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JAEA Reports

FBR metallic materials test manual (2023 revised edition)

Imagawa, Yuya; Toyota, Kodai; Onizawa, Takashi; Kato, Shoichi

JAEA-Testing 2023-004, 76 Pages, 2024/03

JAEA-Testing-2023-004.pdf:2.08MB

This manual describes the methods for conducting material tests in air, argon gas, and sodium, and for organizing the data obtained, as a part of the development of high-temperature structural design technology for fast reactors. This manual reflects the revision of test methods in Japanese Industrial Standards (JIS) to the "FBR Metallic Materials Test Manual, PNC TN241 77-03" published in 1977 and the "FBR Metallic Materials Test Manual (Revised Edition), JNC TN9520 2001-001" published in 2001. Also, it was written with reference to the recommended room temperature / elevated temperature tensile test method by the Japan Society of Mechanical Engineers (JSME) and the test standard for the elevated-temperature low-cycle fatigue test method by the Society of Materials Science, Japan (JSMS), which are the standard for material test methods in the domestic academic society.

Journal Articles

Validation of the applicability of the best-fit fatigue curves for 550$$^{circ}$$C in Mod.9Cr-1Mo steel to 1$$times$$10$$^{11}$$ cycles

Toyota, Kodai; Imagawa, Yuya; Onizawa, Takashi; Kato, Shoichi; Furuya, Yoshiyuki*

Nihon Kikai Gakkai Rombunshu (Internet), 89(928), p.23-00206_1 - 23-00206_15, 2023/12

In order to design fast reactors, it is necessary to consider high cycle fatigue of structural materials up to 1$$times$$10$$^{9}$$ cycles; to evaluate high cycle fatigue at 1$$times$$10$$^{9}$$ cycles, it is necessary to develop a best-fit fatigue curve applicable up to 1$$times$$10$$^{11}$$ cycles. In this study, high cycle fatigue tests were conducted under strain-controlled conditions and ultrasonic fatigue tests were also conducted to develop a high cycle fatigue evaluation method for Mod.9Cr-1Mo steel, which is a candidate material for fast reactor structural materials. Based on the test results, the best-fit fatigue curves were extended and the applicability of the JSME best-fit fatigue curves up to 1$$times$$10$$^{11}$$ cycles was verified.

Journal Articles

Material data acquisition activities to develop the material strength standard for sodium-cooled fast reactors

Toyota, Kodai; Onizawa, Takashi; Wakai, Takashi; Hashidate, Ryuta; Kato, Shoichi

Proceedings of International Conference on Fast Reactors and Related Fuel Cycles; Sustainable Clean Energy for the Future (FR22) (Internet), 10 Pages, 2022/04

JAEA Reports

Evaluation of tensile and creep properties on 9Cr-ODS steel claddings

Yano, Yasuhide; Hashidate, Ryuta; Tanno, Takashi; Imagawa, Yuya; Kato, Shoichi; Onizawa, Takashi; Ito, Chikara; Uwaba, Tomoyuki; Otsuka, Satoshi; Kaito, Takeji

JAEA-Data/Code 2021-015, 64 Pages, 2022/01

JAEA-Data-Code-2021-015.pdf:2.6MB

From a view point of practical application of fast breeder reactor cycles, which takes advantage of safety and economic efficiency and makes a contribution of volume reduction and mitigation of degree of harmfulness of high-level radioactive waste, it is necessary to develop fuel cladding materials for fast reactors (FRs) in order to achieve high-burnup. Oxide dispersion strengthened (ODS) steel have been studied for use as potential fuel cladding materials in FRs owing to their excellent resistance to swelling and their high-temperature strength in Japan Atomic Energy Agency. It is very important to establish the materials strength standard in order to apply ODS steels as a fuel cladding. Therefore, it is necessary to acquire the mechanical properties such as tensile, creep rupture strength tests and so on. In this study, tensile and creep rupture strengths of 9Cr-ODS steel claddings were evaluated using by acquired these data. Because of the phase transformation temperature of 9Cr-ODS steel, temperature range for the evaluation was divided into two ones at AC1 transformation temperature of 850$$^{circ}$$C.

Journal Articles

Proposal of simulation material test technique for clarifying the structure failure mechanisms under excessive seismic loads

Hashidate, Ryuta; Kato, Shoichi; Onizawa, Takashi; Wakai, Takashi; Kasahara, Naoto*

Proceedings of ASME 2021 Pressure Vessels and Piping Conference (PVP 2021) (Internet), 9 Pages, 2021/07

It is very essential to clarify the structure failure mechanisms under excessive seismic loads. However, structural tests using actual structural materials are very difficult and expensive. Therefore, we have proposed the structure test approach using lead alloys in order to simulate the structure failure mechanisms under the excessive seismic loads. In this study, we conducted material tests using lead alloy and verified the effectiveness of the simulated material tests. Moreover, we formulated inelastic constitutive equations (best fit fatigue curve equation and cyclic stress range - strain range relationship equation) of lead alloy based on the results of a series of material tests. Nonlinear numerical analyses, e.g. finite element analyses, can be performed using the proposed equations. A series of simulation material test technique enables structural tests and analyses using lead alloy to simulate the structure failure phenomena under excessive seismic loads.

Journal Articles

High-temperature creep deformation in FeCrAl-oxide dispersion strengthened alloy cladding

Ukai, Shigeharu; Kato, Shoichi; Furukawa, Tomohiro; Otsuka, Satoshi

Materials Science & Engineering A, 794, p.139863_1 - 139863_13, 2020/09

 Times Cited Count:33 Percentile:95.13(Nanoscience & Nanotechnology)

The FeCrAl-oxide dispersion strengthened (ODS) alloy is the promising cladding material for the accident-tolerant fuel (ATF) of the light water reactors (LWR). Ring-creep tests for FeCrAl-ODS alloy cladding were carried out at 973 K and 1273 K. The dislocation detachment stress from the dispersoid was derived by considering the dislocation-dispersoid elastic interaction and the dislocation relaxation effect by climb motion. When the applied stress exceeds the dislocation detachment stress, dislocations overcome the dispersoids with the reduced values of the stress exponent. When the stress is lower than the dislocation detachment stress, grain boundary sliding (GBS) is dominant factor for the low strain rate creep deformation at 1273 K. Based on those findings, new constitutive equations for creep deformation were constructed, which is applicable to low stress, low strain rate and high temperature conditions encountered at the reactor sever accident.

Journal Articles

Proposal of simulation materials test technique and their constitutive equations for structural tests and analyses simulating severe accident conditions

Hashidate, Ryuta; Kato, Shoichi; Onizawa, Takashi; Wakai, Takashi; Kasahara, Naoto*

Proceedings of ASME 2020 Pressure Vessels and Piping Conference (PVP 2020) (Internet), 9 Pages, 2020/08

Although it is very essential to clarify how the structure collapses under the severe accident conditions, the failure mechanisms in excessive high temperatures are not clarified. However, it is very difficult and expensive to perform structural tests using actual structural materials. Therefore, we propose to use lead alloys instead of actual structural materials. For demonstration of analogy between the failure mechanisms of lead alloys structure at low temperature and those of the actual structures at high temperature, numerical analyses are required. Although the authors proposed inelastic constitutive equations for numerical analyses in 2019, the equations could not successfully express because of large variations observed in the material tests of the lead alloy. In this study, we propose the improved inelastic constitutive equations of the lead alloy on the basis of the material test results used by aged alloy which can stabilized the material characteristic.

Journal Articles

Development of ODS tempered martensitic steel for high burn up fuel cladding tube of SFR

Otsuka, Satoshi; Tanno, Takashi; Oka, Hiroshi; Yano, Yasuhide; Tachi, Yoshiaki; Kaito, Takeji; Hashidate, Ryuta; Kato, Shoichi; Furukawa, Tomohiro; Ito, Chikara; et al.

2018 GIF Symposium Proceedings (Internet), p.305 - 314, 2020/05

Oxide Dispersion Strengthened (ODS) steel has been developed worldwide as a high-strength and radiation-tolerant steel used for advanced nuclear system. Japan Atomic Energy Agency (JAEA) has been developing ODS steel as the primary candidate material of Sodium cooled Fast Reactor (SFR) high burn-up fuel cladding tube. Application of high burn-up fuel to SFR core can contribute to improvement of economical performance of SFR in conjunction with volume and hazardousness reduction of radioactive waste. This paper described the current status and future prospects of ODS tempered martensitic steel development in JAEA for SFR fuel application.

JAEA Reports

Material test data of SUS316 and SUS321, 1

Hashidate, Ryuta; Kato, Shoichi; Kurihara, Akikazu

JAEA-Data/Code 2019-005, 117 Pages, 2019/07

JAEA-Data-Code-2019-005.pdf:2.54MB

SUS316 and SUS321 are used for structural materials of the Fast Breeder Reactors (FBRs), because of excellent high creep strength. This report summarized the mechanical properties data on SUS316 and SUS321 obtained in various tests including the long-term material tests and the material tests in sodium.

Journal Articles

Ultra-high temperature creep rupture and transient burst strength of ODS steel claddings

Yano, Yasuhide; Sekio, Yoshihiro; Tanno, Takashi; Kato, Shoichi; Inoue, Toshihiko; Oka, Hiroshi; Otsuka, Satoshi; Furukawa, Tomohiro; Uwaba, Tomoyuki; Kaito, Takeji; et al.

Journal of Nuclear Materials, 516, p.347 - 353, 2019/04

 Times Cited Count:13 Percentile:85.03(Materials Science, Multidisciplinary)

9Cr-ODS steel claddings consisting of tempered martensitic matrix, showed prominent creep rupture strength at 1000 $$^{circ}$$C, which surpassed that of heat-resistant austenitic steels although creep rupture strength of tempered martensitic steels is generally lower than that of austenitic steels at high temperatures. The measured creep rupture strength of 9Cr-ODS steel claddings at 1000 $$^{circ}$$C was higher than that from extrapolated creep rupture trend curves formulated using data at temperatures from 650 to 850 $$^{circ}$$C. This superior strength seemed to be owing to transformation of the matrix from the $$alpha$$-phase to the $$gamma$$-phase. The transient burst strengths for 9Cr-ODS steel were much higher than those for 11Cr-ferritic/martensitic steel (PNC-FMS). Cumulative damage fraction analyses suggested that the life fraction rule can be used for the rupture life prediction of 9Cr-ODS steel and PNC-FMS claddings in the transient and accidental events with a certain accuracy.

Journal Articles

Model calculation of Cr dissolution behavior of ODS ferritic steel in high-temperature flowing sodium environment

Otsuka, Satoshi; Tanno, Takashi; Oka, Hiroshi; Yano, Yasuhide; Kato, Shoichi; Furukawa, Tomohiro; Kaito, Takeji

Journal of Nuclear Materials, 505, p.44 - 53, 2018/07

AA2017-0603.pdf:1.7MB

 Times Cited Count:2 Percentile:21.23(Materials Science, Multidisciplinary)

A calculation model was constructed to systematically study the effects of environmental conditions (i.e. Cr concentration in sodium, test temperature, axial temperature gradient of fuel pin, and sodium flow velocity) on Cr dissolution behavior. Chromium dissolution was largely influenced by small changes in Cr concentration (i.e. chemical potential of Cr) in liquid sodium in the model calculation. Chromium concentration in sodium coolant, therefore, should be recognized as a critical parameter for the prediction and management of Cr dissolution behavior in the sodium-cooled fast reactor (SFR) core. Because the fuel column length showed no impact on dissolution behavior in the model calculation, no significant downstream effects possibly take place in the SFR fuel cladding tube due to the much shorter length compared with sodium loops in the SFR plant and the large axial temperature gradient. The calculated profile of Cr concentration along the wall-thickness direction was consistent with that measured in BOR-60 irradiation test where Cr concentration in sodium bulk flow was set at 0.07 wt ppm in the calculation.

Journal Articles

Thermal fatigue test on dissimilar welded joint between Gr.91 and 304SS

Wakai, Takashi; Kobayashi, Sumio; Kato, Shoichi; Ando, Masanori; Takasho, Hideki*

Proceedings of 25th International Conference on Nuclear Engineering (ICONE-25) (CD-ROM), 7 Pages, 2017/07

This paper describes a thermal fatigue test on a structural model with a dissimilar welded joint. In the present design of JSFR, there may be dissimilar welded joints between ferritic and austenitic steels especially in IHX and SG. Creep-fatigue is one of the most important failure modes in JSFR components. However, the creep-fatigue damage evaluation method has not been established for dissimilar welded joint. To investigate the evaluation method, structural test will be needed for verification. Therefore, a thermal fatigue test on a thick-wall cylinder with a circumferential dissimilar welded joint between Mod.9Cr-1Mo steel and 304SS was performed. Since the coefficients of thermal expansion of these steels were significantly different, buttering layer of Ni base alloy was installed between them. After the completion of the test, deep cracks were observed at the HAZ in 304SS, as well as at HAZ in Mod.9Cr-1Mo steel. There were many tiny surface cracks in BM of 304SS. According to the fatigue damage evaluation based on the finite element analysis results, the largest fatigue damage was calculated at HAZ in 304SS. Large fatigue damage was also estimated at BM of 304SS. Fatigue cracks were observed at HAZ and BM of 304SS in the test, so that analytical results are in a good agreement with the observations. However, though relatively small fatigue damage was estimated at HAZ in Mod.9Cr-1Mo steel, deep fatigue cracks were observed in the test. To identify the cause of such a discrepancy between the test and calculations, we performed a series of finite element analyses. Some metallurgical investigations were also performed.

Journal Articles

Ultra-high temperature tensile properties of ODS steel claddings under severe accident conditions

Yano, Yasuhide; Tanno, Takashi; Oka, Hiroshi; Otsuka, Satoshi; Inoue, Toshihiko; Kato, Shoichi; Furukawa, Tomohiro; Uwaba, Tomoyuki; Kaito, Takeji; Ukai, Shigeharu*; et al.

Journal of Nuclear Materials, 487, p.229 - 237, 2017/04

 Times Cited Count:32 Percentile:96.87(Materials Science, Multidisciplinary)

Ultra-high temperature ring tensile tests were carried out to investigate the tensile behavior of oxide dispersion strengthened (ODS) steel claddings and wrapper materials under severe accident conditions; temperatures ranged from room temperature to 1400$$^{circ}$$C which is near the melting point of core materials. The experimental results showed that tensile strength of 9Cr-ODS steel claddings was highest in the core materials at the ultra-high temperatures between 900 and 1200$$^{circ}$$C, but that there was significant degradation in tensile strength of 9Cr-ODS steel claddings above 1200$$^{circ}$$C. This degradation was attributed to grain boundary sliding deformation with $$gamma$$/$$delta$$ transformation, which was associated with reduced ductility. On the other hand, tensile strength of recrystallized 12Cr-ODS and FeCrAl-ODS steel claddings retained its high value above 1200 $$^{circ}$$C unlike the other tested materials. Present study includes the result of "R&D of ODS ferritic steel fuel cladding for maintaining fuel integrity at the high temperature accident condition" entrusted to Hokkaido University by the Ministry of Education, Culture, Sports, Science and Technology of Japan (MEXT).

Journal Articles

Evaluation on tolerance to failure of ODS ferritic steel claddings at the accident conditions of fast reactors

Uwaba, Tomoyuki; Yano, Yasuhide; Otsuka, Satoshi; Naganuma, Masayuki; Tanno, Takashi; Oka, Hiroshi; Kato, Shoichi; Kaito, Takeji; Ukai, Shigeharu*; Kimura, Akihiko*; et al.

Proceedings of 2017 International Congress on Advances in Nuclear Power Plants (ICAPP 2017) (CD-ROM), 7 Pages, 2017/04

Tolerance of fast rector fuel elements to failure in the typical accident conditions was evaluated for the oxide-dispersion-strengthened (ODS) ferritic steel claddings that are candidate of the cladding material for advanced fast reactors. The evaluation was based on the cladding creep damage, which was quantified by the cumulative damage fractions (CDFs). It was shown that the CDFs of the ODS ferritic steel cladding were substantially lower than the breach limit of 1.0 in the loss of flow and transient over power conditions until a passive reactor shutdown system operates.

Journal Articles

Influence of cyclic softening on high temperature material properties in Mod.9Cr-1Mo steel

Onizawa, Takashi; Nagae, Yuji; Kato, Shoichi; Wakai, Takashi

Zairyo, 66(2), p.122 - 129, 2017/02

The applicability of Modified 9Cr-1Mo steel (ASME Grade 91 steel) as the main structural material in advanced loop-type sodium cooled fast reactor has been explored to enhance the safety, the credibility and the economic competitiveness of fast reactor plants. It is well-known that the steel exhibits cyclic softening behavior. Decrease of tensile and creep strength in softened materials has been already reported by other researchers. This paper discusses the relationship between cyclic softening conditions and high temperature material properties. Grade 91 steel was softened by repeat of plastic strain. The softening behavior could be evaluated by the index of the softening rate. Decrease of tensile and creep strength in softened materials can be evaluated by the softening rate and it depends on the cyclic softening conditions.

Journal Articles

Creep-fatigue tests of double-end notched bar made of Mod.9Cr-1Mo steel

Shimomura, Kenta; Kato, Shoichi; Wakai, Takashi; Ando, Masanori; Hirose, Yuichi*; Sato, Kenichiro*

Proceedings of 23rd International Conference on Nuclear Engineering (ICONE-23) (DVD-ROM), 9 Pages, 2015/05

This paper describes experimental and analytical works to confirm that the design standard for SFR components sufficiently covers possible failure mechanisms. Creep-fatigue damage evaluation method in JSME design standard for SFR components has been constructed based on experiments and/or numerical analyses of conventional austenitic stainless steels, such as 304SS. Since the material characteristics of Mod.9Cr-1Mo steel are substantially different from those of austenitic stainless steels, it is required to verify the applicability of the design standards to the SFR components made of Mod.9Cr-1Mo steel. A series of uni-axial creep-fatigue tests were conducted using double-ended notch bar specimens made of Mod.9Cr-1Mo steel under displacement controlled condition with 30 minute holding. The curvature radii of the specimens were 1.6mm, 11.2mm and 40.0mm. The specimen having 1.6mm notch and 11.2mm notch failed from outer surface but the specimen having 40.0mm notch showed obvious internal crack nucleation. In addition, though total duration time of the creep-fatigue test was only 2,000 hours, a lot of creep voids and inter granular crack growth were observed. To clarify the cause of such peculiar failure, some additional experiments were performed, as well as some numerical analyses. We could point out that such a peculiar failure aspect might result from corresponding stress distribution in the cross section. As a result of a series of investigations, possible causes of such peculiar failure could be narrowed down. A future investigation plan was proposed to clarify the most significant cause.

Journal Articles

Current status of the technology development on lithium safety handling under IFMIF/EVEDA

Furukawa, Tomohiro; Hirakawa, Yasushi; Kato, Shoichi; Iijima, Minoru; Otaka, Masahiko; Kondo, Hiroo; Kanemura, Takuji; Wakai, Eiichi

Fusion Engineering and Design, 89(12), p.2902 - 2909, 2014/12

 Times Cited Count:8 Percentile:53.55(Nuclear Science & Technology)

For the irradiation test of the candidate materials for the fusion DEMO reactor, Engineering Validation and Engineering Design Activities (EVEDA) of the International Fusion Materials Irradiation Facility (IFMIF) are performed under the Broader Approach Activities. As a major Japanese activity on the target facility of the IFMIF, the engineering validation using the EVEDA Lithium Test Loop which is the largest scale liquid lithium test loop has been started in 2012. In parallel with the design and fabrication, the research on the technology establishment for the lithium safety handling was started in 2008, as one of the related technologies under the IFMIF-EVEDA. In the research, experiments of lithium chemical reaction, experiments on lithium fire, establishment of chemical analysis of impurities in lithium and experiments on advanced lithium leak detection system were carried out. This paper describes the results of these experiments.

Journal Articles

Corrosion of austenitic steel in leakage lithium

Furukawa, Tomohiro; Hirakawa, Yasushi; Kato, Shoichi

Fusion Engineering and Design, 88(9-10), p.2502 - 2505, 2013/10

 Times Cited Count:6 Percentile:44.21(Nuclear Science & Technology)

Lithium, which is used as the neutron source of the IFMIF, reacts with oxygen, nitrogen and moisture in atmosphere in case of the leakage accident. In this study, fundamental corrosion test was performed in order to obtain the corrosion behavior of austenitic stainless steel in the estimated lithium compounds. In the experiment, the lithium compounds were filled with the steel into the Tammann pipe made from Al$$_{2}$$O$$_{2}$$, and heated up to 850$$^{circ}$$C. After the test, the specimen was cleaned by alcohol, and then the weight loss measurement and metallurgical examination were performed. Intense corrosion was observed at the environmental conditions containing lithium peroxide. No corrosion was observed in Li$$_{2}$$O environment. According to the consideration based on thermodynamics, Li$$_{2}$$O cannot oxidize iron and lithium is reducing agent. Slight corrosion was observed in LiOH and Li$$_{3}$$N environments.

JAEA Reports

Corrosion and low-cycle fatigue behavior of FBR structural materials in sodium contaminated by oxygen

Yoshida, Eiichi; Kato, Shoichi; Furukawa, Tomohiro

JAEA-Research 2012-034, 68 Pages, 2013/01

JAEA-Research-2012-034.pdf:11.75MB

Oxygen concentration in sodium is the important factor for the corrosion of FBR structural materials. In this study, the experiments have been done to clarify the effect of sodium contaminated by oxygen on corrosion and low cycle fatigue strength of the materials. The materials for use of the experiments were FBR Grade type 316 SS (316FR) and Mod. 9Cr-1Mo steel. The corrosion test has been performed in sodium containing of 1, 10$$^{3}$$ and 10$$^{4}$$ ppm of initial oxygen at 650$$^{circ}$$C for 500 hours. The fatigue test has been done for the post-immersed steels at 650$$^{circ}$$C in air.

JAEA Reports

Compatibility of zirconium alloys in high-temperature sodium

Furukawa, Tomohiro; Kato, Shoichi; Maeda, Shigetaka; Yamamoto, Masaya; Sekine, Takashi; Ito, Chikara

JAEA-Research 2011-039, 20 Pages, 2012/02

JAEA-Research-2011-039.pdf:3.4MB

Application of zirconium alloy as a neutron reflector around the driver fuel region of the Japanese experimental fast reactor JOYO has been planned for a further increase of core average burn-up. In order to investigate the compatibility of the zirconium alloys with high-temperature sodium which is coolant of the JOYO, corrosion test in sodium and tensile test of the exposed alloys were performed. The corrosion test was done at 500$$^{circ}$$C and 650$$^{circ}$$C in stagnant/flowing sodium for two kinds of zirconium alloys, and then weight change measurement and metallurgical observation were carried out. The tensile test was performed in air at the same temperature with the sodium exposure.

133 (Records 1-20 displayed on this page)