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Journal Articles

Synchrotron radiation X-ray diffraction method

Hayashi, Makoto*; Shobu, Takahisa

Residual Stress, p.100 - 132, 2021/00

Structural materials may undergo fatigue fracture or stress corrosion cracking during use. One of the causes is the residual stress generated by heat treatment and processing in the manufacturing process of structural materials. There are various methods for measuring the residual stress. This book introduces measurement techniques using ultrasonic and magnetic methods, starting with laboratory X-rays, synchrotron radiation X-rays, and neutrons. In addition, we will outline examples of measurement of residual stress due to processing and welding of various materials, measurement examples of actual machines, change behavior of residual stress due to static and repeated loads, and evaluation methods of fatigue remaining life based on the change behavior.

Journal Articles

Development of bulk texture measurement technique by time-of-flight neutron diffraction

Xu, P. G.; Hoshikawa, Akinori*; Hayashi, Makoto*; Akita, Koichi; Morii, Yukio*; Ishigaki, Toru*

Nihon Zairyo Gakkai Dai-48-Kai X Sen Zairyo Kyodo Ni Kansuru Shimpojiumu Koen Rombunshu, p.7 - 9, 2014/07

Journal Articles

Development of residual stress measurement apparatus by neutron diffraction and its application to bent carbon steel

Hayashi, Makoto*; Okido, Shinobu*; Minakawa, Nobuaki; Morii, Yukio

Zairyo, 47(4), p.420 - 426, 1998/04

no abstracts in English

Oral presentation

Design of the neutron optics for Ibaraki biomolecular diffractometer

Ohara, Takashi; Kurihara, Kazuo; Kusaka, Katsuhiro; Hosoya, Takaaki; Tanaka, Ichiro*; Niimura, Nobuo*; Ozeki, Tomoji*; Aizawa, Kazuya; Morii, Yukio; Arai, Masatoshi; et al.

no journal, , 

no abstracts in English

Oral presentation

Current status of IBARAKI biological diffractometer in J-PARC; Optimization of design parameters

Kusaka, Katsuhiro; Ohara, Takashi; Tanaka, Ichiro*; Niimura, Nobuo*; Kurihara, Kazuo; Hosoya, Takaaki; Ozeki, Tomoji*; Aizawa, Kazuya; Morii, Yukio; Arai, Masatoshi; et al.

no journal, , 

Ibaraki prefecture has started to construct IBARAKI biological crystal diffractometer for industrial use at MLF, J-PARC. It is designed to achieve the efficiency which is more than 50 times larger than the present high performance diffractometer BIX-4. To realize this performance, the diffractometer will be installed on a coupled moderator has more intense peak but wider pulse shape than a decoupled one. It is expected that some neighbor Bragg spots will overlap partially each other along the time axis. The overlapping of Bragg spots should be considered for optimization of design parameters and it is necessary to de-convolute the overlapped spots. The three original simulation programs of TOF diffraction data with designed parameters of the diffractometer were developed to obtain information of spot-overlapping, completeness of Bragg spots and spot profiles along the time axis. The consideration of important designed parameters will be reported based on the simulation results.

Oral presentation

IBARAKI materials design diffractometer; Versatile neutron diffractometer at J-PARC

Ishigaki, Toru; Hoshikawa, Akinori; Yonemura, Masao*; Kamiyama, Takashi*; Aizawa, Kazuya; Sakuma, Takashi*; Tomota, Yo*; Morii, Yukio; Arai, Masatoshi; Hayashi, Makoto*; et al.

no journal, , 

Ibaraki prefecture, the local government of the area for J-PARC site, was decided to build a versatile neutron diffractometer (IBARAKI Materials Design Diffractometer) to promote an industrial application for neutron beam in J-PARC. This diffractometer is planned to be a high throughput diffractometer so that materials engineers and scientists can use it like the chemical analytical instruments in their materials development process. It covers in d range 0.18 $$<$$ d (${AA}$) $$<$$ 5 with $$Delta$$ d/d = 0.16 % at high resolution bank, and covers $$<$$ d (${AA}$) $$<$$ 800 with gradually changing resolution at three detector bank (90 degree, low angle and small angle). Typical measuring time to obtain a "Rietveld-quality" data is several minutes with the sample size of laboratory X-ray diffractometer. To promote industrial application, a utilization system for this diffractometer is required. We will establish a support system for both academic and industrial users who are willing to use neutron but have not been familiar with neutron diffraction. The construction of this instrument was already beginning and will be completed in the beginning of 2008, as one of day-one instruments for J-PARC. The current status for this instrument also will be reported.

Oral presentation

Current status of IBARAKI biological diffractometer in J-PARC; Design of the neutron optics

Ohara, Takashi; Kurihara, Kazuo; Kusaka, Katsuhiro; Hosoya, Takaaki; Tanaka, Ichiro*; Niimura, Nobuo*; Ozeki, Tomoji*; Aizawa, Kazuya; Morii, Yukio; Arai, Masatoshi; et al.

no journal, , 

Ibaraki Prefectural Government in Japan has started to construct a TOF single crystal neutron diffractometer for biological macromolecules for industrial use at J-PARC. For this diffractometer, design of an efficient neutron transportation system is important because this diffractometer has 40m source-sample distance. Recently, we designed a supermirror neutron guide which can transport 0.7-3.8 Angstrom neutron efficiently. The total length of the mirror section is 25m. At the first 17m, the mirror has curvature (R=4300m) for horizontal direction in order to remove high-energy neutron and $$gamma$$ ray. Simultaneously, all of the mirror section has tapered angle for vertical direction in order to reduce the frequency of neutron reflection at the surface of the supermirror. The neutron flux and profile at the sample position was calculated by Monte Carlo simulation softwares, McStas and IDEAS and compared with a curved, non-tapered guide we had designed previously. In result, the new supermirror system has 2 times gain for 0.7 Angstrom neutron and 1.5 times for 1.5 Angstrom neutron, and the beam profile at the sample position has a rectangular shape.

Oral presentation

Industrial application of neutron stress measurement in Japan

Saito, Toru; Hayashi, Makoto*; Kobayashi, Shinsho*; Morii, Yukio

no journal, , 

Recently, each industry is searching for the most suitable manufacturing process to reduce the cost. Especially, the production method of material, the improvement of processing technique, and the selection of cheap materials are being discussed. Therefore, it is the top-priority issue to examine safety and reliability of the material strength to reexamine these. In the industrial user, residual stress has been evaluated by the X-ray stress measurement or by the finite element method (FEM) etc. Neutron is the only one probe to measure the lattice strain nondestructively at the deep inside of materials. The promotion program of technology transfer on neutron application has been implementing in Japan since 2006. The experiments executed in this program are the residual stress evaluation in the welded boiler tube, carburized steel, and welded sample that imitates the stress measurement in the large structure etc. Some experimental results obtained in the program will be presented at this conference.

Oral presentation

Current status of IBARAKI biological crystal diffractometer in J-PARC

Tanaka, Ichiro*; Ohara, Takashi; Kurihara, Kazuo; Kusaka, Katsuhiro*; Hosoya, Takaaki; Tomoyori, Katsuaki*; Niimura, Nobuo*; Ozeki, Tomoji*; Aizawa, Kazuya; Arai, Masatoshi; et al.

no journal, , 

IBARAKI Biological Crystal Diffractometer is a new single-crystal neutron diffractometer for biological and chemical crystallography, and is now being constructed at J-PARC by Ibaraki Prefectural Government in Japan. This diffractometer is designed for the protein crystals with the cell dimension up to 135 ${AA}$. The measurement efficiency is more than 50 times larger than the present neutron diffractometer, BIX-3/BIX-4 in JRR-3 reactor at JAEA. To achieve this performance, we have selected a coupled moderator, and worked out the optimisation of the neutron guide tube. For the detector, a new wavelength-shifting-fiber type scintillation area detector system with high spatial (0.5-1.0 mm) and time (1ms-) resolution are in development.

Oral presentation

Replacement of diffusers on JRR-3 secondary cooling tower

Imahashi, Masaki; Oba, Toshinobu; Oki, Keiichi; Suzuki, Makoto; Hayashi, Kazuhiko

no journal, , 

no abstracts in English

Oral presentation

Reliability of rapid bulk texture measurement using iMATERIA time-of-flight neutron diffractometer

Xu, P. G.; Hoshikawa, Akinori*; Ishigaki, Toru*; Hayashi, Makoto*; Minemura, Tetsuro*; Harjo, S.; Akita, Koichi

no journal, , 

Oral presentation

Status of JRR-3 corresponding to new regulatory standards, 2; Protection from external events

Suzuki, Makoto; Kawamura, Sho; Kobayashi, Tetsuya; Horiguchi, Hironori; Wada, Shigeru

no journal, , 

no abstracts in English

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