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Okuchi, Takuo*; Sasaki, Shigeo*; Osakabe, Toyotaka; Ono, Yoshiki*; Odake, Shoko*; Kagi, Hiroyuki*
Journal of Physics; Conference Series, 215, p.012188_1 - 012188_9, 2010/03
Times Cited Count：5 Percentile：85.14(Instruments & Instrumentation)We prepared super-hard nano-polycrystalline diamond (NPD) anvils for large-volume compression for intrinsically low-sensitivity methods of measurement, such as neutron scattering and NMR. These anvils are harder, larger and stronger than single crystal diamond anvils, so that they could play an ideal role to accept the larger forces. We tested supported and unsupported anvil geometries separately by using two types of compact high-pressure cells and could generate the pressure of 14 GPa for the sample volume of 0.1 mm
or more. The test results demonstrate a large future potential of NPD anvils for large-volume compression.
Abe, Jun; Hattori, Takanori; Arima, Hiroshi; Sano, Asami; Fukazawa, Hiroshi; Utsumi, Wataru; Komatsu, Kazuki*; Arakawa, Masashi*; Iizuka, Riko*; Kagi, Hiroyuki*; et al.
no journal, ,
In order to confirm the feasibility of high-pressure neutron diffraction at TAKUMI, we have performed a number of R&Ds using a various high-pressure devices. Optimization of materials such as anvil and pressure medium and developments of collimators have made possible reduction of background and contamination noise. Incident and diffracted neutron beams travel through high-pressure device, which causes attenuation of neutron. We investigated the method of attenuation correction.
Hattori, Takanori; Arima, Hiroshi; Sano, Asami; Abe, Jun; Honda, Mitsunori; Fukazawa, Hiroshi; Utsumi, Wataru; Okuchi, Takuo*; Ono, Yoshiki*; Sasaki, Shigeo*; et al.
no journal, ,
The high-pressure neutron experiments above 10 GPa are limited so far due to the small neutron flux, which is insufficient for tiny high-pressure sample. Recent construction of the intense pulsed neutron source around the world has changed the situation. Inspired by the new Japanese pulsed neutron source JSNS at J-PARC, we started the high-P neutron experiments at the already operated beamlines (TAKUMI, NOVA) and the construction of the new beamline dedicated for high-pressure use (PLANET). This talk introduces these activities.
Abe, Jun; Arima, Hiroshi; Hattori, Takanori; Sano, Asami; Fukazawa, Hiroshi; Utsumi, Wataru; Komatsu, Kazuki*; Arakawa, Masashi*; Iizuka, Riko*; Kagi, Hiroyuki; et al.
no journal, ,
We have performed high-pressure neutron diffraction experiments at TAKUMI in J-PARC. Three types of high-pressure devices are used, Paris-Edinburgh Press, Palm cubic anvil cell and NPD-DAC. Optimization of materials such as anvil and pressure medium and developments of collimators have made possible reduction of background and contamination noise. Incident and diffracted neutron beams travel through high-pressure device, which causes attenuation of neutron. We have studied the method of attenuation correction and analyzed crystal structure using corrected neutron diffraction pattern.
