tensile failure, while austenite mainly enhanced ductility via transformation-induced plasticity. Austenite transformed to martensite during L$"u$ders deformation regardless of orientation, though 311-oriented grains tended to remain along the tensile direction.

論文

Thermal analysis of the hydrogen release behavior of sodium hydride and kinetic analysis using master plot methods

土井 大輔

International Journal of Hydrogen Energy, 91, p.1245 - 1252, 2024/11

https://doi.org/10.1016/j.ijhydene.2024.10.227
 被引用回数：1 パーセンタイル：37.00(Chemistry, Physical)

Hydrogen is a major nonmetallic impurity in the coolant of sodium-cooled fast reactors (SFRs) during normal operation. A higher hydrogen concentration than the gas-liquid equilibrium has been transiently detected in the gas space of actual SFR plants. The presence of several sodium compounds can increase hydrogen generation; however, a thorough understanding of the thermal behavior of candidate reactions is lacking. Herein, thermal analysis reveals the hydrogen release behavior of sodium hydride. Mass spectrometry indicates hydrogen generation with decreasing sample mass, indicating thermal decomposition. Detailed kinetic analysis based on master plot methods indicates that the hydrogen release reaction occurred through a mechanism involving random nucleation and growth of nuclei. Furthermore, the reaction rate was newly formulated based on a kinetic model function representing the above mechanism and the Arrhenius-type reaction rate constant comprising an activation energy of 119.0 $$pm$$ 0.8 kJ mol$$^{-1}$$ and a frequency factor of 1.8 $$times$$ 10$$^{7}$$ s$$^{-1}$$. These findings will enable the numerical simulation of the hydrogen release behavior in SFRs.

論文

Measurements of neutron capture cross-sections for nuclides of interest in decommissioning; $$^{45}$$Sc, $$^{63}$$Cu, $$^{64}$$Zn, $$^{109}$$Ag, and $$^{113}$$In

中村 詔司; 芝原 雄司*; 遠藤 駿典; Rovira Leveroni, G.; 木村 敦

Journal of Nuclear Science and Technology, 61(11), p.1415 - 1430, 2024/11

https://doi.org/10.1080/00223131.2024.2346347
 被引用回数：1 パーセンタイル：62.55(Nuclear Science & Technology)

廃止措置においては、生成放射能の評価に資する核データとして、中性子捕獲断面積を整備する必要がある。本研究では、整備すべき対象核種のうち$$^{45}$$Sc, $$^{63}$$Cu, $$^{65}$$Zn, $$^{109}$$Ag及び$$^{113}$$Inを選定し、KURのTC-Pnを用いてそれらの熱中性子捕獲断面積測定を行った。その結果、熱中性子捕獲断面積の結果が、以下のとおり得られた:$$^{45}$$Sc(n, $$gamma$$)$$^{46}$$Sc反応は27.18$$pm$$0.28 barn、$$^{63}$$Cu(n, $$gamma$$)$$^{64}$$Cu反応は4.34$$pm$$0.06 barn、$$^{64}$$Zn(n, $$gamma$$)$$^{65}$$Zn反応は0.719$$pm$$0.011 barn、$$^{109}$$Ag(n, $$gamma$$)$$^{rm 110m}$$Ag反応は4.05$$pm$$0.05 barn、そして$$^{113}$$In(n, $$gamma$$) $$^{114}$$In$$^{m1+m2}$$反応は8.53$$pm$$0.27 barn。ScとZnの結果は、これまでに報告されている評価値を誤差範囲で支持するが、一方、他の核種については評価値と異なる結果となった。得られた結果は、生成量評価にはもちろん、これらの核種を中性束モニタとして利用する場合に用いることが考えられる。

論文

Deep learning-based bubble detection with Swin Transformer

上澤 伸一郎; 吉田 啓之

Journal of Nuclear Science and Technology, 61(11), p.1438 - 1452, 2024/11

https://doi.org/10.1080/00223131.2024.2348023
 被引用回数：0 パーセンタイル：0.00(Nuclear Science & Technology)

本研究では、重なり合う気泡の中から個々の気泡を検出・分割するために、Shifted window Transformer (Swin Transformer)を用いた深層学習ベースの気泡検出器を開発した。検出器の性能を検証するため、学習画像数を変えて平均適合率(AP)を計算した。APは、訓練画像の数が50枚以下の場合は、トレーニング画像の数の増加とともに増加したが、50枚を超える場合は一定であった。50枚以上ではSwin Transformerと一般的なCNNであるResNetのAPはほぼ同じであったが、学習画像が少ない場合はSwin TransformerのAPがResNetのAPを上回った。また、ボイド率が増加すると、Swin TransformerのAPはResNetの場合と同様の減少を示したものの、学習画像が少ない場合はSwin TransformerのAPが全てのボイド率においてResNetのAPを上回った。さらに、合成気泡画像で学習した検出器で、気泡流可視化実験の重なった気泡や変形気泡の検出が可能であることを確認した。このように、Swin Transformerを用いた新しい気泡検出器は、ResNetを用いた検出器よりも少ない学習画像で高いAPを得られることが確認された。

論文

Enhanced cryogenic mechanical properties of heterostructured CrCoNi multicomponent alloy; Insights from ${it in situ}$ neutron diffraction

Naeem, M.*; Ma, Y.*; Knowles, A. J.*; Gong, W.; Harjo, S.; Wang, X.-L.*; Romero Resendiz, L.*; 他6名*

Materials Science & Engineering A, 916, p.147374_1 - 147374_8, 2024/11

https://doi.org/10.1016/j.msea.2024.147374
 被引用回数：2 パーセンタイル：67.89(Nanoscience & Nanotechnology)

Heterostructured materials (HSMs) improve the strength-ductility trade-off of alloys, but their cryogenic performance under real-time deformation is unclear. We studied heterostructured CrCoNi medium-entropy alloy via ${it in situ}$ neutron diffraction at 77 K and 293 K. A significant mechanical mismatch between fine and coarse grains led to an exceptional yield strength of 918 MPa at 293 K, increasing to 1244 MPa at 77 K with a uniform elongation of 34%. This strength-ductility synergy at 77 K is attributed to high dislocation pile-up density, increased planar faults, and martensitic transformation. Compared to homogeneous alloys, HSMs show promise for enhancing cryogenic mechanical performance in medium-/high-entropy alloys.

論文

Deformation behavior of ultrafine-grained TRIP steel observed by neutron diffraction

Harjo, S.; Mao, W.*; Gong, W.; 川崎 卓郎

Proceedings of the 7th International Symposium on Steel Science (ISSS 2024), p.205 - 208, 2024/11

https://doi.org/10.2355/isijisss.2024.0_205

This study aimed to elucidate the effect of grain size on the deformation behavior of TRIP steel. We prepared metastable austenitic Fe-24Ni-0.3C steel samples with average grain sizes of 35 ${textmu}$m (coarse grain: CG) and 0.5 ${textmu}$m (ultrafine-grain: UFG) for in situ neutron diffraction studies during tensile deformation at room temperature. Our observations revealed increases in dislocation density in both samples prior to DIMT, indicating that plastic deformation precedes DIMT regardless of grain size. In the UFG sample, a significant rise in dislocation density occurred just around the yielding point with minimal increases in macroscopic plastic strain. Additionally, the dislocations exhibited strong dipole arrangements.

論文

Martensitic transformation-governed Luders deformation enables large ductility and late-stage strain hardening in ultrafine-grained austenitic stainless steel at low temperatures

Mao, W.*; Gao, S.*; Gong, W.; 川崎 卓郎; 伊東 達矢; Harjo, S.; 辻 伸泰*

Acta Materialia, 278, p.120233_1 - 120233_13, 2024/10

https://doi.org/10.1016/j.actamat.2024.120233
 被引用回数：5 パーセンタイル：85.37(Materials Science, Multidisciplinary)

Using a hybrid method of in situ neutron diffraction and digital image correlation, we found that ultrafine-grained 304 stainless steel exhibits Luders deformation after yielding, in which the deformation behavior changes from a cooperation mechanism involving dislocation slip and martensitic transformation to one primarily governed by martensitic transformation, as the temperature decreases from 295 K to 77 K. Such martensitic transformation-governed Luders deformation delays the activation of plastic deformation in both the austenite parent and martensite product, resulting in delayed strain hardening. This preserves the strain-hardening capability for the later stage of deformation, thereby maintaining a remarkable elongation of 29% while achieving a high tensile strength of 1.87 GPa at 77 K.

論文

Stress-controlled hydrogen embrittlement failure in U-bend high-strength steel

柴山 由樹; 北條 智彦*; 小山 元道*; 秋山 英二*

International Journal of Hydrogen Energy, 88, p.1010 - 1016, 2024/10

https://doi.org/10.1016/j.ijhydene.2024.09.123
 被引用回数：3 パーセンタイル：37.00(Chemistry, Physical)

The effect of plastic deformation on the hydrogen embrittlement behavior of high-strength martensitic steels was investigated using a U-bend test. The hydrogen embrittlement susceptibility appeared to be enhanced with increasing plastic strain. Based on fractographic and stress-strain analyses, the maximum principal stress dominated the hydrogen embrittlement fracture. Although the apparent enhancement with increasing plastic deformation was observed, the origin of the enhancement was increased residual stress arising from the evolution of graded plastic strain during U-bending. We conclude that residual stress rather than plastic strain induced by plastic deformation strongly affects hydrogen embrittlement susceptibility in deformed high-strength steel components.

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