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Journal Articles

Post irradiation experiment about SiC-coated oxidation-resistant graphite for high temperature gas-cooled reactor

Shibata, Taiju; Mizuta, Naoki; Sumita, Junya; Sakaba, Nariaki; Osaki, Takashi*; Kato, Hideki*; Izawa, Shoichi*; Muto, Takenori*; Gizatulin, S.*; Shaimerdenov, A.*; et al.

Proceedings of 9th International Topical Meeting on High Temperature Reactor Technology (HTR 2018) (USB Flash Drive), 7 Pages, 2018/10

Graphite materials are used for the in-core components of High Temperature Gas-cooled Reactor (HTGR). Oxidation damage on the graphite components in air ingress accident is a crucial issue for the safety point of view. SiC coating on graphite surface is a possible technique to enhance oxidation resistance. However, it is important to confirm the integrity of this material against high temperature and neutron irradiation for the application of the in-core components. JAEA and Japanese graphite companies carried out the R&D to develop the oxidation-resistant graphite. JAEA and INP investigated the irradiation effects on the oxidation-resistant graphite by using a framework of ISTC partner project. This paper describes the results of post irradiation experiment about the neutron irradiated SiC-coated oxidation-resistant graphite. A brand of oxidation-resistant graphite shows excellent performance against oxidation test after the irradiation.

Journal Articles

Enhancement of oxidation tolerance of graphite materials for high temperature gas-cooled reactor

Mizuta, Naoki; Sumita, Junya; Shibata, Taiju; Osaki, Takashi*; Kato, Hideki*; Izawa, Shoichi*; Muto, Takenori*; Gizatulin, S.*; Sakaba, Nariaki

Tanso Zairyo Kagaku No Shinten; Nihon Gakutsu Shinkokai Dai-117-Iinkai 70-Shunen Kinen-Shi, p.161 - 166, 2018/10

To enhance oxidation resistance of graphite material for in-core components of HTGR, JAEA and four Japanese graphite companies; Toyo Tanso, IBIDEN, Tokai Carbon and Nippon Techno-Carbon, are carrying out for development of oxidation-resistant graphite by CVD-SiC coating. This paper describes the outline of neutron irradiation test about the oxidation-resistant graphite by WWR-K reactor of INP, Kazakhstan through an ISTC partner project. Prior to the irradiation test, the oxidation-resistant graphite by CVD-SiC coating of all specimens showed enough oxidation resistance under un-irradiation condition. The neutron irradiation test was already completed and out-of-pile oxidation test will be carried out at the hot-laboratory of WWR-K.

Journal Articles

Irradiation test about oxidation-resistant graphite in WWR-K research reactor

Shibata, Taiju; Sumita, Junya; Sakaba, Nariaki; Osaki, Takashi*; Kato, Hideki*; Izawa, Shoichi*; Muto, Takenori*; Gizatulin, S.*; Shaimerdenov, A.*; Dyussambayev, D.*; et al.

Proceedings of 8th International Topical Meeting on High Temperature Reactor Technology (HTR 2016) (CD-ROM), p.567 - 571, 2016/11

Graphite are used for the in-core components of HTGR, and it is desirable to enhance oxidation resistance to keep much safety margin. SiC coating is the candidate method for this purpose. JAEA and four Japanese graphite companies are studying to develop oxidation-resistant graphite. Neutron irradiation test was carried out by WWR-K reactor of INP of Kazakhstan through ISTC partner project. The total irradiation cycles of WWR-K operation was 10 cycles by 200 days. Irradiation temperature about 1473 K would be attained. The maximum fast neutron fluence (E $$>$$0.18 MeV) for the capsule irradiated at a central irradiation hole was preliminary calculated as 1.2$$times$$10$$^{25}$$/m$$^{-2}$$, and for the capsule at a peripheral irradiation hole as 4.2$$times$$10$$^{24}$$/m$$^{-2}$$. Dimension and weight of the irradiated specimens were measured, and outer surface of the specimens were observed by optical microscope. For the irradiated oxidation resistant graphite, out-of-pile oxidation test will be carried out at an experimental laboratory.

Journal Articles

Irradiation test plan of oxidation-resistant graphite in WWR-K research reactor

Sumita, Junya; Shibata, Taiju; Sakaba, Nariaki; Osaki, Hiroki*; Kato, Hideki*; Fujitsuka, Kunihiro*; Muto, Takenori*; Gizatulin, S.*; Shaimerdenov, A.*; Dyussambayev, D.*; et al.

Proceedings of 7th International Topical Meeting on High Temperature Reactor Technology (HTR 2014) (USB Flash Drive), 7 Pages, 2014/10

Graphite materials are used for the in-core components of High Temperature Gas-cooled Reactor(HTGR)which is a graphite-moderated and helium gas-cooled reactor. In the case of air ingress accident in HTGR, SiO$$_{2}$$ protective layer is formed on the surface of SiC layer in TRISO CFP and oxidation of SiC does not proceed and fission products are retained inside the fuel particle. A new safety concept for the HTGR, called Naturally Safe HTGR, has been recently proposed. To enhance the safety of Naturally Safe HTGR ultimately, it is expected that oxidation-resistant graphite is used for graphite components to prevent the TRISO CFPs and fuel compacts from failure. SiC coating is one of candidate methods for oxidation-resistant graphite. JAEA and four graphite companies launched R&Ds to develop the oxidation-resistant graphite and the International Science and Technology Center(ISTC) partner project with JAEA and INP was launched to investigate the irradiation effects on the oxidation-resistant graphite. To determine grades of the oxidation-resistant graphite which will be adopted as irradiation test, a preliminary oxidation test was carried out. This paper described the results of the preliminary oxidation test, the plan of out-of-pile test, irradiation test and post-irradiation test(PIE)of the oxidation-resistant graphite.

Journal Articles

R&D plan for development of oxidation-resistant graphite and investigation of oxidation behavior of SiC coated fuel particle to enhance safety of HTGR

Ueta, Shohei; Sumita, Junya; Shibata, Taiju; Aihara, Jun; Fujita, Ichiro*; Ohashi, Jun*; Nagaishi, Yoshihide*; Muto, Takenori*; Sawa, Kazuhiro; Sakaba, Nariaki

Nuclear Engineering and Design, 271, p.309 - 313, 2014/05

 Times Cited Count:9 Percentile:57.39(Nuclear Science & Technology)

A new concept of the high temperature gas-cooled reactor (HTGR) is proposed as a challenge to assure no event sequences to the harmful release of radioactive materials even when the design extension conditions (DECs) occur by deterministic approach based on the inherent safety features of the HTGR. The air/water ingress accident, one of the DECs for the HTGR, is prevented by additional measures (e.g. facility for suppression to air ingress). With regard to the core design, it is important to prevent recriticality accidents by keeping the geometry of the fuel rod which consists of the graphite sleeve, fuel compact and SiC-TRISO (TRIstructural-ISOtropic) coated fuel particle, and by improving the oxidation resistance of the graphite when air/water ingress accidents occur. Therefore, it is planned to develop the oxidation-resistant graphite, which is coated with gradient SiC layer. It is also planned that the experimental identification of the condition to form the stable oxide layer (SiO$$_{2}$$) for SiC layer on the oxidation-resistant graphite and on the SiC-TRISO fuel. This paper describes the R&D plan for un-irradiation and irradiation test under simulating air/water ingress accident condition to develop oxidation-resistant graphite and to investigate the oxidation behavior of SiC coated fuel particle.

Journal Articles

R&D plan for development of oxidation-resistant graphite and investigation of oxidation behavior of SiC coated fuel particle to enhance safety of HTGR

Ueta, Shohei; Sumita, Junya; Shibata, Taiju; Aihara, Jun; Fujita, Ichiro*; Ohashi, Jun*; Nagaishi, Yoshihide*; Muto, Takenori*; Sawa, Kazuhiro; Sakaba, Nariaki

Proceedings of 6th International Topical Meeting on High Temperature Reactor Technology (HTR 2012) (USB Flash Drive), 6 Pages, 2012/10

A new concept of the High Temperature Gas-cooled Reactor (HTGR), so-called the Naturally Safe HTGR, is proposed as a challenge to assure no event sequences to the harmful release of radioactive materials even when the design extension conditions such as the air/water ingress accidents occur by deterministic approach based on the inherent safety features of the HTGR. For the Naturally Safe HTGR it is important to prevent recriticality accidents by keeping the geometry of the fuel rod which consists of the graphite sleeve, fuel compact and SiC-TRISO coated fuel particle, and by improving the oxidation resistance of the graphite when air/water ingress accidents occur. This paper describes the R&D plan for un-irradiation and irradiation test under simulating air/water ingress accident condition to develop oxidation-resistant graphite and to investigate the oxidation behavior of SiC coated fuel particle.

Oral presentation

Collaboration with Republic of Kazakhstan regarding development of HTGR, 3; Collaboration of development of oxidation-resistant graphite material for HTGR

Shibata, Taiju; Sumita, Junya; Nagata, Hiroshi; Saito, Takashi; Tsuchiya, Kunihiko; Sakaba, Nariaki; Osaki, Hiroki*; Kato, Hideki*; Fujitsuka, Kunihiro*; Muto, Takenori*; et al.

no journal, , 

no abstracts in English

Oral presentation

Digital image analysis of isotropic graphite porosity using 3D X-ray computed tomography

Sumita, Junya; Shibata, Taiju; Muto, Takenori*; Mihashi, Masahiko*; Sato, Masahiro*; Yamashita, Ryo*; Sakaba, Nariaki

no journal, , 

Since graphite is porous material containing 20% of porosity, the characteristics of graphite strongly depends on shape and volume distribution of pore. It is essential to establish the production method for further reducing the characteristic variation of graphite to produce high quality graphite. Therefore, it is necessary to establish the simple method for prediction of the characteristics of graphite. Although they have been characterized as a function of porosity, it is necessary to characterize them as a function of some detailed factors in order to further reduce the characteristic variation and to characterize them with high accuracy. The authors have been developing the method for predicting the characteristics of graphite by analysis of shape and volume distribution of open pore and closed pore using two and three dimensional images in order to characterize graphite with high accuracy. In the present study, quantity of open pore and closed pore analyzed by a digital image analysis was compared with that measured by a mercury porosimeter. Both results indicated that open pore increased with increasing porosity and closed pore showed almost constant value. However, the volume of closed pore by the mercury porosimeter was measured up to 5% larger than that by the digital image analysis. It is necessary to clarify the correlation between the volume of closed pore analyzed by the digital image analysis and that measured by the mercury porosimeter to measure closed pore with high accuracy by the mercury porosimeter in the next step.

Oral presentation

Evaluation on thermal conductivity of fine-grain isotropic graphite on the basis of its porosity

Sumita, Junya; Shibata, Taiju; Muto, Takenori*; Mihashi, Masahiko*; Sato, Masahiro*; Yamashita, Ryo*; Sakaba, Nariaki

no journal, , 

Graphite materials are used for the in-core components of High Temperature Gas-cooled Reactor (HTGR) which is a graphite-moderated and helium gas-cooled reactor. The HTGR is particularly attractive due to capability of producing high temperature helium gas, and its passive and inherent safety features. The Very High Temperature Reactor (VHTR) is one of the most promising candidates as the Generation-IV nuclear reactor systems. Since the thermal conductivity of graphite is one of important properties to evaluate the maximum core temperature of the VHTR, many researchers investigated and reported it. Graphite material is porous material containing 20% of porosity and the thermal conductivity strongly depends on shape and volume distribution of pore. It is important to evaluate the thermal conductivity as a function of them. In the presentation, the evaluation results of the thermal conductivity for fine-grain isotropic graphite as a function of open pores and closed pores measured by a mercury porosimeter were reported. Moreover, the prediction method for the thermal conductivity considering the amount of open and closed pore was discussed.

Oral presentation

Dependency on pore distribution of thermal property of isotropic graphite

Sumita, Junya; Shibata, Taiju; Mihashi, Masahiko*; Muto, Takenori*; Sato, Masahiro*; Yamashita, Ryo*; Sakaba, Nariaki

no journal, , 

The characteristics of graphite have been characterized as a function of porosity. In order to further reduce the characteristic variation and to characterize them with high accuracy, it is necessary to characterize them as a function of some detailed factors. Therefore, we focused on the open and closed pore of graphite and analyzed them based on two and three dimensional images to develop the prediction method for thermal conductivity of graphite. In the present study, it was reported analytical results of pore distribution and comparison result of predicted thermal conductivity to the experimental one.

Oral presentation

The Effect of porosity on isotropic graphite properties

Mihashi, Masahiko*; Muto, Takenori*; Sato, Masahiro*; Sumita, Junya; Shibata, Taiju; Sakaba, Nariaki; Yamashita, Ryo*

no journal, , 

The large size isotropic graphite is required to have small characteristic variation. Since characteristics of graphite are affected by porosity, in the first stage of improvement of large size graphite, porosity of large size isotropic graphite has been examined using mercury porosimeter.

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