Strain analysis of thermoelectric materials using high-resolution synchrotron X-ray diffraction data

Nakasawa, Hayato*; Shobu, Takahisa; Tominaga, Aki; Fujii, Masashi*; Matsumoto, Hironari*; Matsuda, Michiko*; Shimada, Takeshi*; Trivedi, V.*; Tachibana, Makoto*; Tsujii, Naohito*; et al.

Funtai Oyobi Fummatsu Yakin, 72(Suppl.), p.S997 - S1001, 2025/03

https://doi.org/10.2497/jjspm.15P-T21-07

Effect of grain refinement on transgranular stress corrosion cracking in SUS304L under boiling water reactor conditions

Hirota, Noriaki; Nakano, Hiroko; Takeda, Ryoma; Ide, Hiroshi; Tsuchiya, Kunihiko; Kobayashi, Yoshinao*

Zairyo No Kagaku To Kogaku, 61(6), p.248 - 252, 2024/12

A comparative analysis of the 0.2 % yield stress in SUS304L stainless steel revealed that lower strain rates and higher temperatures significantly reduce yield stress. Grain refinement from 68.6 m to 0.59 m minimally impacted the rate of yield stress reduction at slower strain rates. However, finer grains showed a decrease in yield stress at reactor operating temperature compared to room temperature. In slow strain rate tests under conditions promoting intragranular stress corrosion cracking (SCC), SUS304L with grain sizes of 28.4 m or smaller exhibited similar fracture strains comparable to those at reactor operating temperatures, whereas coarse-grained SUS304L showed reduced fracture strain. Microstructural analysis showed that in smaller grains, over 87 % of the fracture surface was ductile. In particular, SUS304L with 0.59 m grains exhibited a higher presence of {111} / 3 boundaries, which decreased with grain growth. These results indicate that grain refinement will suppress intragranular SCC by slowing corrosion progression through increased {111} / 3 boundaries.

Effect of dissolved oxygen concentration on dynamic strain aging and stress corrosion cracking of SUS304 stainless steel under high temperature pressurized water

Hirota, Noriaki; Nakano, Hiroko; Fujita, Yoshitaka; Takeuchi, Tomoaki; Tsuchiya, Kunihiko; Demura, Masahiko*; Kobayashi, Yoshinao*

The IV International Scientific Forum "Nuclear Science and Technologies"; AIP Conference Proceedings 3020, p.030007_1 - 030007_6, 2024/01

https://doi.org/10.1063/5.0192888

Dynamic strain aging (DSA) and intergranular stress corrosion cracking (intragranular SCC) occur in high temperature pressurized water simulating a boiling water reactor environment due to changes in dissolved oxygen (DO) content, respectively. In order to clearly understand the difference between these phenomena, the mechanism of their occurrence was summarized. As a result, it was found that DSA due to intragranular cracking occurred in SUS304 stainless steel at low DO 1 ppb, while DSA was suppressed at DO 100 to 8500 ppb due to the formation of oxide films on the surface. On the other hand, when DO was increased to 20000 ppb, the film was peeled from the matrix, O element diffused to the grain boundary of the matrix, resulting in intergranular SCC. These results are indicated that the optimum DO concentration must be adjusted to suppress crack initiation due to DSA and intergranular SCC.

Influence of the strain effect on magnetocrystalline anisotropy in CoFeMnSi Heusler alloys

Nabialek, A.*; Chumak, O. M.*; Aleshkevych, P.*; Domagala, J. Z.*; Pacewicz, A.*; Salski, B.*; Krupka, J.*; Seki, Takeshi*; Takanashi, Koki; Baczewski, L. T.*; et al.

Scientific Reports (Internet), 13, p.17016_1 - 170169, 2023/10

https://doi.org/10.1038/s41598-023-43979-x

The Multiaxial creep-fatigue failure mechanism of Mod. 9Cr-1Mo steel under non-proportional loading; Effect of strain energy on failure lives

Ogawa, Fumio*; Nakayama, Yuta*; Hiyoshi, Noritake*; Hashidate, Ryuta; Wakai, Takashi; Ito, Takamoto*

Transactions of the Indian National Academy of Engineering (Internet), 7(2), p.549 - 564, 2022/06

https://doi.org/10.1007/s41403-021-00279-y

The strain energy-based life evaluation method of Mod. 9Cr-1Mo steel under non-proportional multiaxial creep-fatigue loading is proposed. Inelastic strain energy densities were calculated as the areas inside the hysteresis loops. The effect of mean-stress has been experimentally considered and the relationship between inelastic strain energy densities and creep-fatigue lives was investigated. It was found from the investigation of hysteresis loops, the decrease in maximum stress leads to prolonged failure life, while stress relaxation during strain holding causes strength reduction. The correction method of inelastic strain energy density was proposed considering the effect of maximum stress in hysteresis loop and minimum stress during strain holding, and strain energy densities for uniaxial and non-proportional multiaxial loading were obtained. Based on these results, the mechanisms governing creep-fatigue lives under non-proportional multiaxial loading have been discussed.

Evaluation of internal strain distribution of dissimilar laser welding using high energy X-rays

Shobu, Takahisa; Shiro, Ayumi*; Muramatsu, Toshiharu*

SPring-8/SACLA Riyo Kenkyu Seikashu (Internet), 9(5), p.318 - 323, 2021/08

https://doi.org/10.18957/rr.9.5.318

Laser welding has already been put into practical use for various metal materials because the irradiation area is very small and the control is easy. In this study, we evaluated strain, stress, deformation, etc. near the processing affected area by high-energy synchrotron radiation X-ray diffraction method, which is one of the problems of laser welding of different materials that are expected to be put into practical use. As a result of internal deformation measurement of the bonding of dissimilar materials of copper and iron, it was confirmed that the copper side with a high coefficient of linear expansion was hardly deformed, strong tensile strain on the iron side, and a plastic deformation region on the heat-affected zone. In addition, a retained austenite phase, which is thought to be caused by the mixture of copper, was observed in the plastic deformation region of iron, and further problems were clarified in the evaluation of material strength in the mixed metallic materials.

Constraint effect on fracture mechanics evaluation for an under-clad crack in a reactor pressure vessel steel

Shimodaira, Masaki; Tobita, Toru; Takamizawa, Hisashi; Katsuyama, Jinya; Hanawa, Satoshi

Proceedings of ASME 2020 Pressure Vessels and Piping Conference (PVP 2020) (Internet), 7 Pages, 2020/08

https://doi.org/10.1115/PVP2020-21441

In JEAC 4206 which prescribes the methodology for assessing the structural integrity of reactor pressure vessels (RPVs), an under-clad crack (UCC) at the inner surface of RPV is postulated, and it is required that the fracture toughness of RPV steels is higher than stress intensity factor for at the crack tip during the pressurized thermal shock event. In the present study, to investigate the effect of cladding on the fracture toughness, we performed three-point bending fracture toughness tests and finite element analyses (FEAs) for an RPV steel containing an UCC or a surface crack, and the constraint effect for UCC was also discussed. As the result, we found that the fracture toughness for UCC was considerably higher than that for surface crack. On the other hand, the FEAs showed that the cladding decreased the constraint effect for UCC.

Intergranular strains of plastically deformed austenitic stainless steel

Suzuki, Kenji*; Shobu, Takahisa

E-Journal of Advanced Maintenance (Internet), 10(4), p.9 - 17, 2019/02

In materials with an elastic anisotropy, a stress difference is generated between crystals when plastic deformation occurs, and it is known that this is deeply involved in material fracture. In this study, the residual stress for load direction in the plastically deformed material was investigated for each crystal orientation using the high-energy synchrotron radiation diffraction method. As a result, it was found that the residual stress is a tensile residual stress at an index with a high X-ray elastic constant (Young's modulus obtained for each diffraction surface) and a compressive residual stress at an index with a low X-ray elastic constant. We believe that this result will be useful for the technique of controlling the crystal orientation like the texture as improving the material strength.

Evaluation of thermal strain induced in components of NbSn strand during cooling

Suwa, Tomone*; Hemmi, Tsutomu*; Saito, Toru*; Takahashi, Yoshikazu*; Koizumi, Norikiyo*; Luzin, V.*; Suzuki, Hiroshi; Harjo, S.

IEEE Transactions on Applied Superconductivity, 28(3), p.6001104_1 - 6001104_4, 2018/04

https://doi.org/10.1109/TASC.2018.2793190

Mizunami Underground Research Laboratory Project; Rock mechanical investigations at the -500m stage

Kuwabara, Kazumichi; Sato, Toshinori; Sanada, Hiroyuki; Takayama, Yusuke

JAEA-Research 2015-005, 378 Pages, 2015/07

JAEA-Research-2015-005.pdf:125.5MB
JAEA-Research-2015-005.zip:0.53MB

This report presents the results of following rock mechanical investigations conducted at the -500m Stage. (1) Laboratory tests using cores and block samples obtained at the -500m Stage. (2) In-situ stress measurement using Compact Conical-ended Borehole Overcoring (CCBO) method at the -500m Stage. (3) In-situ stress measurements using Differential Strain Curve Analysis(DSCA) method at the -500m Stage. (4) Development of rock mechanical model.