Actual stress analysis of small-bore butt-welded pipe by complementary use of synchrotron X-rays and neutrons

Suzuki, Kenji*; Miura, Yasufumi*; Shiro, Ayumi*; Toyokawa, Hidenori*; Saji, Choji*; Shobu, Takahisa; Morooka, Satoshi

Zairyo, 72(4), p.316 - 323, 2023/04

https://doi.org/10.2472/jsms.72.316

Report of the design examination and the installation work for the radiation shield at the beam injection area in the 3 GeV synchrotron

Nakanoya, Takamitsu; Kamiya, Junichiro; Yoshimoto, Masahiro; Takayanagi, Tomohiro; Tani, Norio; Kotoku, Hirofumi*; Horino, Koki*; Yanagibashi, Toru*; Takeda, Osamu*; Yamamoto, Kazami

JAEA-Technology 2021-019, 105 Pages, 2021/11

JAEA-Technology-2021-019.pdf:10.25MB

Since a user operation startup, the 3 GeV synchrotron accelerator (Rapid-Cycling Synchrotron: RCS) gradually reinforced the beam power. As a result, the surface dose rate of the apparatus located at the beam injection area of the RCS, such as the magnet, vacuum chambers, beam monitors, etc., increases year by year. The beam injection area has many apparatuses which required manual maintenance, so reducing worker's dose is a serious issue. To solve this problem, we have organized a task force for the installation of the shield. The task force has aimed to optimize the structure of the radiation shield, construct the installation procedure with due consideration of the worker's dose suppression. As the examination result of the shield design, we have decided to adopt removal shielding that could be installed quickly and easily when needed. We carried out shield installation work during the 2020 summer maintenance period. The renewal work required to install the shielding has been carried out in a under high-dose environment. For this reason, reducing the dose of workers was an important issue. So, we carefully prepared the work plan and work procedure in advance. During the work period, we implemented various dose reduction measures and managed individual dose carefully. As a result, the dose of all workers could be kept below the predetermined management value. We had installed removal shielding at the beam injection area in the 2020 summer maintenance period. We confirmed that this shield can contribute to the reduction of the dose during work near the beam injection area. It was a large-scale work to occupy the beam injection area during almost of the summer maintenance period. However, it is considered very meaningful for dose suppression in future maintenance works.

Evaluation of internal strain distribution of dissimilar laser welding using high energy X-rays

Shobu, Takahisa; Shiro, Ayumi*; Muramatsu, Toshiharu*

SPring-8/SACLA Riyo Kenkyu Seikashu (Internet), 9(5), p.318 - 323, 2021/08

https://doi.org/10.18957/rr.9.5.318

Laser welding has already been put into practical use for various metal materials because the irradiation area is very small and the control is easy. In this study, we evaluated strain, stress, deformation, etc. near the processing affected area by high-energy synchrotron radiation X-ray diffraction method, which is one of the problems of laser welding of different materials that are expected to be put into practical use. As a result of internal deformation measurement of the bonding of dissimilar materials of copper and iron, it was confirmed that the copper side with a high coefficient of linear expansion was hardly deformed, strong tensile strain on the iron side, and a plastic deformation region on the heat-affected zone. In addition, a retained austenite phase, which is thought to be caused by the mixture of copper, was observed in the plastic deformation region of iron, and further problems were clarified in the evaluation of material strength in the mixed metallic materials.

Quantifying the dislocation structures of additively manufactured Ti-6Al-4V alloys using X-ray diffraction line profile analysis

Yamanaka, Kenta*; Kuroda, Asumi*; Ito, Miyu*; Mori, Manami*; Bian, H.*; Shobu, Takahisa; Sato, Shigeo*; Chiba, Akihiko*

Additive Manufacturing, 37, p.101678_1 - 101678_12, 2021/01

https://doi.org/10.1016/j.addma.2020.101678

Improving fatigue performance of laser-welded 2024-T3 aluminum alloy using dry laser peening

Sano, Tomokazu*; Eimura, Takayuki*; Hirose, Akio*; Kawahito, Yosuke*; Katayama, Seiji*; Arakawa, Kazuto*; Masaki, Kiyotaka*; Shiro, Ayumi*; Shobu, Takahisa; Sano, Yuji*

Metals, 9(11), p.1192_1 - 1192_13, 2019/11

AA2019-0690.pdf:3.91MB

https://doi.org/10.3390/met9111192

The purpose of the present study was to verify the effectiveness of dry laser peening (DryLP), which is the peening technique without a sacrificial overlay under atmospheric conditions using femtosecond laser pulses on the mechanical properties such as hardness, residual stress, and fatigue performance. After DryLP treatment of the laser-welded 2024 aluminum alloy, the softened weld metal recovered to the original hardness of base metal, while residual tensile stress in the weld metal and heat-affected zone changed to compressive stresses. The fatigue life almost doubled at a stress amplitude of 180 MPa and increased by a factor of more than 50 at 120 MPa. As a result, DryLP was found to be more effective for improving the fatigue performance of laser-welded aluminum specimens with welding defects at lower stress amplitudes.

Effect of metal structure on damping characteristics of cymbals

Ogawa, Wataru*; Shobu, Takahisa; Kakehi, Mizue*; Kuratani, Fumiyasu*; Koide, Toshio*; Monju, Yoshiyuki*; Mizuta, Taiji*

Nihon Kinzoku Gakkai-Shi, 83(4), p.128 - 135, 2019/04

https://doi.org/10.2320/jinstmet.J2018056

Cymbals are percussion musical instruments with a simpler structure than other musical instruments. Therefore, their material composition basically decides the sound quality and decay time rather than the skill of the player. In this study, specimens of cymbals to which Titanium, Zirconium and Iron were added were prepared. From the difference of diffraction rings by synchrotron radiation X-rays, the crystal structure of the specimens of cymbals prepared by various manufacturing processes was analyzed in order to investigate the relationship between the crystal structure associated with the material and manufacturing process used and the damping of the sound of cymbals. As a result, it was found that the changes in the crystal structure were due to the manufacturing process used. In addition, it was clarified that the changes affected the damping of the sound of cymbals.

Intergranular strains of plastically deformed austenitic stainless steel

Suzuki, Kenji*; Shobu, Takahisa

E-Journal of Advanced Maintenance (Internet), 10(4), p.9 - 17, 2019/02

In materials with an elastic anisotropy, a stress difference is generated between crystals when plastic deformation occurs, and it is known that this is deeply involved in material fracture. In this study, the residual stress for load direction in the plastically deformed material was investigated for each crystal orientation using the high-energy synchrotron radiation diffraction method. As a result, it was found that the residual stress is a tensile residual stress at an index with a high X-ray elastic constant (Young's modulus obtained for each diffraction surface) and a compressive residual stress at an index with a low X-ray elastic constant. We believe that this result will be useful for the technique of controlling the crystal orientation like the texture as improving the material strength.

Preheat effect on titanium plate fabricated by sputter-free selective laser melting in vacuum

Sato, Yuji*; Tsukamoto, Masahiro*; Shobu, Takahisa; Yamashita, Yoshihiro*; Yamagata, Shuto*; Nishi, Takaya*; Higashino, Ritsuko*; Okubo, Tomomasa*; Nakano, Hitoshi*; Abe, Nobuyuki*

Applied Physics A, 124(4), p.288_1 - 288_6, 2018/04

https://doi.org/10.1007/s00339-018-1712-4

The dynamics of titanium (Ti) melted by laser irradiation was investigated in a synchrotron radiation experiment. As an indicator of wettability, the contact angle between a selective laser melting (SLM) baseplate and the molten Ti was measured by synchrotron X-rays at 30 keV during laser irradiation. As the baseplate temperature increased, the contact angle decreased, down to 28 degrees at a baseplate temperature of 500C. Based on this result, the influence of wettability of a Ti plate fabricated by SLM in a vacuum was investigated. It was revealed that the improvement of wettability by preheating suppressed sputtering generation, and a surface having a small surface roughness was fabricated by SLM in a vacuum.

Dislocation density of GlidCop with compressive strain applied at high temperature

Sano, Mutsumi*; Takahashi, Sunao*; Watanabe, Atsuo*; Shiro, Ayumi*; Shobu, Takahisa

Materials Research Proceedings, Vol.2, p.609 - 614, 2017/00

https://doi.org/10.21741/9781945291173-103

Dislocation densities of GlidCop with compressive strain applied at high temperature were examined by X-ray line profile analyses with synchrotron radiation. In order to evaluate the dislocation density, we applied the modified Williamson-Hall and modified Warren-Averbach method. The dislocation densities of GlidCop with compressive strain from 0.011-0.04 were in the range of 5.7-8.010m.

Hydrostatic compression behavior and high-pressure stabilized -phase in -based titanium aluminide intermetallics

Liss, K.-D.*; Funakoshi, Kenichi*; Dippenaar, R. J.*; Higo, Yuji*; Shiro, Ayumi*; Reid, M.*; Suzuki, Hiroshi; Shobu, Takahisa; Akita, Koichi

Metals, 6(7), p.165_1 - 165_22, 2016/07

https://doi.org/10.3390/met6070165

Titanium aluminides find application in modern light-weight, high-temperature turbines, such as aircraft engines, but suffer from poor plasticity during manufacturing and processing. Huge forging presses enable materials processing in the 10 GPa range and hence, it is necessary to investigate the phase-diagrams of candidate materials under these extreme conditions. Here we report on an in-situ synchrotron X-ray diffraction study in a large-volume-press of a modern ( + ) two-phase material, Ti-45Al-7.5Nb-0.25C, under pressures up to 9.6 GPa and temperatures up to 1686 K. At room temperature, the volume response to pressure is accommodated by the transformation rather than volumetric strain, expressed by apparently high bulk moduli of both constituent phases. Crystallographic aspects, specifically lattice strain and atomic order are discussed in detail. It is interesting to note that this transformation takes place despite an increase in atomic volume, which is due to the high ordering energy of . Upon heating under high pressure, both the eutectoid and -solvus transition temperatures are elevated, and a third, cubic -phase is stabilized above 1350 K. Earlier research has shown that this -phase is very ductile during plastic deformation, essential in near-conventional forging processes. Here, we were able to identify an ideal processing window for near-conventional forging, while the presence of the detrimental -phase is not present under operating conditions. Novel processing routes can be defined from these findings.