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Tozawa, Kazukiyo*; Kiriyama, Koji*; Mitsui, Takaya; Shiwaku, Hideaki; Harami, Taikan
JAERI-Tech 2004-041, 27 Pages, 2004/03
Liquid-N-cooled Si crystals replaced water-cooled diamond crystals for the double-crystal monochromator on BL11XU at SPring-8. To use the whole energy from 6 keV to 70 keV, we developed the system of dual symmetric Si geometry, Si(111)/Si(311), which can be switched by a horizontal translation (X) stage perpendicular to the beam axis. The off-line experiment was performed to estimate the degree of the crystal strain, which may arise from the way of assembling in the crystal holder. With MoK
, rocking curves from the crystals were measured for the second crystal of the double-crystal diffractometer of parallel setting. Each of the observed full-width at half maximum (FWHM) was almost constant and identical to the calculated value wherever X-rays hit on the crystal surface. By the use of synchrotron radiation from the undulator the crystals were tested and then the characterization was performed. The observed intensities and rocking curves resulted in that each crystal was good for BL11XU and that the performance of X-ray reflection was improved.
Shiwaku, Hideaki; Mitsui, Takaya; Tozawa, Kazukiyo*; Kiriyama, Koji*; Harami, Taikan; Mochizuki, Tetsuro*
AIP Conference Proceedings 705, p.659 - 662, 2004/00
We developed a multi-crystal switching system on a cryogenically cooled monochromator of JAERI materials science beamline, BL11XU. In order to study our science, it is necessary for ensuring at least the energy range of 6 - 70keV to employ Si(111) and Si(311) crystals. The principle of the crystal switching is that, two pair of crystals is arranged side by side, and they are translated in horizontal direction for exchanging. Indium sheets were inserted between both sides of crystals in order to improve thermal contact. Some adjustment stages of the monochromator were removed to avoid the crystal vibration and a sheet heater was installed on an X-axis stage to prevent over-cooling of X-axis stages. The monochromator is under commissioning at present. In comparison with a previous indirect water cooling diamond (111) crystal monochromator, this monochromator provides high flux intensity from 4 times to 7 times. It takes only 5 minutes to exchange and adjust crystals geometry. This mechanism will be easily applied to other crystals, for example asymmetrical-cut crystals.
Hara, Toru*; Shirasawa, Katsutoshi*; Takeuchi, Masao*; Seike, Takamitsu*; Saito, Yuji; Muro, Takayuki*; Kitamura, Hideo*
Nuclear Instruments and Methods in Physics Research A, 498(1-3), p.496 - 502, 2003/02
Times Cited Count:59 Percentile:95.35(Instruments & Instrumentation)no abstracts in English
Ikezoe, Yasumasa
Hoshasen Kagaku Kiso Katei Kenkyu No Shintenkai, p.130 - 131, 1990/03
no abstracts in English